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Low Temperature Specific Heat and Thermal Stability of Fe–B Ultrafine Amorphous Alloy Particles

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Abstract

Fe–B ultrafine amorphous alloy particles (UFAAP) were prepared by chemical reduction of Fe3+ with NaBHO4 and confirmed to be ultrafine amorphous particles by transmission electron microscopy and X-ray diffraction. The specific heat of the sample was measured by a high precision adiabatic calorimeter, and a differential scanning calorimeter was used for thermal stability analysis. A topological structure of Fe-B atoms is proposed to explain two crystallization peaks and a melting peak observed at T=600, 868 and 1645 K, respectively.

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Authors and Affiliations

  1. Thermochemistry Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian, 116023, China

    L. Wang, Z. C. Tan & S. H. Meng

  2. Environmental Engineering Laboratory, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian, 116023, China

    D. B. Liang

  3. Institute of Material and Technology, Dalian Maritime University, Dalian, 116026, China

    S. J. Ji & Z. K. Hei

Authors
  1. L. Wang
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  2. Z. C. Tan
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  3. S. H. Meng
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  4. D. B. Liang
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  5. S. J. Ji
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  6. Z. K. Hei
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Wang, L., Tan, Z.C., Meng, S.H. et al. Low Temperature Specific Heat and Thermal Stability of Fe–B Ultrafine Amorphous Alloy Particles. Journal of Thermal Analysis and Calorimetry 66, 409–414 (2001). https://doi.org/10.1023/A:1013130515314

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  • DOI: https://doi.org/10.1023/A:1013130515314

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