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Phosphate Derivatives of Natural Lactones. II. Synthesis of Novel Dialkylphosphonates of Arteannuin B

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Abstract

Novel dialkylphosphonates of arteannuin B were synthesized in 45-47% yields by reaction of this cadinanolide with dialkylphosphites. Their structures were established using IR, PMR, 13C and 31P NMR spectroscopy, and two-dimensional 1H-1H NMR (COSY) spectroscopy. The reaction of arteannuin B and dialkylphosphites is highly stereoselective.

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Authors and Affiliations

  1. Institute of Phytochemistry, Ministry of Education and Science, Republic of Kazakhstan, Karaganda, ul. M. Gazalieva 4

    R. I. Dzhalmakhanbetova, E. M. Suleimenov, B. B. Rakhimova, N. A. Talzhanov, A. T. Kulyyasov & S. M. Adekenov

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  1. R. I. Dzhalmakhanbetova
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  2. E. M. Suleimenov
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  3. B. B. Rakhimova
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  4. N. A. Talzhanov
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  5. A. T. Kulyyasov
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  6. S. M. Adekenov
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Dzhalmakhanbetova, R.I., Suleimenov, E.M., Rakhimova, B.B. et al. Phosphate Derivatives of Natural Lactones. II. Synthesis of Novel Dialkylphosphonates of Arteannuin B. Chemistry of Natural Compounds 38, 553–556 (2002). https://doi.org/10.1023/A:1022630603323

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  • DOI: https://doi.org/10.1023/A:1022630603323

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