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Crystal structure of a new double salt hydrate SrCd2Cl6⋅8H2O

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Abstract

SrCd2Cl6⋅8H2O crystallizes in the space group \(P\bar 1\) and has the unit cell dimensions a = 9.688(2) Å, b = 11.212(2) Å, c = 7.732(3) Å, α = 99.85(21)°, β = 89.95(22)°, γ = 75.81(13)°, and Z = 2. After refinement through full-matrix least-squares methods, the reliability factor R in the final cycle is 4.65%. A very persistent occurrence of twinning by pseudosymmetry was observed. The twin element is a twofold axis [001]. The title compound exhibits five endothermic peaks, which have been detected by differential scanning calorimetry and interpreted from thermogravimetry.

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Authors and Affiliations

  1. Faculté des sciences de Sfax, Laboratoire de L'Etat solide, BP 802, 3018 Sfax, Tunisia

    S. Yahyaoui, R. Ben Hassen & A. Ben Salah

Authors
  1. S. Yahyaoui
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  2. R. Ben Hassen
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  3. A. Ben Salah
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Correspondence to R. Ben Hassen.

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Yahyaoui, S., Hassen, R.B. & Salah, A.B. Crystal structure of a new double salt hydrate SrCd2Cl6⋅8H2O. Journal of Chemical Crystallography 32, 243–250 (2002). https://doi.org/10.1023/A:1020249006294

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  • DOI: https://doi.org/10.1023/A:1020249006294

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