Abstract
The 1-(diphenylmethylene)-2-(thiazolo[4,5-b]pyridin-2-yl)hydrazine compound (IV) is synthesized based on a 3-amion-2-chloropyridine precursor and characterized by single crystal X-ray diffraction. The structural analysis reveals that compound IV belongs to the monoclinic system, space group P21/c, a = 11.869(5) Å, b = 13.155(6) Å, c = 10.970(5) Å, β = 102.431(5)°, V = 1672.6(12) Å3, Z = 4. In the crystal structure, the molecular species are linked by intermolecular N-H...N hydrogen bonds into onedimensional chains.
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References
O. O. Ajani, C. A. Obafemi, O. C. Nwinyi, et al., Bioorg. Med. Chem., 18, No. 1, 214–221 (2010).
J. R. Dimmock, S. C. Vashishtha, and J. P. Stables, Eur. J. Med. Chem., 35, No. 2, 241–248 (2000).
C. Loncle, J. M. Brunel, N. Vidal, et al., Eur. J. Med. Chem., 39, No. 12, 1067–1071 (2004).
L. W. Zheng, L. L. Wu, B. X. Zhao, et al., Bioorg. Med. Chem., 17, No. 5, 1957–1962 (2009).
S. Gemma, L. Savini, M. Altarelli, et al., Bioorg. Med. Chem., 17, No. 16, 6063–6072 (2009).
O. I. El-Sabbagh and H. M. Rady, Eur. J. Med. Chem., 44, No. 9, 3680–3686 (2009).
S. J. Peng, J. Chem. Crystallogr., 41, No. 3, 280–285 (2011).
S. Mukherjee, S. Chowdhury, A. P. Chattapadhyay, et al., Inorg. Chim. Acta, 373, No. 1, 40–46 (2011).
A. Bacchi, M. Carcelli, P. Pelagatti, et al., J. Inorg. Biochem., 75, No. 2, 123–133 (1999).
T. Horiuchi, J. Chiba, K. Uoto, et al., Bioorg. Med. Chem. Lett., 19, No. 2, 305–308 (2009).
F. Chimenti, B. Bizzarri, A. Bolasco, et al., Eur. J. Med. Chem., 46, No. 1, 378–382 (2011).
M. A. A. El-Sayed, N. A. Abdel-Aziz, A. A.M. Abdel-Aziz, et al., Bioorg. Med. Chem., 19, No. 11, 3416–3424 (2011).
J. Easmon, G. Heinisch, J. Hofmann, et al., Eur. J. Med. Chem., 32, No. 5, 397–408 (1997).
H. R. Lawrence, Z. Li, M. L. R. Yip, et al., Bioorg. Med. Chem. Lett., 19, No. 14, 3756–3759 (2009).
I. G. Pervova, S. A. Melkozerov, P. A. Slepukhin, et al., Russ. J. Gen. Chem., 80, No. 5, 817–823 (2010).
S. R. Girish, V. K. Revankar, and V. B. Mahale, Transition. Met. Chem., 21, No. 5, 401–405 (1996).
G. M. Sheldrick, SHELXS-97 and SHELXL-97, Programs for Crystal Structure Refinement, Univ. Göttingen, Germany (1997).
C. L. Klein, D. Gray, and E. D. Stevens, Struct. Chem., 4, No. 6, 377–384 (1993).
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Original Russian Text © 2014 S. B. Miao, B. M. Ji, L. Zhou.
The text was submitted by the authors in English. Zhurnal Strukturnoi Khimii, Vol. 55, No. 2, pp. 405–408, March–April, 2014.
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Miao, S.B., Ji, B.M. & Zhou, L. Crystal structure of 1-(diphenylmethylene)-2-(thiazolo[4,5-b]pyridin-2-yl)hydrazine. J Struct Chem 55, 384–387 (2014). https://doi.org/10.1134/S0022476614020310
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DOI: https://doi.org/10.1134/S0022476614020310