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Synthesis of Aminomethylphosphines with Triazaadamantane Fragments

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Abstract

The reaction of (hydroxymethyl)diphenylphosphine with 7-amino-1,3,5-triazaadamantane, followed by ready oxidation of the initially formed aminomethylphosphine gave diphenyl[(1,3,5-triazaadamantan-7-yl)aminomethyl]phosphine oxide. The reactions of bis(hydroxymethyl)phenylphosphine with 2 mol of 7-amino-1,3,5-triazaadamantane in the absence and in the presence of Paraform provided bis[(1,3,5-triazaadamantan-7-yl)aminomethyl]phenylphosphine and 1,3-bis(1,3,5-triazaadamantan-7-yl)-5-phenyl-1,3,5-diazaphosphorinane, respectively.

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Authors and Affiliations

  1. Arbuzov Institute of Organic and Physical Chemistry, Kazan Research Center, Russian Academy of Sciences, Kazan, Tatarstan, Russia

    R. M. Kuznetsov, A. S. Balueva, T. M. Serova & G. N. Nikonov

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  1. R. M. Kuznetsov
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  2. A. S. Balueva
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  3. T. M. Serova
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  4. G. N. Nikonov
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Kuznetsov, R.M., Balueva, A.S., Serova, T.M. et al. Synthesis of Aminomethylphosphines with Triazaadamantane Fragments. Russian Journal of General Chemistry 71, 899–902 (2001). https://doi.org/10.1023/A:1012327301121

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  • DOI: https://doi.org/10.1023/A:1012327301121

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