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Crystal structure of a novel bis(guanidiniums) compound incorporated by sulfate anion

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Abstract

Crystal structure of a novel bis(guanidiniums) compound 1 by sulfate anion and water, C11H20N6OċSO4ċH2O, was measured by X-ray crystallographic analysis with an “imaging plate” method. It possesses space group P21/c, with a = 7.6433(15), b = 19.447(4), c = 12.115(2) Å, β = 107.81(3)°, and φcalc = 1.420 mg/m3 for Z = 4. Crystal data indicate that the architecture network is formed through hydrogen bonds, electrostatic interactions, and arene–arene stacking interaction among the bis(guanidiniums) compound, the sulfate anion and water molecule.

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References

  1. Heys, L.; Moore, C.G.; Murphy, P. J. Chem. Soc. Rev. 2000, 29, 57.

    Google Scholar 

  2. Schmidtchen, F.P.; Berger, M. Chem. Rev. 1997, 97, 1609.

    Google Scholar 

  3. Ohtani, I.; Kusumi, T.; Kakisawa, H.; Kashman, Y.; Hirsh, S. J. Am. Chem. Soc. 1992, 114, 8472.

    Google Scholar 

  4. Rama Rao, A.V.; Gurjar, M.K.; Islam, A. Tetrahedron Lett. 1993, 34, 4993.

    Google Scholar 

  5. Murphy, P.J.; Williams, H.L.; Hibbs, D.E.; Hursthouse, M.B.; Malik, K.M.A. Tetrahedron 1996, 52, 8315.

    Google Scholar 

  6. Kinnel, R.B.; Gehrken, H.P.; Swali, R.; Skoropowski, G.; Scheuer, P.J. J. Org. Chem. 1998, 63, 3281.

    Google Scholar 

  7. Russel, V.A.; Etter, M.C.; Ward, M.D. J. Am. Chem. Soc. 1994, 116, 1941.

    Google Scholar 

  8. Evans, C.C.; Sukarto, L.; Ward, M.D. J. Am. Chem. Soc. 1999, 121, 320.

    Google Scholar 

  9. Dietrich, B.; Fyles, D.L.; Fyles, T.M.; Lehn, J.-M. Helv. Chim. Acta. 1979, 62, 2763.

    Google Scholar 

  10. Bell, M.; Edwards, A.J.; Hoskins, B.F.; Kachab, E.H. Robson, R. J. Am. Chem. Soc. 1989, 111, 3603.

    Google Scholar 

  11. Altomare, A.; Burla, M.C.; Camalli, M.; Cascarano, M.; Giacovazzo, C.; Guagliardi, A.; Polidori, G. J. Appl. Crystallogic. 1994, 27, 435.

    Google Scholar 

  12. SHELXTL (version 5.0), Reference Manual; Siemens Industrial Automation, Madison WI, 1995.

  13. TEXSAN, Crystal Structure Analysis Package, Molecular Structure Corporation, 1985, 1992.

  14. Gobbi, A.; Frenking, G. J. Am. Chem. Soc. 1993, 115, 2362.

    Google Scholar 

  15. (a) Hunter, C.A. Chem. Soc. Rev. 1994, 101; (b) Hunter, C.A. Angew. Chem. Int. Ed. Engl. 1993, 32, 1584 and references cited there in.

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Authors
  1. Guo-Yuan Lu
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  2. Wei Song
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  3. Feng Tang
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  4. Xiao-Bin Wan
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  5. Fang Liu
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  6. Chuan-Min Jin
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Lu, GY., Song, W., Tang, F. et al. Crystal structure of a novel bis(guanidiniums) compound incorporated by sulfate anion. Journal of Chemical Crystallography 30, 483–487 (2000). https://doi.org/10.1023/A:1011359702042

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