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Synthesis and structure investigation of Co(III) complex salts with the perrhenate anion

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Abstract

Complex salts of the composition [Co(NH3)6](ReO4)3·2H2O (I), [Co(en)3](ReO4)3 (II), [Co(NH3)5H2O](ReO4)3·2H2O (III), and [Co(NH3)5Cl](ReO4)2·0.5H2O (IV) are obtained. Their crystal structures are determined by single crystal XRD. Crystallographic characteristics: (I) a = 9.9797(3) Å, b = 12.6994(3) Å, c = 14.7415(4) Å, β = 102.870(1)°, C2/c space group; (II) a = 8.0615(3) Å, b = 8.4483(4) Å c = 8.8267(4) Å, α = 61.923(2)°, β = 89.552(2)°, γ = 72.295(2)°, P1 space group; (III) a = 8.0086(4) Å, b = 12.9839(6) Å, c = 17.5122(7) Å, β=91.858(1)°, P21/n space group; (IV) a = 14.9446(3) Å, b = 14.6562(4) Å, c = 12.2434(4) Å, Cmc21 space group.

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Authors and Affiliations

  1. A. V. Nikolaev Institute of Inorganic Chemistry, Siberian Division, Russian Academy of Sciences, Novosibirsk, Russia

    I. A. Baidina, E. Yu. Filatov, E. V. Makotchenko & A. I. Smolentsev

  2. Novosibirsk State University, Novosibirsk, Russia

    E. Yu. Filatov & E. V. Makotchenko

Authors
  1. I. A. Baidina
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  2. E. Yu. Filatov
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  3. E. V. Makotchenko
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  4. A. I. Smolentsev
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Correspondence to I. A. Baidina.

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Original Russian Text Copyright © 2012 by I. A. Baidina, E. Yu. Filatov, E. V. Makotchenko, and A. I. Smolentsev

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Translated from Zhurnal Strukturnoi Khimii, Vol. 53, No. 1, pp. 117–123, January–February, 2012.

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Baidina, I.A., Filatov, E.Y., Makotchenko, E.V. et al. Synthesis and structure investigation of Co(III) complex salts with the perrhenate anion. J Struct Chem 53, 112–118 (2012). https://doi.org/10.1134/S0022476612010143

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  • DOI: https://doi.org/10.1134/S0022476612010143

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