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Analysis of the volatile oil from the stem of Acanthopanax Senticosus (Rupr. et Maxim.) harms with several hyphenated methods of chromatography

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Frontiers of Chemistry in China

Abstract

Gas chromatography/quadrupole mass spectrometry (GC/qMS), gas chromatography/Fourier transform infrared spectrometry (GC/FTIR) and gas chromatography/orthogonal acceleration time-of-flight mass spectrometry (GC/oaTOFMS) were applied to analyze the volatile oil from the stem of Acanthopanax Senticosus (Rupr. et Maxim.) Harms. Based on the mass spectra search function of GC/qMS with the aid of the discriminability of the geometrical isomer by GC/FTIR and the ability to determine the accurate mass charge ratio (m/z) by GC/oaTOFMS, 68 GC eluants were identified successfully. Compared with the results obtained by GC/qMS only, the analytical results obtained by these hyphenated methods of gas chromatography are more credible.

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Authors and Affiliations

  1. Advanced Analytical Center, Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian, 116023, China

    Yu Wanying

  2. Dalian Institute of Chemical Physics, Chinese Academy of Sciences, Dalian, 116023, China

    Zhang Hua, Huang Weidong, Chen Jiping & Liang Xinmiao

Authors
  1. Yu Wanying
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  2. Zhang Hua
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  3. Huang Weidong
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  4. Chen Jiping
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  5. Liang Xinmiao
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Corresponding authors

Correspondence to Yu Wanying or Chen Jiping.

Additional information

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Translated from Chinese Journal of Chromatography, 2005, 23(2)(in Chinese)

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Yu, W., Zhang, H., Huang, W. et al. Analysis of the volatile oil from the stem of Acanthopanax Senticosus (Rupr. et Maxim.) harms with several hyphenated methods of chromatography. Front. Chem. China 1, 193–198 (2006). https://doi.org/10.1007/s1458-006-0008-y

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  • DOI: https://doi.org/10.1007/s1458-006-0008-y

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