Skip to main content
SpringerLink
Log in

Synthesis of SrFe12O19 magnetic nanoparticles by EDTA complex method

  • Physical Chemistry of Nanoclusters and Nanomaterials
  • Published:
Russian Journal of Physical Chemistry A Aims and scope Submit manuscript

Abstract

A modified polyacrylamide gel route was used to prepare SrFe12O19 magnetic nanoparticles; ethylenediaminetetraacetic acid (EDTA) was used as a carboxyl chelating agent. The phase purity, morphology and magnetic properties of as-prepared samples were analyzed via X-ray diffraction (XRD), Raman spectroscopy, scanning electron microscopy (SEM), transmission electron microscopy (TEM) and vibrating sample magnetometery (VSM). XRD analysis indicates that high-purity SrFe12O19 magnetic nanoparticles can be synthesized at 700°C in air. The characteristic peaks of as-prepared sample at 210, 283, 321, 340, 381, 411, 432, 475, 532, 618, 686, and 726 cm–1 were observed in Raman spectra. SEM and TEM show that the synthesized SrFe12O19 magnetic nanoparticles are uniform with the mean particle size of ~60 nm. VSM measurement shows that the maximum magnetic energy product (BH)max of sample prepared using EDTA as a chelating agent is higher than that of sample prepared using citric acid as a chelating agent.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Log in via an institution

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Institutional subscriptions

Similar content being viewed by others

References

  1. M. Pardavi-Horvath, J. Magn. Magn. Mater. 216, 171 (2000).

    Article  Google Scholar 

  2. H. N. Bertram, Theory of Magnetic Recording (Cambridge Univ. Press, Cambridge, 1994).

    Book  Google Scholar 

  3. Z. F. Zi, Y. P. Sun, X. B. Zhu, Z. R. Yang, and W. H. Song, J. Magn. Magn. Mater. 320, 2746 (2008).

    Article  CAS  Google Scholar 

  4. Y. F. Wang, Q. L. Li, C. R. Zhang, and B. D. Li, J. Magn. Magn. Mater. 321, 3368 (2009).

    Article  CAS  Google Scholar 

  5. C. R. Zhang, Q. L. Li, and Y. Ye, Synth. Met. 159, 1008 (2009).

    Article  CAS  Google Scholar 

  6. Y. F. Wang, Q. L. Li, C. R. Zhang, and H. X. Jing, J. Alloys Compd. 467, 284 (2009).

    Article  CAS  Google Scholar 

  7. X. Yang, Q. Li, J. Zhao, B. Li, and Y. Wang, J. Alloys Compd. 475, 312 (2009).

    Article  CAS  Google Scholar 

  8. M. Jean, V. Nachbaur, J. Bran, and J. M. le Breton, J. Alloys Compd. 496, 306 (2010).

    Article  CAS  Google Scholar 

  9. G. R. Gordani, A. Ghasemi, and A. Saidi, Ceram. Int. 40, 4945 (2014).

    Article  CAS  Google Scholar 

  10. Z. Y. Wang, L. M. Zhong, J. L. Lv, H. C. Qian, Y. L. Zheng, Y. Z. Fang, M. G. Jin, and J. Y. Xu, J. Magn. Magn. Mater. 322, 2782 (2010).

    Article  CAS  Google Scholar 

  11. Y. F. Wang, Q. L. Li, C. R. Zhang, and H. X. Jing, Chin. J. Inorg. Chem. 32, 1983 (2007).

    Google Scholar 

  12. S. F. Wang, C. F. Zhang, G. A. Sun, B. Chen, W. Liu, X. Xiang, H. Wang, L. M. Fang, Q. Tian, Q. P. Ding, and X. T. Zu, J. Sol-Gel Sci. Technol. 73, 371 (2015).

    Article  CAS  Google Scholar 

  13. C. M. Fang, F. Kools, R. Metselaar, G. de With, and R. A. de Groot, J. Phys.: Condens. Matter. 15, 6229 (2003).

    CAS  Google Scholar 

  14. P. Hernandez-Gomez, C. Torres, C. de Francisco, J. M. Munoz, O. Alejos, J. I. Iniguez, and V. Raposo, J. Magn. Magn. Mater. 272–276, 1843 (2004).

    Article  Google Scholar 

  15. R. Ianos, S. Borcănescu, and R. Lazăău, Chem. Eng. J. 240, 260 (2014).

    Article  CAS  Google Scholar 

  16. G. Theophil Anand, L. John Kennedy, U. Aruldoss, and J. Judith Vijaya, J. Mol. Struct. 1084, 244 (2015).

    Article  CAS  Google Scholar 

  17. S. F. Wang, G. Z. Sun, L. M. Fang, L. Lei, X. Xiang, and X. T. Zu, Sci. Rep-UK 5, 12849 (2015).

    Article  CAS  Google Scholar 

  18. R. K. Sahu, O. Mohanta, and A. K. Pramanik, J. Alloy. Comp. 532, 114 (2012).

    Article  CAS  Google Scholar 

  19. A. Morel, J. M. Le Breton, J. Kreisel, G. Wiesinger, F. Kools, and P. Tenaud., J. Magn. Magn. Mater. 242–245, 1405 (2002).

    Article  Google Scholar 

  20. J. Dong, Y. Zhang, X. Zhang, Q. Liu, and J. Wang, Mater. Lett. 120, 9 (2014).

    Article  CAS  Google Scholar 

  21. L. Zhang, and Z. Li, J. Alloy. Comp. 469, 422 (2009).

    Article  CAS  Google Scholar 

  22. H. Kusama, N. Wang, Y. Miseki, and K. Sayama, J. Comb. Chem. 12, 356 (2010).

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. New Technology Research and Development Center, Lanzhou Institute of Physics, Gansu, Lanzhou, 73000, P.R. China

    Shifa Wang, Danming Li, Yuhua Xiao & Wenqiang Dang

  2. Science and Technology on Vacuum Technology and Physics Laboratory, Lanzhou Institute of Physics, Lanzhou, Gansu, 730000, P.R. China

    Shifa Wang, Danming Li, Yuhua Xiao & Wenqiang Dang

  3. Electric Propulsion Division, Lanzhou Institute of Physics, Gansu, Lanzhou, 73000, P.R. China

    Jie Feng

Authors
  1. Shifa Wang
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Danming Li
    View author publications

    You can also search for this author in PubMed Google Scholar

  3. Yuhua Xiao
    View author publications

    You can also search for this author in PubMed Google Scholar

  4. Wenqiang Dang
    View author publications

    You can also search for this author in PubMed Google Scholar

  5. Jie Feng
    View author publications

    You can also search for this author in PubMed Google Scholar

Corresponding author

Correspondence to Shifa Wang.

Additional information

The article is published in the original.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Wang, S., Li, D., Xiao, Y. et al. Synthesis of SrFe12O19 magnetic nanoparticles by EDTA complex method. Russ. J. Phys. Chem. 91, 1981–1986 (2017). https://doi.org/10.1134/S003602441710034X

Download citation

  • Received:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1134/S003602441710034X

Keywords

Search

Navigation