Skip to main content
SpringerLink
Log in

SYNTHESIS, CHARACTERIZATION, AND COMPUTATIONAL STUDIES OF N-[(9E)-8,10,17-TRIAZATETRACYCLO[8.7.0.02,7.011,16]HEPTADECA- 1(17),2,4,6,11(16),12,14-HEPTAEN-9-YLIDENE]BENZAMIDE

  • Published:
Journal of Structural Chemistry Aims and scope Submit manuscript

This article has been updated

Abstract

N-[(9E)-8,10,17-Triazatetracyclo[8.7.0.02,7.011,16]heptadeca-1(17),2,4,6,11(16),12,14-heptaen-9-ylidene] benzamide (I) is synthesized and characterized by spectroscopy, microanalysis, and single crystal X-ray diffractometry. Compound I crystallizes in the monoclinic space group P21/c with a = 15.8980(7) Å, b = 4.8067(2) Å, c = 21.0455(10) Å, β = 101.153(2)°, and Z = 4. The experimental bond lengths and bond angles are contrasted with computed bond lengths and bond angles.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Scheme 1
Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7

Similar content being viewed by others

Change history

  • 28 October 2020

    Added ESM information into HTML version of the Article.

REFERENCES

  1. T. M. Das, C. P. Rao, and E. Kolehmainen. Carbohydr. Res., 2001, 334, 261–269.

  2. Y. S. Chhonker, B. Veenu, S. R. Hasim, N. Kaushik, D. Kumar, and P. Kumar. Eur. J. Adv. Chem. Res., 2009, 6(S1), S342–S346.

  3. H. Pessoa-Mahana, C. D. Pessoa-Mahana, R. Salazar, J. A. Valderrama, E. Saez, and R. Araya-Maturana. Synthesis, 2004, 3, 436–440.

  4. P. P. Joshi and S. G. Shirodkar. World J. Pharm. Pharm. Sci., 2014, 3(9), 950–958.

  5. B. A. Insuasty, H. Torres, J. Quiroga, R. Abonia, R. Rodriguez, M. Nogeras, A. Sanchez, C. Saitz, S. L. Avarez, and S. A. Zacchino. J. Chil. Chem. Soc., 2006, 51(2), 927–932.

  6. A. L. Bagdasarian, H. H. Nguyen. T. A. Palazzo, J. C. Fettinger, M. J. Haddadin, and M. J. Kurth. J. Org. Chem., 2016, 81, 3924–3928.

  7. H. C. Ouyang, R. Y. Tang, P. Zhong, X. G. Zhang, and J. H. Li. J. Org. Chem., 2011, 76, 223–228.

  8. X. Ji, Y. Zhou, J. Wang, H. Zhao, H. Jiang, and H. Liu. J. Org. Chem., 2013, 78, 4312–4318.

  9. A. J. Ndakala, R. K. Gessner, P. W. Gitari, N. October, K. L. White, A. Hudson, F. Fakorede, D. M. Shackleford, M. Kaiser, C. Yeates, S. A. Charman, and K. Chibale. J. Med. Chem., 2011, 54, 4581–4589.

  10. I. T. Weber and J. Agniswamy. Viruses, 2009, 1, 1110–1136.

  11. G. Dou, M. Wang, and D. Shi. J. Comb. Chem., 2009, 11, 151–154.

  12. Z. Li, H. Huang, H. Sun, H. Jiang, and H. Liu. J. Comb. Chem., 2008, 10, 484–486.

  13. APEX2, SADABS and SAINT. Madison, Bruker AXS: WI, USA, 2010.

  14. G. M. Sheldrick. Acta. Crystallogr., Sect. A, 2008, 64, 112–122.

  15. C. B. Hübschle, G. M. Sheldrick, and B. Dittrich. J. Appl. Crystallogr., 2011, 44, 1281–1284.

  16. M. J. Frisch, G. W. Trucks, H. B. Schlegel, G. E. Scuseria, M. A. Robb, J. R. Cheeseman, J. A. Montgomery, T. Vreven, K. N. Kadin, J. C. Burant, J. M. Millam, S. S. Iyengar, J. Tomasi, V. Barone, B. Mennucci, M. Cossi, G. Scalmani, N. Rega, G. A. Petersson, H. Nakatsuji, M. Hada, M. Hears, K. Toyota, R. Fukuda, J. Hasegawa, M. Ishida, T. Nakajim, Y. Honda, O. Kitao, H. Nakai, M. Klene, X. Li, J. E. Knox, H. P. Hratchian, J. B. Cross, V. Bakken, C. Adamo, J. Jaramillo, R. Gomperts, R. E. Stratmann, O. Yazyev, A. J. Austin, R. Cammi, C. Pomelli, J. W. Ochterski, P. Y. Ayala, K. Morokuma, G. A. Voth, P. Salvador, J. J. Dannenberg, V. G. Zakrzewski, S. Dapprich, A. D. Daniels, M. C. Strain, O. Farkas, D. K. Malick, A. D. Rabuck, K. Raghavachari, J. B. Foresman, J. V. Ortiz, Q. Cui, A. G. Baboul, S. Clifford, J. Cioslowski, B. B. Stefanov, G. Liu, A. Liashenko, P. Piskorz, I. Komaromi, R. L. Martin, D. J. Fox, T. Keith, M. A. Al-Laham, C. Y. Peng, A. Nanayakkara, M. Challacombe, P. M. W. Gill, B. Johnson, W. Chen, M. W. Wong, C. Gonzalez, J. A. Pople. Gaussian 03, revision B03. Gaussian: Pittsburgh, 2003.

  17. P. C. Hariharan and J. A. Pople. Theor. Chim. Acta, 1973, 28, 213–322.

  18. P. C. Hariharan and J.A. Pople. Mol. Phys., 1974, 27, 209–214.

  19. W. Kohn, A. D. Becke, and R. G. Parr. J. Phys. Chem., 1996, 100, 12974–12980.

  20. A. Frisch, A. B. Nielson, and A. J. Holder. GAUSSVIEW User Manual. Gaussian: Pittsburg, 2000.

  21. F. Odame, E. C. Hosten, and Z. R. Tshentu. J. Struct. Chem., 2018, 59(8), 1804–1809.

  22. F. Odame and E. C. Hosten. Acta Chim. Slov., 2018, 65, 531–538.

Download references

Author information

Authors and Affiliations

  1. Department of Basic Sciences, University of Health and Allied Sciences, Ho, Republic of Ghana

    F. Odame

  2. Department of Chemistry, Nelson Mandela University, Port Elizabeth, Republic of South Africa

    F. Odame, E. C. Hosten & Z. R. Tshentu

Authors
  1. F. Odame
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. E. C. Hosten
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Z. R. Tshentu
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to F. Odame.

Ethics declarations

The authors declare that they have no conflict of interests.

Supplementary material

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Odame, F., Hosten, E.C. & Tshentu, Z.R. SYNTHESIS, CHARACTERIZATION, AND COMPUTATIONAL STUDIES OF N-[(9E)-8,10,17-TRIAZATETRACYCLO[8.7.0.02,7.011,16]HEPTADECA- 1(17),2,4,6,11(16),12,14-HEPTAEN-9-YLIDENE]BENZAMIDE. J Struct Chem 61, 1177–1185 (2020). https://doi.org/10.1134/S0022476620080016

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S0022476620080016

Keywords

Search

Navigation