Abstract
This research work presents the investigation of H13 tool steel powder in the production of parts characterized by complex features via selective laser melting. The authors proposed a benchmark geometry with 40 mm nominal height, self-supported overhanging structure and internal channels. To investigate powder printability and process capabilities, an experimental campaign was designed as a function of laser power, scan speed and hatching distance. Full dense parts exhibiting 99.92% internal density have been achieved by imposing a laser power equal to 150 W, a scan speed equal to 500 mm/s and a hatching distance equal to 120 µm, while high geometrical accuracy in terms of no material drops along sample edges and low-dimensional deviations of the realized sloping surfaces (i.e., + 0.23° and − 0.90° for nominal 35° and 40° overhang, respectively) has been achieved for 150 W, 1000 mm/s, and 100 µm. Findings open the way to use SLM technology in the design of advanced cutting tool solutions.
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1 Introduction
The technological need for designing advanced cutting tool solutions exhibiting longer working life in conjunction with improved wear resistance and high-precision material removal is driving the industry to explore new cost-effective manufacturing solutions enabling the production of highly complex cutting tools exhibiting enhanced performance. Selective laser melting (SLM) is a powder bed fusion (PBF) technique capable to fabricate high-density metal parts with high-complex geometrical designs impossible to reach by means of conventional technologies [1,2,3,4]. Recently, industrial and academic efforts have focused on characterizing the processability of H13 steel powder through SLM for the design and manufacturing of complex-shaped cutting tool solutions [5,6,7,8,9].
Several research works have analyzed the influence of SLM process parameters [10,11,12,13], raster patterns [14], preheating [15] and post-tempering treatments [16] on the final density, residual stress, and microstructure of SLM-fabricated high-carbon steel components. Laakso et al. [10] assessed the influence of the laser power (100–300 W), scan speed (400–1200 mm/s), and hatching distance (90–150 µm) on the final structural quality of H13 components, achieving notable results in terms of part porosity (up to 99%) for a power of 200 W, a scan speed of 1200 mm/s and a hatching distance lower than 120 µm. A similar analysis was designed by Fonseca et al. [11] where a parameter set for minimal linear crack density, minimal porosity and maximum density was found setting a laser power of 172 W, a scan speed of 700 mm/s and hatching distance equal to 80 µm. Acceptable mechanical properties were achieved by Katancik et al. [12] by means of SLM process optimization, observing a final density, microstructure, and microhardness of the as-fabricated H13 comparable to those of formed H13 tool steel parts. Yan et al. [13] focused their analysis on the residual stress of manufactured samples produced with a laser power of 150 W, a scan speed of 300 mm/s and a hatch spacing of 50 μm, finding values in a range between 940 and 1420 MPa. The authors concluded that the main reason for the high detected compressive residual stresses was the martensitic transformation that occurred during the SLM of the H13 steel. To reduce part porosity, Kurzynowski et al. [14] tested different scan strategies demonstrating that a proper selection of the chessboard strategy with small dimensions of individual fields prevented the influence of the size of the scan section on the relative density of the manufactured parts. A structured experimental campaign for the SLM of H13 employing 200 °C substrate preheating was performed by Narvan et al. [15], demonstrating that application of the preheating process not only enhances the relative density (99.7%) but also helps in eliminating the thermally induced cracks. Building upon these studies, the common processing defects in SLM have been classified by considering all contributing factors, for process monitoring and control purpose [17]. In addition, numerical models have been developed to enhance understanding of the multi-physics involved in the process [18].
Despite the remarkable results obtained from the above studies, the performed analyses mainly focus on the final quality of H13 simple-shaped geometries (e.g., cubes) without considering the influence of the main SLM process parameters on both the structural integrity and geometrical accuracy of geometrically complex H13 parts. Specifically, for highly complex geometrical designs where support structures cannot be placed due to accessibility constraints imposed by part’s functionalities (e.g., conformal channels), the SLM process has to be optimized to ensure a defect-free and geometrically sound realization of the self-support features. Such process optimization often requires the implementation of different combinations of process parameters for the manufacturing of a single component, depending on the design complexity and geometrical features to be realized. In addition, all the cited studies report the manufacturing of samples with maximum heights of about 10 mm, neglecting the influence of the build height on the final quality of the as-built components (i.e., the effect of the increasing distance from the heated plate, discussed in [19, 20] for different materials). To the best of the authors’ knowledge, few efforts have been currently performed to address the fabrication of complex H13 shapes taking into account process, material, and design constraints [21,22,23,24,25,26,27,28], missing in design rules driving the SLM process optimization of functionally shaped cutting tools for relevant industrial applications.
This research work focuses on the influence of the main SLM process parameters (i.e., laser power, scan speed, and hatching distance) on both the achievable geometrical accuracy and final structural quality of as-built geometrically complex H13 specimens. The 3D bulk geometries were designed to exhibit self-supporting features based on the design of a milling sleeve previously optimized for AM [23]. The main experimental results showed that the manufacturing of high-quality H13 parts needs an adaptation of the SLM process parameters based on the geometrical complexity of the part design. The achieved experimental outcomes encourage the employment of combinations of SLM process parameters involving low laser power (i.e., 150 W) and medium–low volumetric energy densities (i.e., 80 J/mm3). Section 2 introduces the experimental equipment employed for sample manufacturing and the followed experimental methodology. Sections 3 and 4 deal with the achieved results and discussion, respectively. Finally, the main conclusions are discussed in Sect. 5.
2 Materials and methods
2.1 Materials and bulk geometry design
The metal powder used for sample manufacturing was AISI H13 powder (provider: Kind Special Alloy, Collegno, Italy). The particle size distribution was evaluated according to ASTM B822-20 standard [29] while the chemical composition was estimated through combustion analytical technique and inductively plasma optical emission according to ASTM E1019-18 and ASTM E1479-16 standard [30, 31]. Tables 1 and 2 report particle size distribution and chemical composition of the involved metal powder.
The bulk sample geometry was engineered considering the maximum height and the geometrical complexity of the milling tool presented by the authors in [23] (see Fig. 1). Specifically, the sample design was divided in four zones with the goal to analyze the influence of geometrical complexity on the structural integrity of the part (see Fig. 1a). Zone 1 aimed to analyze the effect of process parameters on the structural quality of the realized sample avoiding any issue related to part geometry; zone 2 meant to study the effect of an increasing distance from the heated plate in conjunction with a reduced layer size; in zones 3 and 4, the capability of the SLM process to generate self-supporting H13 structures was tested. Zone 3 was characterized by the presence of two overhanging surfaces with different slopes (35° and 40°—see Fig. 1b), whereas in zone 4, two different internal channels with different sizes and cross-sections were placed (i.e., an isosceles triangle cross-section and a rectangular triangle cross-section—see Fig. 1c).
2.2 SLM machine and experimental campaign design
The SLM system used for sample manufacturing was a Printsharp 250 (supplier: Prima Additive, Turin, Italy). The machine was equipped with an Yb laser with an emission wavelength ranging between 1060 and 1080 nm and a maximum power of 500 W on a focused 70 µm beam diameter. The SLM process was performed in an Argon inert building environment, ensuring an O2 level of less than 500 ppm for all the AM process duration. To evacuate the smoke generated during the process and shield the f-Θ lens and laser optics, a 20 l/min Argon gas flow homogeneously distributed above the powder bed was used during sample manufacturing. The gas flow moved following the path indicated by the green arrows in Fig. 2a and was previously optimized to maximize smoke evacuation without blowing away the deposited powder bed.
To characterize the effect of the SLM process parameters on the final quality of H13 samples, an experimental campaign consisting of 3 input variables (i.e., P, v, h) and 3 levels each was designed, considering a volumetric energy density (VED) ranging between 42 to 250 J/mm3 (see Table 3). VED is defined as
where P is the laser power (W), v is the scan speed (mm/s), h is the hatching distance (µm) and t is the layer thickness (µm). To explore the variable space correlated to the chosen energy range, P was set at 150, 225, and 350 W, v was set at 500, 750, and 1000 mm/s, and h was set at 80, 100, and 200 µm. Three repetitions for each combination of process parameters were executed, whereas t was kept constant at 30 µm. Table 3 summarizes the process variables and the VED calculated for each experimental combination. Another pivotal parameter involved in the SLM process is the surface specific energy (Es—J/mm2) irradiated by the laser on the powder bed, defined as
where d is the diameter of the focalized laser beam (mm). This parameter was also taken into account during the results’ discussion since it significantly affected the processability of the H13 powder.
For each build job, 5 different combinations of process parameters and 3 repetitions each (see Fig. 2b) were realized for a total of 15 3D bulk geometries for each plate. Samples’ positioning was designed to ensure a minimum 30 mm distance between each realized geometry. Sample manufacturing was performed using 200 °C substrate preheating. Each layer was filled using a 5 mm width stripe building strategy (see Fig. 2c, d, e), changing the raster angle layer by layer according to the following sequence: 10°, 135°, 200°, 306°, 45°, 170°, 215°, and 345°. The building strategy and the raster angles were selected considering anisotropic studies founded in SLM literature, aiming to reduce the residual stresses inside the manufactured samples [32, 33].
Six AISI 316L plates for a total of 81 samples were used to complete the experimental campaign (5 full and 1 half-full plates, see Fig. 3). No support structures were designed for the manufacturing of the bulk geometries to characterize the influence of the evaluated process parameters on the final quality of self-supporting geometrical features.
2.3 Methods analysis
The overall sample quality was assessed following two screening criteria to both evaluate the influence of the process parameters on the final quality of the realized specimens and assess the capabilities of the SLM system in printing geometrically complex AISI H13 features.
First screening step: the process status was monitored by visual observations to identify detrimental defects formed during part fabrication, such as protrusions (i.e., metallic material accumulated on the layer borders, exceeding the height of the powder bed and inducing an uneven layer growth—see Fig. 4a), which compromised the building process by colliding the polymeric wiper of the recoater during the spreading of fresh powder. Indeed, repeated impacts between metallic protrusions and the recoater cause local notching of the polymeric wiper (see Fig. 4b), leading to an uneven powder bed formation when a new layer is being formed and affecting the fabrication of the other specimens located on the building area (see Fig. 4c). Once a collision was visually detected by the machine operator (no online monitoring systems were used in this research work), the fabrication of the pertaining faulty parts was aborted.
Second screening step: the samples that successfully finished printing were detached 5 mm from the baseplate through a double vertical column band saw and an optical characterization of the samples’ cross-sections was performed to assess the final achieved geometrical accuracy and internal structural integrity. Cross-section preparation was performed on the sample surface marked by the yellow arrow in Fig. 1a by a face milling operation followed by polishing to remove the typical staircase morphology of the SLM process. Image acquisition was performed through a RH 2000 digital microscope (Hirox, Tokyo, Japan) and the auto-count function tool integrated in the microscope software was used for porosity analysis, setting an investigation area of 8.5 × 3.5 mm. Internal cracks assessment and overhang measurements in terms of achieved sloping angle were performed by means of the open-source ImageJ software (U. S. National Institutes of Health, Maryland, USA). Each sample was coded as laser power_scan speed_hatching distance (i.e., Test 500_225_80 refers to the bulk geometry obtained imposing 500 W laser power, 225 mm/s scan speed, and 80 µm hatching distance). Cross-section analysis was performed according to the zones defined in Fig. 1a. The authors first investigated the zone 4 to assess the capability of the SLM process in realizing internal cavity and unsupported geometries, comparing the obtained features with the nominal ones (see Fig. 5a, b), then they focused on zone 3 to characterize the quality of overhanging structures (see Fig. 5c), measuring the achieved sloping angle. Finally, the analysis of the internal quality of zones 1 and 2 in terms of pores (see Fig. 6), lack of fusion, cracks, and delamination was performed.
3 Results
The results are reported according to the screening criteria introduced in the materials and methods section. During the first screening step (i.e., the visual observation of the process status), the printing of all the samples involving 300 W laser power and of six specimens fabricated at 225 W was stopped due to the formation of strong protrusions along the sample contours (see Table 4). In addition, the process combination involving P = 150 W, v = 500 mm/s, and h = 80 µm failed, exhibiting building defects in the infill area of the realized layers of zone 1 of the designed sample geometry (see Fig. 1a). Figure 7a shows the observed defects occurring during the manufacturing of test 150_500_80, while protrusions occurring for 300 W are shown in Fig. 7b. Table 4 shows the samples successfully printed and the ones interrupted. At the end of the experimental campaign, 33 out of 81 H13 samples were entirely produced without any evidence of protrusions (see Fig. 7c).
The second screening step was focused on the inspection of the internal quality of the successfully realized parts starting from zone 4 to zone 1. The performed analysis highlighted the presence of three categories of defects:
-
(1)
high porosity in the core of zone 3 and 4 (see Fig. 8a);
-
(2)
contour defect in overhanging structure of zone 3 and in internal channel of zone 4 (see Fig. 8b);
-
(3)
material drops or jagged profiles at the vertical fillet radii (see Fig. 8c).
-
(1)
Zones 1 and 2 exhibited a lower porosity (i.e., 0.11% and 0.09% on average, respectively) compared to zones 3 and 4 (i.e., 0.15% and 0.51% on average, respectively). Pores sizes vary in a range of 60–130 µm in zone 3 and 4 and between 45 and 70 µm in zone 1 and 2 in accordance with research findings discussed in the literature [34,35,36]. The lower porosity was obtained for tests 150_500_120, 150_1000_80, and 150_1000_100, showing an average internal density ranging between 99.91% and 99.93%. Table 5 and Fig. 9 summarizes the detected internal porosity for each analyzed sample zone.
-
(2)
The measured overhang angles varied between + 4.91° and − 0.78°, and between + 3.62° and -1.76° compared to the nominal sloping angle of 35° and 40°, respectively. In particular, for 225 W laser power, the nominal 35° inclined surfaces exhibited significant material drops along the downskin, which degraded the geometrical accuracy of the realized part (see Figs. 5c, 8b).
-
(3)
The cross-sections of the analyzed internal channels revealed significant material drops at the vertical fillet radii when medium laser energies were employed, observing a general jagged profile for each characterized process condition (see Fig. 5b, 8c).
Table 6 summarizes the experimental results in terms of measured overhang angle and geometrical quality of the vertical fillet radius of the realized cross-sections of the internal channels.
The experimental investigation reported in Table 6 showed that the combinations of process parameters involving 225 W resulted in the largest and in the smallest dimensional deviations of the measured inclined angle (i.e., test 225_750_100 showed a measured angle deviation of + 4.91° and + 3.62° for 35° and 40°, respectively, while test 225_500_120 showed a measured angle deviation of − 0.51° and + 0.09). Nevertheless, for both cases, a high degradation of the part edges in terms of material drops and jagged edges was detected. On the contrary, using low laser power limited the formation of geometrical defects, increasing the overall quality of the realized samples. However, for energy densities ranging between 83.3 and 150 J/mm3, strong deviations of the overhang angle were observed even for 150 W. The cross-sections of the inner channels generally showed a 100 µm–300 µm material collapse at the vertical fillet radii followed by indented edges. Figure 10 reports micrographs sections of test 150_1000_80 and 150_1000_100 as a function of the designed zones.
4 Discussion
Considering the results of the first screening step reported in Table 4, the reason for the building failure was the fusion/combustion debris accumulated on the border of the samples, resulting in thick solidified protrusions (see Figs. 10b and 11a), combined with a significant particle spattering occurring at high laser power, that contaminated the surrounding powder bed due to a considerable ejection of molten material (see Fig. 12a). The formation of solidified protrusions damaged the polymeric wiper of the recoater and it was no longer possible to properly cover the building plate with fresh H13 powder (see Fig. 4b). This kind of defect was observed for all the combinations of process parameters involving high laser power (i.e., 300 W—see Fig. 12a) as confirmed by Narvan et al. [15] which demonstrated protrusions’ formation for high VED. Moreover, the intense sparks and combustion debris occurring at 300 W compromised the fabrication of test samples located in their proximity, which involved lower laser power (i.e., 225 W and 150 W) and medium–low VED ranging between 125 and 62.5 J/mm3. The strong contamination and quality degradation of the powder bed surrounding 300 W test samples forced to interrupt the fabrication of tests 1 (see Fig. 7a), 3, 8, and 25 (see Fig. 3) due to defects’ formation induced by spattering and the impact of protrusion with the recoater wiper (see Fig. 3 and Table 4). In addition, the realization of tests 11, 12, and 13 involving 225 W and a scan speed of 1000 mm/min/s was interrupted due to protrusion formation that mainly occurred in zone 3 (see Fig. 12b). At the moment of article writing, the reason for the occurrence of this phenomenon for these last three samples (11, 12, and 13) is hardly explainable and further analysis is required. The authors have planned to repeat the test samples involving a laser power of 225 W to avoid the influence of particle spattering occurring at 300 W during sample manufacturing and deeply characterize the correlation between the SLM process parameters and the protrusion formation for a laser power of 225 W.
On the contrary, the printing of test samples involving a laser power of 150 W was successfully completed. The lower value of the laser power limited the formation of sparks and dense fumes, preventing the detrimental contamination of the powder bed and enabling the complete printing of the samples.
The internal analysis performed on the successful as-built samples confirmed the previous investigation concerning the detrimental influence of intense fumes and sparks on the structural quality of the realized part. All the samples involving 225 W exhibited a marked internal porosity increasing with sample height. The worst case was the test 225_750_100 showing an internal density that decreased from 99.73% to 99.35% moving from Zone 1 to Zone 4 (see Table 7). On the contrary, H13 samples fabricated at low laser power showed a higher internal density with a more homogeneous pore distribution. The performed internal analysis highlighted the importance to limit the formation of fumes and sparks during the SLM manufacturing of H13 samples, underlining the significance of optimizing SLM process parameters to reduce the powder bed contamination and increase process quality. For this reason, the authors chose to perform the following analyses focusing on the observed geometrical and internal quality of the as-built samples realized at 150 W, neglecting the tests performed at 225 W due to the poor detected structural quality.
Except for test 150_500_80, which failed due to its proximity to the sample manufactured at 300 W, all the as-built H13 samples realized at 150 W showed an internal density higher than 99.00%, exhibiting an internal porosity ranging between 0.08% and 0.69% (see Table 5). This result demonstrated that, for the evaluated experimental range, the employment of low levels for the laser power enabled the fabrication of dense H13 samples also for VED ranging between 50 and 100 J/mm3 and Es ranging between 2.1 and 4.3 J/mm2. On the contrary, the lowest level of VED (i.e., 41.7 J/mm3) in conjunction with the lowest level of Es (i.e., 2.1 J/mm2) did not ensure a full melt pool formation resulting in a high number of lack of fusions which degraded the internal density of the part, increasing the internal porosity up to 0.69%. This outcome was deeply explained by [15, 36] and it is mainly related to the increase of the laser speed that, for constant laser power, results in insufficient energy input to properly melt the powder particles, with a consequent lack of fusion between layers. The presence of irregular pores due to lack of fusion reduces both the resistance to failure and the ductility of as-built SLM parts as demonstrated in [37]. For this reason, combinations of process parameters resulting in lacks of fusions should be avoided in the manufacturing of metallic components by SLM.
Considering the milling tool component presented by the authors in [23] and from which the sample geometry was designed, acceptable densities for application range between 99.80% and 99.99%. In our work, the majority of the realized samples exhibited an internal density higher than 99.80% (e.g., the lower internal porosity of 0.08% was achieved by test 150_500_120). However, all the completed samples are currently undergoing stress relief and HIP treatments that could improve the internal density of samples 4, 16, and 20 (see Table 5). A second work will reconsider all the porosity measurements post-heat treatments for all the processed samples.
Low geometrical deviations from the nominal 35° overhang angle were obtained for VED ranging between 50 and 62.5 J/mm3. For VED higher than 62.5 J/mm3, an increase in the dimensional deviation was observed. In particular, for VED ranging between 83.3 and 100 J/mm3, a strong degradation of the edges’ accuracy was observed, detecting a significant material drops along the downskin side of the inclined surface. The reason of such behavior was mainly related to the input energy involved in powder melting and melt pool cooling rate. High VED increases the size and the temperature of the melt pool, reducing both the viscosity and the cooling rate of the molten material which drops downwards due to the gravity force, not being able of self-supporting. At constant VED, this phenomenon was amplified for high Es, causing dimensional deviations up to + 4.34°. On the contrary, for 41.7 J/mm3 the process was unable to properly reproduce the designed overhang due to the high presence of lack of fusions which compromises the integrity of the parts’ edges and feature profile. Compared to the nominal 35° overhang, for the nominal 40° overhang, dimensional deviations lower than 2° were achieved for a wider range of VED, detecting a strong geometry degradation only for test 150_500_100, which involved a VED of 100 J/mm3.
Larger deviations from the nominal dimensions were obtained for the cross-sections of the internal channels. Contrary to the realized overhang, defects such as material drop or jagged edges were observed for all the evaluated combinations of process parameters (see Fig. 10). Specifically, the dimension of the material collapse detected at the vertical fillet radii increased with the involved laser power and VED, reaching a maximum length of 300 µm. Nevertheless, for low laser power (150 W) and medium–high hatching distance (80–100 μm), acceptable results were obtained. These results provided an indication on the capabilities of the SLM process in manufacturing self-supported features.
5 Conclusion
A structured experimental campaign was conducted to establish a set of process parameters suitable for the SLM additive manufacturing of H13 tool steel powder. Sample geometries were designed based on the dimensions and the geometric features of a milling tool previously presented by the authors: two overhanging surfaces with different slopes (35° and 40°) and internal channels with different triangular cross-sections and vertical fillet radii between 0.5 and 0.6 mm.
The experimental campaign highlighted the importance to limit the formation of fumes and sparks during SLM process optimization of H13 tool steel powder to reduce the powder bed contamination, prevent protrusion formation, and increase process quality. In particular, a laser power equal to 150 W ensured high internal quality in terms of porosity homogeneity reaching an 99.9% internal density. Among these combinations, medium–low values of VED (< 65 J/mm3) and Es (< 3 J/mm2) resulted in low geometrical deviations from the nominal overhang angles with limited material drop, increasing the final geometrical accuracy of the realized H13 parts. However, the lowest level of VED (41.7 J/mm3) in conjunction with the lowest level of Es (2.1 J/mm2) resulted in a high number of lack of fusions.
Finally, the experimental outcomes underlined that high-quality H13 parts exhibiting high internal density and low deviations from the nominal design are feasible by means of an adaptation of the SLM process parameters based on both the geometrical shape and requirements of the part to be realized. In particular, with regard to the evaluated experimental range, H13 samples showing an internal density of 99.92% and a low geometrical deviation of + 0.23° and − 0.90° of the measured 35° and 40° sloping angle, respectively, can be achieved involving 150 W, 500 mm/s, and 120 µm for the layer infill in conjunction with 150 W, 1000 mm/s, and 100 µm for the layer contour.
The fabricated samples are currently undergoing a sequence of heat treatments (such as stress relieving and HIP) to analyze the evolution of residual stresses and microstructure behavior as a function of the treatment temperature profile and have a final porosity and geometry evaluation, comparing the results obtained pre- and post-heat treatments. The analysis will integrate the results reported in this work to finally select a suitable process parameters combination for the SLM manufacturing of H13 tools. The exploitation of these results for defect classification and parameter analysis will provide valuable insights into the intricacies of the observed defects, contributing in future research works to get targeted and efficient approaches to monitoring and control. Furthermore, these findings will be helpful in validating numerical models for SLM.
Data availability
The authors declare that the data supporting the findings of this study are available within the paper. Supplementary information can be requested from the corresponding author.
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Acknowledgements
The authors would like to thank Schneider Tools, Kind Special Alloy and Prima Power, who sponsored and supported the research. The authors would like to mention that the present work has been carried out in the framework of the AITeM-PromozioneL@ser association.
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Impaziente, F., Giorleo, L. & Mazzucato, F. Selective laser melting of H13 tool steel powder: effect of process parameter on complex part production. Prog Addit Manuf 9, 1071–1084 (2024). https://doi.org/10.1007/s40964-023-00504-w
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DOI: https://doi.org/10.1007/s40964-023-00504-w