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O-benzyl-N-(2-furoyl)thiocarbamate

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Abstract

The O-benzyl-N-(2-furoyl)thiocarbamate (1) was obtained by direct reaction between furoyl isothiocyanate and benzyl alcohol. The X-ray diffraction analysis of 1 showed an orthorhombic system, with a = 7.811(4) Å, b = 9.685(4) Å, c = 33.562(15) Å, and space group P212121. This compound showed two different arrays of structure, corresponding to two conformers in the same crystal unit. In one conformer the carbonyl and thiocarbonyl groups are in a syn arrangement while in the other the groups are anti. Both structures present a non-restricted conformation and show NH—OC hydrogen bonding between them.

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reference

  1. Quas, L.; Schroder, V.; Beyer, L. Solvent Extr. Ion Exch. 2000, 18, 1167.

    Google Scholar 

  2. Quas, L.; Ristau, T.; Schroder, V.; Dietze, F.; Beyer, L. Z. Anorg. Allg. Chem. 2001, 627, 1909.

    Google Scholar 

  3. Otazo-Sánchez, E.; Pérez-Marin, L.; Estevez-Hernandez, O.; Rojas-Lima, S.; Alonso-Chamarro, J. J. Chem. Soc. Perkin Trans. 2001, 2, 2211.

    Google Scholar 

  4. SHELXTL-NT Version 5.1; Bruker Analytical X-Ray Systems: Madison, USA, 1998.

  5. Spek, A.L. Acta Cryst. Sect. C. 1990, A46, 34.

    Google Scholar 

  6. SAINT+NT Version 6.01; Bruker Analytical X-ray Systems: Madison, USA, 1999.

  7. Farrugia, L.J. J. Appl. Cryst. 1997, 30, 565.

    Google Scholar 

  8. Bondi, A. J. Phys. Chem. 1964, 68, 441.

    Google Scholar 

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Authors and Affiliations

  1. Centro de Investigaciones Químicas (CIQ), Universidad Autónoma del Estado de Hidalgo, Carretera Pachuca-Tulancingo km 4.5, Ciudad Universitaria, 42074, Pachuca, México

    Luis Alberto Montiel-Ortega, Susana Rojas-Lima & Roberto Villagómez-Ibarra

  2. Instituto Tecnológico de Toluca (ITT), Av. Instituto Tecnologico s/n Metepec, 52140, Toluca, México

    Elena Otazo-Sanchez

Authors
  1. Luis Alberto Montiel-Ortega
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  2. Susana Rojas-Lima
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  3. Elena Otazo-Sanchez
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  4. Roberto Villagómez-Ibarra
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Correspondence to Luis Alberto Montiel-Ortega.

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Montiel-Ortega, L.A., Rojas-Lima, S., Otazo-Sanchez, E. et al. O-benzyl-N-(2-furoyl)thiocarbamate. Journal of Chemical Crystallography 34, 89–93 (2004). https://doi.org/10.1023/B:JOCC.0000014694.33182.ff

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  • DOI: https://doi.org/10.1023/B:JOCC.0000014694.33182.ff

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