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Use of plasma atomic emission spectrometry for the quality control of grade lead

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Abstract

An inductively coupled plasma atomic emission spectroscopy method for speciation of Ag, Cu, Bi, Sb, As, Ni, Cd, Zn, Sn, and Fe in grade lead is described. The spectrometer was calibrated using water solutions with known concentrations of trace elements. The matrix effects were taken into account using an internal standard added to the reference-sample, calibrated-blank, reagent-blank, and tested-sample solutions. The metrological examination of the technique was accomplished. The repeatability rms error does not exceed 0.10. The systematic error is not statistically significant.

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Authors and Affiliations

  1. Subsidiary State Enterprise “Eastern Research Institute of Nonferrous Metals,”, Ust’-Kamenogorsk, Kazakhstan

    N. G. Pelevina

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  1. N. G. Pelevina
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Original Russian Text © N. G. Pelevina, 2008, published in Zavodskaya Laboratoriya. Diagnostika materialov, 2008, Vol. 44, No. 14, pp. 12–16.

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Pelevina, N.G. Use of plasma atomic emission spectrometry for the quality control of grade lead. Inorg Mater 44, 1554–1558 (2008). https://doi.org/10.1134/S0020168508140112

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  • DOI: https://doi.org/10.1134/S0020168508140112

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