# A new technique for identification of flow units of shaly sandstone reservoirs

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## Abstract

The available techniques for identification of flow units of shaly sandstone reservoirs are based on different concepts, do not provide satisfactory results, and usually show discrepancy. This research is devoted to evaluating current techniques and developing a new concept capable to identify flow units constituting shaly sandstone reservoirs. A new mathematical model has been developed and validated to identify flow units in shaly sandstone reservoirs. The newly developed concept is called shale number (SN) and combines rock properties, fluid properties, petrophysical properties, and hydraulic flow conditions of shaly reservoir rocks. Fifteen actual, reserved, and fracture-free reservoir samples of shaly sandstone reservoir are used to develop SEM images and measure required rock properties of porosity, permeability, and oil/brine relative permeability. The developed data using SEM images and lab experiments are used to characterize the rocks, test feasibility of permeability-porosity crossplot and flow zone index (FZI) techniques, and validate the newly developed mathematical model. The results revealed that the SEM images are capable to identify the clay types as detrital clays and hairy illites plus clay distribution as filling micropores and coating grains of shaly sandstone formations. The results have proven that techniques of porosity–permeability crossplot and FZI have severe scattering degree of data and poor capability for identification of flow units of shaly sandstone reservoirs. The developed model of SN has been validated and showed superior accuracy in application. A plot of SN versus reservoir quality \( \left( {\sqrt {K/\varphi } } \right) \) provided unique straight lines passing through the origin and capable to delineate flow units of shaly sandstone reservoirs. The newly developed shale number overcomes several drawbacks of previous and current techniques used for identification of flow units. Therefore, the application of the new technique provides improved reservoir description of shaly sandstone reservoirs, which secures better development planning.

### Keywords

Shaly reservoirs Reservoir characterization Flow units Reservoir description### List of symbols

*A*,*B*,*C*Empirical constants

*A*_{o},*A*_{1}Empirical constants for fabric technique

*B*_{o},*B*_{1}Empirical constants for fabric technique

*D*_{p}Pore diameter, inch

*K*_{sh},*K*Shaly sandstone and clean permeability, respectively, md

- GV
Grain volume, cm

^{3}- J(
*S*_{w}) J-function, dimensionless

*K*Rock permeability, md

*K*_{ro},*K*_{rw}End points of oil and water relative permeability curves

- IFT
Interfacial tension, N/cm

- PV
Pore volume, cubic centimeter

*R*_{w}Water resistivity, ohm-m

*R*_{t-irr}True formation resistivity at irreducible water condition, ohm-m

- RQI
Reservoir quality index, micron

- FZI
Flow zone index

- SEM
Scanning electron microscope

- SN
Shale number, dimensionless

- FU
Flow unit

*R*_{x}Pore throat radius at x saturation (%) of a non-wetting phase

*V*_{sh}Shale content, fraction

- RQI
Reservoir Quality Index, micron (μm)

*S*_{w}Water saturation, fraction PV

*V*_{o}·*V*_{w}Velocity of oil and water, respectively, m/sec

### Symbols

- \( \lambdabar \)
Rock-fabric number

- ϕ
_{sh} Shaly sandstone porosity, fraction

- Φz
Pore volume-to-grain volume ratio

- µo
Viscosity, centipoises

- \( \rho_{o} \)
Oil density, gm/cm

^{3}- \( \sigma_{{{\text{O}} - {\text{W}}}} \)
Oil–water interfacial tension, dyne/cm

### Super/subscripts

- EP
End point of relative permeability curve

- irr
Irreducible

- m
_{sh} _{C}ementation exponent for shaly formation- o
Oil

- sh
Shale

- w
Water

- wir
Water irreducible

## Introduction and literature review

Better understanding of reservoir characterization represents key element and critical component for successful field development planning of shaly reservoirs. Accurate reservoir characterization is a prerequisite for efficient and better management of heterogeneous shaly reservoirs. It is important to have a comprehensive understanding of heterogeneity and structural complexity of shaly reservoir under development.

Reservoir characterization is defined as a combined technology using geostatistics, geophysics, petrophysics, geology, and reservoir engineering data to provide detailed description of the reservoir for better reservoir development planning to attain the highest recovery at minimum cost and reduce to a minimum uncertainty in production forecasts (Haldorsen and Damsleth 1993; Phillips 1996). Practical reservoir characterization for compartmentalized heterogeneous reservoirs still represents a real challenge for shaly formations and very difficult endeavor in the oil industry.

The method of hydraulic flow unit has been widely used for classification of rock types in pore scale according to flow properties based on geological parameters and physics of flow. These flow units represent similar compartments of the whole reservoir which have similar geological and petrophysical properties that affect fluid flow and are different from other compartments of the reservoir (Shedid et al. 1998a, b, c; Shedid 2001).

Geologists defined the flow units based on similar depositional and diagenetic environments, using core description and core analysis in cored wells and described them as geological flow units or lithofacies (Ebanks 1987). Geoscientists and geostatisticians (Lee and Datta-Gupta 1999; Duval 2002) introduced and applied the concepts of lithofacies, seismic facies, and electrofacies, but none of these techniques has provided satisfactory results in explanation of complex nature of shales and hydraulics of the reservoirs. Electrofacies analysis is a system for identifying rock types with similar properties out from wireline logs and then delineates the reservoir rocks from the non-reservoir rocks. The technique uses the clustering permeability (K)-mean algorithm which is based on log responses to identify electrofacies.

Petrophysicists characterize flow units based on similar responses of log measurements and describe them as electrofacies. Reservoir engineers characterize flow units based on similar pore size distribution and capillary pressure data with consideration of reservoir conditions (Tiab and Donaldson 2004).

For reservoir engineering applications, reservoir characterization is defined as a reservoir modeling technique that considers rock and fluid properties and predicts the fluid behavior in the reservoir using all available sources of reservoir data including relative permeability (Shedid and Almehaideb 2003).

Shale is type of clastic sedimentary rock comprised dominantly of clay minerals and other clay size fragments contains some silt-sized grains of quartz and feldspar, but other minerals may contain organic frags of source rock. Shale is a fissile rock that splits along bedding planes but claystone has a massive appearance and not fissile. Shales can cause complications for the petrophysicist because they are generally conductive and may therefore mask the high-resistance characteristic of hydrocarbons (Toby 2005). In addition, special equipment is required for evaluation shaly rocks due to a very heterogeneous nature and extreme variation of shale properties.

Nowadays, there is a challenging endeavor of defining the reservoir rock regions that have similar petrophysical and geological properties and also consistently different from surrounding zones for better characterization, modeling and simulation of shaly reservoirs. Modeling reservoir zonation has attracted considerable interests for clean (non-shaly) reservoirs. In the meantime, shaly reservoirs have a little attention because of complexity of shale types and various distribution modes. A brief review of the common flow unit delineation techniques is presented below.

## Reservoir characterization techniques

Geologists, geostatisticians, and reservoir engineers proposed several techniques for reservoir characterization but many of them are in an empirical fashion and mainly not developed for shaly formations. Popular techniques for flow unit zonation of clean and shaly reservoirs are briefly summarized below;

### Permeability–porosity crossplot technique

*K*

_{air}is air permeability (md) and ∅ is rock porosity (fraction).

*R*

_{x}is the pore-throat radius at x saturation (%) of a non-wetting phase and

*A*,

*B*, and

*C*are different empirical constants for sandstone and carbonate reservoirs. Theoretically, all points of the same

*R*

_{x}should have the same flow unit and lie on a straight line on a log–log plot of permeability and porosity.

*R*

_{w}is water resistivity (ohm-m) and

*R*

_{t-irr}is true formation resistivity at irreducible water condition (ohm-m) and coefficient W is approximated ~2.0. Equation 2 is restricted in application to the existence of irreducible water condition, which often disappears after primary phase.

Revil and Cathles (1999) developed the following equation for predicting permeability of shaly reservoirs;

*K*

_{sh}and

*K*

_{o}are shaly and clean permeability (md), respectively. ∅

_{sh}and ∅

_{o}are shaly and clean porosity (fraction), respectively. The cementation exponent is

*m*

_{sh}for shaly formation. The cementation exponent (

*m*

_{sh}) is not only a positive function of the shale content but can reach values much higher than 2.0.

*A*

_{o},

*A*

_{1},

*B*

_{o}, and

*B*

_{1}are empirical constants and parameter \( \lambdabar \) is the rock-fabric characteristic number. The rock-fabric number showed the correlation between porosity (∅), water saturation, and capillary pressure derived from mercury injection.

Apparently, there is no theoretical basis to support the traditional crossplot of the logarithm of permeability versus porosity. Permeability is plotted as a log function only because it appears to be log-normally distributed.

### The J-function technique

*K*is rock permeability (md), ∅ is effective rock porosity (fraction),

*σ*

_{o-w}is oil–water interfacial tension (dyne/cm), and ϴ is contact angle reflecting rock wettability.

The J-function is popular in averaging capillary pressure data for specific rock type from a given reservoir and can sometimes be extended to different reservoirs having the same lithology. It is important to use extreme caution in assuming that this can be done. The reasons for the Leverette J-function inaccuracy may be attributed to the existence of capillary pressure, which is restricted to only the transition zones and lower values of applied capillary pressure measurements. In addition, the J-function inability to identify the flow units is due to the functional form of the J-function combining porosity, permeability, capillary pressure, and contact angle does not allow for reservoir flow unit characterization.

Shedid (2001) developed another J-function suitable for shaly reservoirs. It is based on using in situ conventional well logging data, which is more representative to wettability condition and also have less error chance than routine core measurements of porosity and permeability.

### Carman–Kozeny-based techniques

*k*is clean rock permeability (md) and φ

_{e}is effective porosity (fraction).

_{z}) and flow zone index (FZI) can be calculated by the following equations;

Equation 9 presents a straight line with slope of unity in a log–log plot of RQI vs, φz. The points which lines meet φz = 1 is the average FZI for respective hydraulic unit. Average FZI is useful for estimating permeability of the wells which have no cores. Intersection of this straight line in φ_{z} equal to one is the flow zone index (FZI). Samples which are on a straight line happen to have similar properties and so contribute to make a flow unit. Straight lines with slope of unity are firstly expected for non-shale containing sandstone formation.

The same concept of RQI, given by Eq. 6, was extended for identifying hydraulic flow units in shaly sand reservoirs using different water saturation models of laminated, dispersed, and cation exchange capacity (CEC) shaly sands (Jongkittinarukorn and Tiab 1997; Shedid Elgaghah et al. 2001a, b). These models suffer from absence of irreducible water condition for depleted reservoirs and also they still rely on Carmen–Kozeny idealized porous media represented by a bundle of capillary tubes.

The main objectives of this study are to develop a new model capable to overcome drawbacks of current methods based on Carmen–Kozeny model and identify hydraulic flow units in shaly sandstone reservoirs. The newly developed model combines rock properties, fluid properties, rock-fluid properties and also dynamic conditions of fluid flowing into the shaly sandstone porous medium.

## Experimental setup, procedures and results

Field under consideration is an onshore oil reservoir, located in the Middle East and producing from a shaly sandstone formation. The reservoir is a saturated oil reservoir and geologically has an anticline structure. The provided data by the operating company has shown that zone B of the field contains two geologically different rock lithofacies of C and K.

The laboratory tests were performed to provide routine data of porosity, absolute permeability, saturation, and special data of brine/oil relative permeability. A suit of fifteen actual core samples free of fractures was extracted from three wells A, B and C of an actual shaly sandstone oil reservoir. These cores were coated with aluminum foil and sealed in plastic bags for preservation purpose. The samples were brought to the laboratory and actual formation brine (130,700 mg/liter salinity) of viscosity of 1.01 cp was used as a bit lubricant to cut the cores parallel to the bedding plan with dimensions of 2 inch diameter and 3 inch length. The dean shark was used to clean the cores in cold solvent (chloroform & methanol) extraction soxhlets.

The samples were placed in a drying humidity oven at 75 °C until constant weights were achieved. The plug samples were left to cool to room temperature at 32 °C in a sealed container containing silica gel before start of testing. Chemical and microscopic checks were undertaken to ensure removal of all contaminants prior to testing and core analysis. During this step, the volume of actual brine required to completely saturate the core was measured and used to calculate pore volume of core samples. Then, effective rock porosity was calculated volumetrically.

It is important for shaly rocks to consider only absolute and relative permeability measurements to be carried out with saline water. Moore et al. (1982) showed that fresh water destabilizes clay minerals, and the permeabilities measured with fresh water are greatly underestimated.

Rock properties of actuals samples used

Sample/well # | ∅ | | ∅ | RQI µm | \( \sqrt {K/\varphi } \) SQRT(md) | SN dimensionless |
---|---|---|---|---|---|---|

1-A | 0.228 | 30.42 | 0.295 | 0.363 | 11.55 | 71.25 |

2-A | 0.321 | 43.56 | 0.473 | 0.366 | 11.65 | 71.87 |

3-A | 0.264 | 38.56 | 0.359 | 0.379 | 12.09 | 74.57 |

4-A | 0.096 | 1.83 | 0.244 | 0.401 | 12.76 | 78.75 |

5-A | 0.187 | 1.90 | 0.095 | 0.367 | 11.70 | 72.16 |

6-B | 0.216 | 0.70 | 0.157 | 0.279 | 8.87 | 54.73 |

7-B | 0.136 | 10.71 | 0.082 | 0.489 | 15.58 | 96.13 |

8-B | 0.155 | 1.14 | 0.070 | 0.131 | 4.188 | 25.84 |

9-B | 0.283 | 1.04 | 0.395 | 0.236 | 7.529 | 46.45 |

10-B | 0.175 | 52.10 | 0.212 | 0.542 | 17.25 | 106.46 |

11-C | 0.213 | 28.20 | 0.271 | 0.361 | 11.51 | 70.99 |

12-C | 0.323 | 11.80 | 0.477 | 0.190 | 6.04 | 61.22 |

13-C | 0.197 | 56.34 | 0.245 | 0.531 | 16.91 | 104.34 |

14-C | 0.274 | 36.34 | 0.377 | 0.362 | 11.52 | 71.06 |

15-C | 0.246 | 41.45 | 0.326 | 0.408 | 12.98 | 80.09 |

*S*

_{wi}) and was used as the base permeability when calculating relative permeability ratio (

*K*

_{rw}/

*K*

_{ro}). The flood oil displaced and total production were recorded as a function of time. The flow was terminated when zero oil production recovered. Oil–water interfacial tension is measured to be 28.30 dyne/cm. An example of the brine-oil relative permeability result of sample 13-C is presented in Table 2.

Brine/oil relative permeability measured for sample 13-C

Depth | 6513 ft | Sample # | 13-C |

Brine K | 56.34 md | Porosity | 19.7% |

| 53.13 md | | 44.4% |

| 11.02 md | | 26.5% |

Brine saturation (% PV) | | | |
---|---|---|---|

44.3 | 1.0000 | – | – |

50.2 | 0.4073 | 0030 | 0.074 |

51.5 | 0.3205 | 0.038 | 0.119 |

52.9 | 0.2438 | 0.046 | 0.188 |

54.9 | 0.1723 | 0.058 | 0.339 |

57.1 | 0.1236 | 0.071 | 0.578 |

58.8 | 0.0905 | 0.084 | 0.929 |

60.7 | 0.0618 | 0.101 | 1.641 |

62.7 | 0.0397 | 0.115 | 2.897 |

64.8 | 0.0221 | 0.133 | 6.026 |

67.4 | 0.0981 | 0.157 | 15.92 |

69.6 | 0.0042 | 0.175 | 41.40 |

71.1 | 0.0019 | 0.192 | 99.54 |

73.5 | – | 0.206 | – |

## Application and evaluation of reservoir characterization techniques

The measured experimental data of porosity and permeability, listed in Table 1, and end points of relative permeability, in Table 2, are used to test the suitability of permeability-porosity crossplot and FZI techniques, respectively, for identification of flow units of shaly sandstone reservoirs.

### Application of permeability-porosity crossplot technique

The above relationship, Eq. 10, shows a poor correlating coefficient (*R* ^{2}) = 0.1509. Equation 10 cannot be used generally throughout the reservoir to predict permeability using porosity data for other facies of the field. The developed permeability correlation have the following disadvantages: (1) They do not have good correlation coefficients (*R* ^{2}) = 0.15 for wells A, B, and C, which make them not representative tools for predicting permeability, and (2) they are not capable of predicting flow units of the reservoir. A graphical plot of permeability versus porosity is depicted in Fig. 2.

### Application of flow zone index (FZI) technique

According to the above plot, Fig. 3, it is obvious that data from wells A, B, and C did not delineate hydraulic flow units. Logarithmic plot of RQI vs. φz should have unity slope lines in an ideal condition and each line describes a single-hydraulic flow unit.

## Microscopic rock characterization using SEM analysis

Thin slices of 2 mm each of four core samples (# 4-A, 5-A, 8-B, and 9-B) were used for microscopic rock characterization.

## Development and application of shale number (SN) technique

_{o-w}is oil–water interfacial tension (dyne/cm), µ

_{o}is oil viscosity (cp), \( \rho_{o} \) is oil density (gm/cm

^{3}), k

_{ro}and k

_{rw}are end-point oil and water relative permeability, respectively, φ

_{sh}is shaly sandstone porosity (fraction), and K

_{sh}is shaly sandstone permeability (md). The shale number (SN) is calculated and plotted versus reservoir quality \( \sqrt {K/\varphi } \) yielding three well-defined flow units, as shown in Fig. 8.

Inspection of Fig. 8 shows that the geologically defined facies B consists of three distinct hydraulic flow units. The identified flow units pass through wells A, B and C unless there is a geological barrier. This result is very interesting and means that the shale number technique is capable to produce a more refined reservoir description over the description provided using the porosity–permeability crossplot and FZI, as obtained in this study and presented-above in Figs. 2 and 3, respectively. The sole reason for this more refined reservoir description is that the shale number (SN) considers almost all the important variables of the reservoir such as rock properties (porosity and permeability), contained fluid properties (viscosity and density of oil), and oil-rock petrophysical properties (relative permeability of oil and water, and oil–water interfacial tension).

It is important to emphasize that the application of the RQI concept requires a log–log plot, which usually accumulates data points and reduces accuracy to minimize scattering degree. This RQI log–log plot is based on obtaining a straight line characterizing single flow unit, but the final result still shows high scattering degree of data points and incapability to delineate flow units for shaly sandstone reservoir under investigation, Fig. 3. On the other side, the newly developed shale number (SN) uses a Cartesian plot, which is more accurate for variation of reservoir properties. The SN plot provides the minimum scattering degree. The SN technique also has another advantage of plotting more rock/fluid variables involved in the SN versus dual parameter of permeability and porosity \( \left( {\sqrt {K/\varphi } } \right) \) and not versus ratio of pore volume to grain volume (φz) as for FZI technique.

The above equation, Eq. 12, indicates a very good correlating coefficient *R* ^{2} = 1.0 and has a unique characteristic of a straight line passing through the origin. This equation also can be used to predict the shale number using porosity and permeability of shaly reservoirs. This equation represents a very valuable tool to achieve the minimum cost by calculating shale number without need for other parameters involved in Eq. 11 above.

The developed model in Eq. 13 above reveals that a log–log plot of SN versus reservoir quality should develop a unit slope line describing a flow unit with unique slope of unity.

## Conclusions

- 1.
Scanning electron microscope (SEM) has been used successfully for microscopic reservoir characterization. The SEM images are capable to identify clay type as detrital clays and hairy illites plus clay distribution as filling micropores and coating grains of shaly sandstone formations.

- 2.
Permeability–porosity crossplot and flow zone index techniques have shown poor performance and incapability to identify flow units in shaly sandstone reservoirs.

- 3.
A new concept/technique has been developed to identify flow units constituting shaly sandstone reservoirs. This technique is called shale number (SN) and considers rock and fluid properties, petrophysical properties and dynamic flow conditions.

- 4.
A mathematical model is developed using dimensional analysis and has been validated using actual shaly sandstone rock and fluid samples.

- 5.
The results indicated better identification of flow units using the shale number model in comparison to other rock characterization techniques.

## Notes

### Acknowledgements

This work is conducted as a part of a funded research project supported by the American University in Cairo, AUC, under the contract agreement # SE-PENG-FY 17-RG (2)-2016. The author is grateful to the AUC management for funding this project and encouragement for publication. The author would also like to thank the operating company for continuous support and provision of required fluid and rock samples.

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