Abstract
The synthesis and X-ray crystal structure of 1,2;5,6-di-O-isopropylidene-3-O-(phenylacetyl)-D-glucofuranose is reported. It crystallizes in the orthorhombic system with space group P212121 (No. 19); a = 9.9313(12) Å, b = 10.0657(12) Å, c = 20.343(2) Å, and Z = 4. The solid state structure is discussed in terms of the use of the title compound for further chemistry.
Similar content being viewed by others
References
Horton, D.; Roski, J.P.; Norris, P. J. Org. Chem. 1996, 61, 3783.
Berndt, D.F.; Norris, P. Tetrahedron Lett. 2002, 43, 3961.
SMART, Software for the CCD Detector System, version 5.625; Bruker Analytical X-Ray Instruments, Inc.: Madison, WI, 2001.
SAINT-Plus, Data Processing Software for the CCD Detector System, version 6.22; Bruker Analytical X-Ray Instruments, Inc.: Madison, WI, 2001.
Sheldrick, G.M. SADABS, Software for Area Detector Absorptions and Other Corrections, version 2.03; University of Göttingen: Germany, 2001.
Sheldrick, G.M. SHELXTL NT, Software Package for the Refinement of Crystal Structures, version 6.10; University of Göttingen: Germany, 2000.
Author information
Authors and Affiliations
Corresponding author
Rights and permissions
About this article
Cite this article
Sheville, J., Berndt, D., Wagner, T. et al. Crystal structure of 1,2;5,6-di-O-isopropylidene-3-O-(phenylacetyl)-D-glucofuranose. Journal of Chemical Crystallography 33, 409–412 (2003). https://doi.org/10.1023/A:1024234231567
Issue Date:
DOI: https://doi.org/10.1023/A:1024234231567