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Detection of calcium based neutralizers in milk and milk products by AAS

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Abstract

Current study was carried out with the intent to standardize detection and estimation method for calcium (Ca) based neutralizers in milk and milk based indigenous products (khoa and paneer) using atomic absorption spectroscopy (AAS). Neutralized milk, khoa and paneer samples were prepared using milk with developed acidity to which calculated quantity of neutralizer (Ca based) was added. Rosalic acid test results get masked at times due to developed acidity which neutralizes the alkalinity imparted by neutralizer and hence gives false result with time in neutralizer added samples. Atomic absorption spectroscopy proved to be an accurate estimate which could detect the abnormal rise in mineral concentration even with slight addition of neutralizers in comparison with control milk and milk products. Formalin, which is a commonly used preservative in milk samples for chemical analysis, did not have any significant impact on estimation of calcium in the neutralized milk during storage.

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References

  • Ballance R (1996) Physical and chemical analyses. Water quality monitoring—A practical guide to the Design and implementation of freshwater quality studies and monitoring programmes. UNEP/WHO p:7–103.

  • BIS. 1961. IS (1479) Method of tests for dairy industry. Part II. Chemical analysis of milk. Bureau of Indian standards, Manak Bhavan, New Delhi

    Google Scholar 

  • Boghra VR, Mathur ON (1991) Chemical quality of some marketed indigenous milk products: Major constituents and mineral composition of paneer. J Food Sci Tech 28(1):57–58

    CAS  Google Scholar 

  • De S, Roy SC (1953) Studies on the indigenous method of khoa making. Part I. the influence of the conditions of dehydration and the type of milk on the production of khoa. Indian J Dairy Sci 5(3):147–165

    Google Scholar 

  • Fox PF, McSweeney PLH (1998) Salts of milk. In: Dairy chemistry and biochemistry,1st edn. Thomas Science, London, pp 239–264

    Google Scholar 

  • FSSAI (2012). Executive summary on National Survey on Milk Adulteration.

  • Gunnery KS (1979) Additives in milk and their detection. Ind Dairyman 31(9):665–669

    Google Scholar 

  • IS: SP:18 (1981) ISI handbook of food analysis, Part XI. Dairy products. Indian Standard Institution, Manak Bhawan, New Delhi

    Google Scholar 

  • Juarez M, Martin-Hernandez MC (1983) Content of mineral elements in cheeses from the Spanish market determined by AAS. Rev Agroquim technology Aliment 23:417–426

    CAS  Google Scholar 

  • Khan SU, Pal MA (2010) Quality of paneer made from high solid reconstituted milk as influenced by calcium phosphate incorporation. J Food Technol 8(4):169–174

    Article  CAS  Google Scholar 

  • Mathur MP, Dattaroy D, Dinakar P (1999). Minerals vitamins and minor constituents of milk. In: Text book of Dairy Chemistry. Directorate of Information and Publications of Agriculture, Indian Council of Agricultural Research, Pusa, New Delhi. p.183-214.

  • Mohanan S, Thomas PPG, Lilly I, Laila M, Domini I, Bindu RG (2001) A new ultrasonic method to detect chemical additives in branded milk. Pramana-J Phys 59(3):525–529

    Article  Google Scholar 

  • Pollman RM (1991) AAS determination of calcium and magnesium and colorimetric of phosphorous in cheese: collaborative study. J Assoc Off Analyt Chem 74(1):27–31

    CAS  Google Scholar 

  • Satoskar RS, Bhanderkar SD, Ainapure SS (2000) Pharmacology and Pharmacotherapeutics, 17th edn. Popular Prakashan, Mumbai, 591

    Google Scholar 

  • Snedecor GW, Cochran WG (1989) Statistical methods, 8th edn. Affiliated East–west Press, Iowa State Univ Press, USA

    Google Scholar 

  • Suddendrof RF, Cook KK (1984) Inductively coupled plasma emission spectroscopic determination of nine elements in infant formula: collaborative study. J Assoc Off Analyt Chem 67:985–992

    Google Scholar 

  • Vaessen HAMG, Van de Kamp CG (1990) Reference material based collaborative test of flame AAS determination of calcium and magnesium in foods and biological materials. Z Lebensm Unters Forsch 190(3):199–204

    Article  CAS  Google Scholar 

  • Vishweshwaraiah L, Anantakrishnan CP (1985) A study on technological aspects of preparing paneer from cow’s milk. Asian J Dairy Res 4(3):171–176

    Google Scholar 

  • Wehr HM, Frank JF (2004) Standard methods for the examination of dairy products, 17th edn. American Public Health Association, Washington, pp 519–527

    Book  Google Scholar 

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Sowmya, R., Indumathi, K.P., Arora, S. et al. Detection of calcium based neutralizers in milk and milk products by AAS. J Food Sci Technol 52, 1188–1193 (2015). https://doi.org/10.1007/s13197-013-1091-y

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  • DOI: https://doi.org/10.1007/s13197-013-1091-y

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