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Heat treatment temperature effects on structural and electrochemical properties of PVDC-based disordered carbons

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Abstract

X-ray diffraction (XRD), BET surface area, Raman spectroscopy and electrochemical measurement were used to investigate the morphological behaviors of poly(vinylidene chloride) (PVDC)-based carbons in the heat treatment temperature range 700 to 3000°C. X-ray diffraction and Raman scattering results proposed that PVDC-based carbons heat treated up to 3000°C behaved as typically non-graphitizable carbons. The structural parameters were correlated with discharge/charge characteristics of Li ions into PVDC-based carbons. It was realized that the Li ion storage capacity of PVDC-based carbons during the first cycle tended to decrease with increasing the heat-treatment temperature due to the reduction of hydrogen content and the reduction of the specific surface area from pores.

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Authors and Affiliations

  1. Faculty of Applied Chemical Engineering, Chonnam National University, 300 youngbong-dong, Buk-gu, Gwangju, 500-757, South Korea

    Chan Kim & Kap Seung Yang

  2. Faculty of Engineering, Shinshu University, 500 Wakasato, Nagano, 380-0922, Japan

    Y. J. Kim & M. Endo

Authors
  1. Chan Kim
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  2. Kap Seung Yang
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  3. Y. J. Kim
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  4. M. Endo
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Correspondence to Kap Seung Yang.

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Kim, C., Yang, K.S., Kim, Y.J. et al. Heat treatment temperature effects on structural and electrochemical properties of PVDC-based disordered carbons. Journal of Materials Science 38, 2987–2991 (2003). https://doi.org/10.1023/A:1024429828872

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