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Crystal Structure of Ammonium Undecafluorotriantimonate(III) (NH4)2Sb3F11

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Abstract

The crystal structure of a novel antimony(III) fluoride complex, ammonium undecafluorotriantimonate(III) (NH4)2Sb3F11, was determined. The crystals are triclinic: a = 7.780(2) Å, b = 8.370(2) Å, c = 10.620(1) Å, α = 71.06(1)°, β = 89.03(1)°, γ = 63.58(1)°, V = 579.1(2) Å3, Z = 2, ρ(calcd) = 3.500 g/cm3, ρ(exp) = 3.51 g/cm3, F(000) = 548.0, space group P \(\overline 1\). The structure consists of anionic [Sb3F11]2– chains and ammonium cations combined into a framework by the N–H···F hydrogen bonds.

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Authors and Affiliations

  1. Russian Academy of Sciences, Institute of Chemistry, Far East Division, pr. Stoletiya Vladivostoka 159, Vladivostok, 690022, Russia

    A. A. Udovenko, L. A. Zemnukhova & R. L. Davidovich

  2. Russian Academy of Sciences, Kurnakov Institute of General and Inorganic Chemistry, Leninski pr. 31, Moscow, 117907

    Yu. E. Gorbunova & Yu. N. Mikhailov

Authors
  1. A. A. Udovenko
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  2. L. A. Zemnukhova
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  3. Yu. E. Gorbunova
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  4. Yu. N. Mikhailov
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  5. R. L. Davidovich
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Udovenko, A.A., Zemnukhova, L.A., Gorbunova, Y.E. et al. Crystal Structure of Ammonium Undecafluorotriantimonate(III) (NH4)2Sb3F11. Russian Journal of Coordination Chemistry 28, 12–14 (2002). https://doi.org/10.1023/A:1013703518486

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  • DOI: https://doi.org/10.1023/A:1013703518486

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