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Magnetic solid-phase extraction of quercetin on magnetic-activated carbon cloth (MACC)

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Abstract

Magnetic-activated carbon cloth (MACC) was synthesized, characterized, and used as magnetic adsorbent in magnetic solid-phase extraction of quercetin prior to UV–visible spectrophotometric determination. Different parameters such as pH, amount of MACC, effect of volume, and elution time were optimized for the determination of quercetin using UV–visible spectrophotometer at 370 nm. In this procedure, quercetin molecules in aqueous sample phase were adsorbed on the 10 mg of the adsorbent at pH 4.0 and desorbed with acidic methanol solution by using vortex mixer. Limit of detection (LOD), limit of quantification (LOQ), and relative standard deviation were found as 1.4 ng mL−1, 4.8 ng mL−1 and lower than 10%, respectively. The applicability of the developed magnetic solid-phase extraction method was proved on onion samples.

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Acknowledgements

Muhammad Balal Arain is very much thankful to the Scientific and Technological Research Council of Turkey (TUBITAK) under “2216 Research Fellowship Programme for Foreign Citizens” for financial support. The authors also would like to thank to Erciyes University, Kayseri, Turkey, for providing all laboratory facilities and pleasant environment.

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Sciences, Erciyes University, 38039, Kayseri, Turkey

    Muhammad Balal Arain & Mustafa Soylak

  2. Department of Chemistry, University of Karachi, Karachi, Sindh, 75270, Pakistan

    Muhammad Balal Arain

  3. Department of Chemistry, Abdul Wali Khan University, Mardan, KPK, 23200, Pakistan

    Muhammad Balal Arain

  4. Department of Analytical Chemistry, Faculty of Pharmacy, Erciyes University, 38039, Kayseri, Turkey

    Erkan Yilmaz

  5. Nanotechnology Research Center (ERNAM), Erciyes University, 38039, Kayseri, Turkey

    Erkan Yilmaz

  6. Engineering Faculty, Akdeniz University, 07058, Antalya, Turkey

    Numan Hoda

  7. National Center of Excellence in Analytical Chemistry, University of Sindh, Jamshoro, 76080, Pakistan

    Tasneem Gul Kazi

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  1. Muhammad Balal Arain
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  2. Erkan Yilmaz
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Correspondence to Mustafa Soylak.

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Arain, M.B., Yilmaz, E., Hoda, N. et al. Magnetic solid-phase extraction of quercetin on magnetic-activated carbon cloth (MACC). J IRAN CHEM SOC 16, 1365–1372 (2019). https://doi.org/10.1007/s13738-019-01622-5

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  • DOI: https://doi.org/10.1007/s13738-019-01622-5

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