Abstract
2-Ethyl-2-methyl-5-methylene-1,3-dioxolan-4-one and 5-methylene-2,2-pentamethylene-1,3-dioxolan-4-one were synthesized by reaction of β-chlorolactic acid with methyl ethyl ketone and cyclohexanone, respectively, followed by dehydrochlorination of intermediate 5-chloromethyl derivatives.
This is a preview of subscription content, log in via an institution to check access.
Similar content being viewed by others
REFERENCES
Shilyaeva, N.P., Annenkova, V.M., Malysheva, S.F., Kozyreva, O.B., and Annenkova, V.Z., Vysokomol. Soedin., Ser. A, B, 1996, no. 10, pp. 1773-1775.
Heterocyclic Compounds, Elderfield, R.C., Ed., New York: Wiley, 1957, vol. 5; Balashov, A.L., Danov, S.M., and Chernov, A.A., Abstracts of Papers, Mezhdunarodnaya konferentsiya po naukoemkim khimicheskim tekhnologiyam (Int. Conf. on High Chemical Technology), Yaroslavl, 1998, pp. 110-111; Lugovkin, S.N., Shevchuk, A.S., Ustavshchikov, B.F., Podgornova, V.A., and Popova, V.V., Abstracts of Papers, Mezhdunarodnaya konferentsiya po naukoemkim khimicheskim tekhnologiyam (Int. Conf. on High Chemical Technology), Yaroslavl, 1998, pp. 151-152.
Carey, F.A. and Sundberg, R.J., Advanced Organic Chemistry, New York: Plenum, 1977.
Ogorodnikov, S.K., Lesteva, T.M., and Kogan, V.V., Azeotropnye smesi (Azeotropic Mixtures), Leningrad: Khimiya, 1971.
Roberts, J.D. and Caserio, M., Basic Principles of Organic Chemistry, New York: W.A. Benjamin, 1975, 2nd ed.
Khramushina, M.I., Cand. Sci. (Chem.) Dissertation, Dzerzhinsk, 1983.
Author information
Authors and Affiliations
Rights and permissions
About this article
Cite this article
Shevchuk, A.S., Podgornova, V.A. & Ustavshchikov, B.F. Synthesis of 1,3-Dioxolane Derivatives from β-Chlorolactic Acid and Ketones. Russian Journal of Organic Chemistry 37, 704–706 (2001). https://doi.org/10.1023/A:1012408119584
Issue Date:
DOI: https://doi.org/10.1023/A:1012408119584