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Composition, structure, and morphology of the surface of nanodimensional platinum-containing films obtained from sols

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Abstract

This work is aimed at studying the composition, structure, and morphology of the surface of nanodimensional platinum-containing silica films synthesized according to the sol–gel technology. An analysis of the data of optical and atomic-force microscopy, X-ray reflectometry, and the method of the Rutherford backscattering made it possible to reveal the regularities of the effect of the synthesis conditions such as the concentration of the initial reagents, duration of sol ripening, and temperature of treatment on the structure and composition of the films.

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Authors and Affiliations

  1. Institute of Chemistry of Silicates, Russian Academy of Sciences, ul. Makarova 2, St. Petersburg, 199034, Russia

    O. A. Shilova & N. N. Gubanova

  2. St. Petersburg State Electrotechnical University LETI, ul. Prof. Popova 5, St. Petersburg, 197376, Russia

    O. A. Shilova

  3. National Research Center Kurchatov Institute, St. Petersburg Institute of Nuclear Physics, Orlova Roshcha 1, Gatchina, 188300, Russia

    N. N. Gubanova, V. A. Matveev & V. Yu. Bayramukov

  4. Joint Institute forNuclear Research, ul. Joliot-Curie, Dubna, 141980, Russia

    A. P. Kobzev

Authors
  1. O. A. Shilova
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  2. N. N. Gubanova
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  3. V. A. Matveev
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  4. V. Yu. Bayramukov
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  5. A. P. Kobzev
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Correspondence to O. A. Shilova.

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Original Russian Text © O.A. Shilova, N.N. Gubanova, V.A. Matveev, V.Yu. Bayramukov, A.P. Kobzev, 2016, published in Fizika i Khimiya Stekla.

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Shilova, O.A., Gubanova, N.N., Matveev, V.A. et al. Composition, structure, and morphology of the surface of nanodimensional platinum-containing films obtained from sols. Glass Phys Chem 42, 78–86 (2016). https://doi.org/10.1134/S1087659616010168

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  • DOI: https://doi.org/10.1134/S1087659616010168

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