Skip to main content
Log in

Influence of Cryo-cross Rolling and Post-Rolled Annealing on Microstructure and High Cycle Fatigue Properties of Al-5052 Alloy

  • Peer-Reviewed Paper
  • Published:
Metallography, Microstructure, and Analysis Aims and scope Submit manuscript

Abstract

The present work investigates the influence of cryo-cross rolling (CCR) followed by annealing (CCR + AN) on high cycle fatigue (HCF) of ultrafine grain (UFG) Al 5052 alloy. CCR process was utilized to reduce the thickness of Al 5052 alloy sheets nearly 90% of initial thickness at liquid nitrogen temperature (− 196 °C). In order to investigate the effect of heat treatment on mechanical properties such as yield strength, tensile strength and high cycle fatigue properties, the CCR specimen was heated at a temperature range of 100–250 °C for 45 min. Microstructure of all the specimens and their synergistic effects were analyzed through electron back scattered diffraction, transmission electron microscopy and field emission scanning electron microscope. The formation of UFG-based microstructure and reduced grain size eliminates the chances of stress concentration near the fracture point, resulting higher HCF strength in CCR sample compared to solution treated alloy. On annealing CCR + AN alloy showed exceptional HCF properties, up to 100 °C. This is attributed to enhancement in fracture growth resistance caused by precipitation interaction at grain boundaries. The HCF strength slowly decreases as temperature of annealing rises from (100–250 °C), owing to grain coarsening due to recrystalisation and recovery process in the mentioned temperature range.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6

Similar content being viewed by others

References

  1. G. Wang, D. Song, Z. Zhou, N. Liang, Y. Wu, A. Ma, J. Jiang, Developing high-strength ultrafine-grained pure Al via large-pass ECAP and post cryo-rolling. J. Mater. Res. Technol. 15, 2419–2428 (2021)

    Article  CAS  Google Scholar 

  2. J. Liu, Y. Wu, L. Wang, H. Wang, C. Kong, A. Pesin, P. Zhilayaeav, H. Yu, Fabrication and characterization of high-bonding-strength Al/Ti/Al-laminated composites via cryorolling. Acta Metall. Sin. Engl. Lett. 33, 871–880 (2020)

    Article  CAS  Google Scholar 

  3. F. Taghavi, H. Saghafian, Y.H.K. Kharrazi, Study on the effect of prolonged mechanical vibration on the grain refinement and density of A356 aluminum alloy. Mater. Des. 30, 1604–1611 (2009)

    Article  CAS  Google Scholar 

  4. P. Kaur, D.K. Dwivedi, P.M. Pathak, Effects of electromagnetic stirring and rare earth compounds on the microstructure and mechanical properties of hypereutectic Al–Si alloys. Int. J. Adv. Manuf. Technol. 63, 415–420 (2012)

    Article  Google Scholar 

  5. L. Katgerman, F. Dom, Rapidly solidified aluminium alloys by meltspinning. Mater. Sci. Eng. A. 375–377, 1212–1216 (2004)

    Article  Google Scholar 

  6. X. Chen, G. Huang, S. Liu, W. Mingwei, B. Jiang, A. Tang, Y. Zhu, F. Pan, Grain refinement and mechanical properties of pure aluminum processed by accumulative extrusion bonding. Trans. Nonferrous Met. Soc. China Engl. Ed. 29, 437–447 (2019)

    Article  CAS  Google Scholar 

  7. S. Liu, W. Yang, X. Shi, B. Li, S. Duan, H. Guo, J. Guo, Influence of laser process parameters on the densification, microstructure, and mechanical properties of a selective laser melted AZ61 magnesium alloy. J. Alloys Compd. 808, 151160 (2019)

    Article  CAS  Google Scholar 

  8. F. Liu, H. Yuan, S. Goel, Y. Liu, J.T. Wang, Bulk nanolaminated nickel: preparation, microstructure, mechanical property, and thermal stability. Metall. Mater. Trans. A Phys. Metall. Mater. Sci. 49, 576–594 (2018)

    Article  CAS  Google Scholar 

  9. Y. Sun, M. Aindow, R.J. Hebert, T.G. Langdon, E.J. Lavernia, High-pressure torsion-induced phase transformations and grain refinement in Al/Ti composites. J. Mater. Sci. 52, 12170–12184 (2017)

    Article  CAS  Google Scholar 

  10. H. Yu, M. Yan, J. Li, A. Godbole, C. Lu, K. Tieu, H. Li, C. Kong, Mechanical properties and microstructure of a Ti–6Al–4V alloy subjected to cold rolling, asymmetric rolling and asymmetric cryorolling. Mater. Sci. Eng. A. 710, 10–16 (2018)

    Article  CAS  Google Scholar 

  11. L. Wang, Y. Xiao, C. Kong, H. Yu, Improvement in strength and ductility of asymmetric-cryorolled copper sheets under low-temperature annealing. Int. J. Lightweight Mater. Manuf. 49, 4398–4403 (2018)

    Google Scholar 

  12. C.H. Su, T.C. Chen, L.W. Tsay, Improved fatigue strength of Cr-electroplated 7075–T6 Al alloy by micro-shot peening. Int. J. Fatigue. 167, 107354 (2023)

    Article  CAS  Google Scholar 

  13. S.K. Panigrahi, R. Jayaganthan, Effect of rolling temperature on microstructure and mechanical properties of 6063 Al alloy. Mater. Sci. Eng. A. 492, 300–305 (2008)

    Article  Google Scholar 

  14. V. Kumar, D. Kumar, Investigation of tensile behaviour of cryorolled and room temperature rolled 6082 Al alloy. Mater. Sci. Eng. A. 691, 211–217 (2017)

    Article  CAS  Google Scholar 

  15. A. Joshi, K.K. Yogesha, R. Jayaganthan, Influence of cryorolling and followed by annealing on high cycle fatigue behavior of ultrafine grained Al 2014 alloy. Mater. Charact. 127, 253–271 (2017)

    Article  CAS  Google Scholar 

  16. R. Pant, S. Singh, A. Joshi, K. Joshi, K.K. Saxena, Mechanical performance and characteristics evaluation of material through Cryo rolling process: a review. Mater. Today Proc. 62, 3086–3096 (2022)

    Article  Google Scholar 

  17. Y.B. Lee, D.H. Shin, K.T. Park, W.J. Nam, Effect of annealing temperature on microstructures and mechanical properties of a 5083 Al alloy deformed at cryogenic temperature. Scr. Mater. 51, 355–359 (2004)

    Article  CAS  Google Scholar 

  18. S.K. Panigrahi, R. Jayaganthan, V. Pancholi, Effect of plastic deformation conditions on microstructural characteristics and mechanical properties of Al 6063 alloy. Mater. Des. 30, 1894–1901 (2009)

    Article  CAS  Google Scholar 

  19. M.K. Pathak, A. Joshi, K.K.S. Mer, Improvement of tensile and fracture toughness properties of Al 2014 alloy processed by different rolling method followed by post-ageing treatment. Trans. Indian Inst. Met. 74, 679–689 (2021)

    Article  CAS  Google Scholar 

  20. G.V.S. Kumar, K.R. Mangipudi, G.V.S. Sastry, L.K. Singh, Excellent combination of tensile ductility and strength due to nanotwinning and a biamodal structure in cryorolled austenitic stainless steel. Sci. Rep. (2020). https://doi.org/10.1038/s41598-019-57208-x

    Article  Google Scholar 

  21. Y. Li, Y. Chen, X. Zhou, Effects of cryogenic treatment and tempering on mechanical properties and microstructure of 0.25C–0.80Si–1.6Mn steel. Adv. Mater. Sci. Eng. (2020). https://doi.org/10.1155/2020/1501474

    Article  Google Scholar 

  22. K. Hockauf, M.F.-X. Wagner, T. Halle, T. Niendorf, M. Hockauf, T. Lampke, Influence of precipitates on low-cycle fatigue and crack growth behavior in an ultrafine-grained aluminum alloy. Acta Mater. 80, 250–263 (2014)

    Article  CAS  Google Scholar 

  23. S. Vigneshwaran, K. Sivaprasad, R. Narayanasamy, K. Venkateswarlu, Superior strength with enhanced fracture resistance of Al–Mg–Sc alloy through two-step cryo cross rolling. Metall. Mater. Trans. A Phys. Metall. Mater. Sci. 50, 3265–3281 (2019)

    Article  CAS  Google Scholar 

  24. M.J. Eskandari, M.A. Asadabad, R. Tafrishi, A. Shafyei, Evolution of Nanostructure in Al 1050 sheet deformed by cryo-cross-rolling. J. Mater. Eng. Perform. 25, 1643–1649 (2016)

    Article  CAS  Google Scholar 

  25. S. Goel, J. Rengaswamy, I. Singh, D. Srivastava, G.K. Dey, N. Saibaba, Texture evolution and ultrafine grain formation in cross-cryo-rolled zircaloy-2. Acta Metall. Sin. Engl. Lett. 28, 837–846 (2015)

    Article  CAS  Google Scholar 

  26. S. Rawat, B.S. Rawat, A. Gupta, M.K. Pathak, A. Joshi, P. Rawat, P.K. Pant, EBSD studies on cryorolled LM6 Al alloy. Mater. Today Proc. 44, 1969–1974 (2021)

    Article  CAS  Google Scholar 

  27. A. Joshi, N. Kumar, K.K. Yogesha, R. Jayaganthan, S.K. Nath, Mechanical properties and microstructural evolution in Al 2014 alloy processed through multidirectional cryoforging. J. Mater. Eng. Perform. 25, 3031–3045 (2016)

    Article  CAS  Google Scholar 

  28. K.K. Yogesha, A. Joshi, R. Jayaganthan, Fatigue behavior of ultrafine-grained 5052 Al alloy processed through different rolling methods. J. Mater. Eng. Perform. 26, 2826–2836 (2017)

    Article  CAS  Google Scholar 

  29. K.K. Yogesha, A. Joshi, A. Raviraj, R.J. Raja, High-cycle fatigue behaviour of ultrafine grained 5052 Al alloy processed through cryo-forging. Miner. Met. Mater. Ser. (2019). https://doi.org/10.1007/978-3-030-05728-2_14

    Article  Google Scholar 

  30. M. Tayyebi, D. Rahmatabadi, A. Karimi, M. Adhami, R. Hashemi, Investigation of annealing treatment on the interfacial and mechanical properties of Al5052/Cu multilayered composites subjected to ARB process. J. Alloys Compd. 871, 159513 (2021)

    Article  CAS  Google Scholar 

  31. D. Singh, P. Nageswara Rao, R. Jayaganthan, High cyclic fatigue behaviour of ultrafine grained Al 5083 alloy. Mater. Sci. Technol. (U. K.). 30, 1835–1842 (2014)

    Article  CAS  Google Scholar 

  32. P. Das, R. Jayaganthan, T. Chowdhury, I.V. Singh, Fatigue behaviour and crack growth rate of cryorolled Al 7075 alloy. Mater. Sci. Eng. A. 528, 7124–7132 (2011)

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Amit Joshi.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Pant, R., Joshi, A., Singh, S. et al. Influence of Cryo-cross Rolling and Post-Rolled Annealing on Microstructure and High Cycle Fatigue Properties of Al-5052 Alloy. Metallogr. Microstruct. Anal. 12, 505–514 (2023). https://doi.org/10.1007/s13632-023-00961-3

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s13632-023-00961-3

Keywords

Navigation