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Synthesis and Crystal Structure of 3-Carbamoyl-6-methyl-5-phenylcarbamoyl-2-thioxo-1,2,3,4-tetrahydropyridine-4-spirocyclohexane

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

3-Carbamoyl-6-methyl-5-phenylcarbamoyl-2-thioxo-1,2,3,4-tetrahydropyridine-4-spirocyclohexane has been synthesized by the condensation of cyclohexylidenecyanothioacetamide with acetoacetanilide and piperidine. The structure of the product was established by X-ray structural analysis.

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REFERENCES

  1. V. P. Litvinov, S. G. Krivokolysko, and V. D. Dyachenko, Khim. Geterotsikl. Soedin., 579 (1999).

  2. L. A. Rodinovskaya, Dissertation for Doctor of Chemical Sciences, Moscow (1994).

  3. V. D. Dyachenko, Dissertation for Doctor of Chemical Sciences, Moscow (1998).

  4. A. A. Krauze, A. Rumler, F. Khagen, Kh.-I. Ensh', I. G. Shturm, and G. Ya. Dubur, Khim. Geterotsikl. Soedin., 75 (1992).

  5. L. A. Rodinovskaya, A. M. Shestopalov, and V. N. Nesterov, Khim. Geterotsikl. Soedin., 1376 (1996).

  6. A. Krauze, J. Popelis, and G. Dubur, Heterocycl. Commun., 3, 515 (1997).

    Google Scholar 

  7. A. Alberola, L. A. Calvo, A. G. Ortega, M. C. S. Ruiz, P. Yustos, S. G. Granda, and E. Garcia-Rodriguez, J. Org. Chem., 64, 9493 (1999).

    Google Scholar 

  8. A. A. Krauze, E. E. Liepin'sh, Z. A. Kalme, Yu. E. Pelcher, and G. Ya. Dubur, Khim. Geterotsikl. Soedin., 1504 (1984).

  9. V. D. Dyachenko, S. G. Krivokolysko, and V. P. Litvinov, Khim. Geterotsikl. Soedin., 1533 (1997).

  10. N. S. Zefirov and V. A. Palyulin, Dokl. Akad. Nauk SSSR, 252, 111 (1980).

    Google Scholar 

  11. A. Bond, J. Phys. Chem., 68, 3, 441 (1964).

    Google Scholar 

  12. R. W. Alder, N. C. Goode, T. J. King, J. M. Mellor, and B. W. Miller, J. Chem. Soc., Chem. Commun., No. 5, 173 (1976).

  13. M. Burke-Laing and M. Laing, Acta Crystallogr., B32, 3216 (1976).

    Google Scholar 

  14. T. Offersen, Acta Chem. Scand., Ser. A, 29, 939 (1975).

    Google Scholar 

  15. L. N. Kuleshova and P. M. Zorkii, Acta Crystallogr., B37, 1363 (1981).

    Google Scholar 

  16. F. H. Allen, G. M. Bird, R. S. Rowland, and P. R. Raithby, Acta Crystallogr., B53, 680 (1997).

    Google Scholar 

  17. G. M. Sheldrick, SHELXS-86. Program for the Solution of Crystal Structures, University of Göttingen, Göttingen, Germany (1986).

    Google Scholar 

  18. G. M. Sheldrick, SHELXL-93. Program for the Refinement of Crystal Structures, University of Göttingen, Göttingen, Germany (1993).

    Google Scholar 

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Authors and Affiliations

  1. T. Shevchenko State Pedagogical University, Lugansk, 91011, Ukraine

    A. D. Dyachenko & V. D. Dyachenko

  2. V. N. Karazin Kharkiv National University, Kharkiv, 61077, Ukraine

    S. M. Desenko

  3. National Academy of Sciences of the Ukraine, Institute of Organic Chemistry, Kiev, 02094, Ukraine

    E. B. Rusanov

Authors
  1. A. D. Dyachenko
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  2. S. M. Desenko
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  3. V. D. Dyachenko
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  4. E. B. Rusanov
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Dyachenko, A.D., Desenko, S.M., Dyachenko, V.D. et al. Synthesis and Crystal Structure of 3-Carbamoyl-6-methyl-5-phenylcarbamoyl-2-thioxo-1,2,3,4-tetrahydropyridine-4-spirocyclohexane. Chemistry of Heterocyclic Compounds 39, 744–748 (2003). https://doi.org/10.1023/A:1025690927825

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  • DOI: https://doi.org/10.1023/A:1025690927825

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