Skip to main content
Log in

Small-angle X-ray studies of the GaAs0.7Se0.3 solid solution at energies close to as and Se absorption edges

  • Proceedings of the Conference “Methods for Studying the Composition and Structure of Functional Materials,” October 21–25, 2013, Novosibirsk
  • Published:
Journal of Structural Chemistry Aims and scope Submit manuscript

Abstract

The possibility of a simultaneous use of X-ray diffraction and X-ray absorption techniques in order to characterize the sizes, shapes, and chemical composition of grains in a sample (the solution of the extended uncertainty problem due to the Babinet principle) is shown. A sample of the GaAs0.7Se0.3/GaAs solid solution is investigated on the developed laboratory device for a simultaneous performance of X-ray diffraction and X-ray absorption experiments. It is shown that the GaAs0.7Se0.3 sample decomposes into separate GaAs and GaSe domains forming a mosaic structure. The sizes of GaAs and GaSe domains are estimated. Components with a linear geometry are sometimes revealed in the composition of GaSe grains.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. Z. G. Pinsker, Dynamic X-Ray Scattering in Ideal Crystals [in Russian], Nauka, Moscow (1974).

    Google Scholar 

  2. M. D. Sharkov, K. Yu. Pogrebitskii, and S. G. Konnikov, Technical Physics Letters, 33, No. 7, 619 (2007).

    Article  CAS  Google Scholar 

  3. D. C. Koningsberger and R. Prins (eds.), in: X-Ray Absorption: Principles, Applications, Techniques of EXAFS, SEXAFS, and XANES, V. 92, Eindhoven, The Netherlands: Eindhoven University of Technology; John Wiley & Sons Inc., New York-Chichester-Brisbane-Toronto-Singapore (1988).

    Google Scholar 

  4. M. D. Sharkov, K. Ju. Pogrebitsky, M. E. Boiko, and S. G. Konnikov, Precision Instrument and Mechanology,. 1, No. 2, 32 (2012).

    Google Scholar 

  5. K. Yu. Pogrebitskii and M. D. Sharkov, Semiconductors, 44, No. 6, 723 (2010).

    Article  Google Scholar 

  6. O. Glatter and O. Kratky (eds.), in: Small Angle X-Ray Scattering, Academic Press, London (1982).

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to M. D. Sharkov.

Additional information

Original Russian Text © 2014 M. D. Sharkov, M. E. Boiko, A. M. Boiko, A. V. Bobyl, S. G. Konnikov.

__________

Translated from Zhurnal Strukturnoi Khimii, Vol. 55, No. 4, pp. 821–825, July–August, 2014.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Sharkov, M.D., Boiko, M.E., Boiko, A.M. et al. Small-angle X-ray studies of the GaAs0.7Se0.3 solid solution at energies close to as and Se absorption edges. J Struct Chem 55, 786–790 (2014). https://doi.org/10.1134/S0022476614040301

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S0022476614040301

Keywords

Navigation