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New Method of Synthesis of 5-Acetyl-3-cyano-6-methylpyridine-2(1H)-Thione and Its Properties

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Chemistry of Heterocyclic Compounds Aims and scope

Abstract

5-Acetyl-3-cyano-6-methylpyridine-2(1H)-thione was obtained by the reaction of ethoxymethyleneacetylacetone with cyanothioacetamide in the presence of N-methylmorpholine. Its alkylation, bromination of the 2-methylthio derivative, and the conversions of its 5-bromoacetyl derivative have been studied.

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Authors and Affiliations

  1. Lugansk Taras Shevchenko State Pedagogical University, Lugansk, 91011, Ukraine

    Ya. Yu. Yakunin & V. D. Dyachenko

  2. N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, Moscow, 117913

    V. P. Litvinov

Authors
  1. Ya. Yu. Yakunin
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  2. V. D. Dyachenko
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  3. V. P. Litvinov
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Yakunin, Y.Y., Dyachenko, V.D. & Litvinov, V.P. New Method of Synthesis of 5-Acetyl-3-cyano-6-methylpyridine-2(1H)-Thione and Its Properties. Chemistry of Heterocyclic Compounds 37, 581–587 (2001). https://doi.org/10.1023/A:1011656605605

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  • DOI: https://doi.org/10.1023/A:1011656605605

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