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Analysis of microscopic pore structures of the silty clay before and after freezing–thawing under the subway vibration loading

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Abstract

With the rapid development of the subway rail transit, the effect of the cyclic loading on the surrounding foundations and buildings has drawn wide attention. In addition to the in situ tests and the laboratory triaxial tests, microscopic tests also provide an effective way to clarify the physical and mechanical characteristics of soils. On the other hand, the characteristics of the soft silty clay before and after freezing–thawing has been less studied. In this paper, the scanning electron microscope (SEM) tests following the cyclic triaxial tests of silty clay layer were performed to investigate the variations of the microscopic pore structures of the layer before and after freezing–thawing. The corrected Otsu method was used to obtain the binary SEM images of silty clay. The porosity results demonstrate that the magnifications from 1000× up to 5000× were suitable for observation of the silty clay microstructures. The binary SEM images of soil pore structures were quantitatively analyzed, including the porosity, the size distribution, the pore shape coefficient, the pore orientation distribution and the fractal dimension. The pore orientation of samples without loading is arranged in the horizontal direction, while the pores of samples under cyclic loadings are arranged in the vertical. After freezing–thawing, the mean anisotropy value of the microscopic pore structures increased about 12% and the porosity of samples without loadings increases about 11.24%. The lower the freezing temperature is, the larger the porosity within the samples becomes. However, the freezing–thawing has little effect on the pore shape coefficient of the silty clay. The porosity of the silty clay increases with an increase in pore diameter, but it decreases with the increase in excess pore pressure. In addition, the microscopic pore structures of the silty clay exhibit fractal characteristics. The fractal dimension is reduced by the disturbance from the effect of freezing–thawing, coupled with the effect of cyclic loading.

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References

  • Bird N, Diaz MC, Saa A et al (2006) Fractal and multifractal analysis of pore-scale images of soil. J Hydrol 322(1):211–219

    Article  Google Scholar 

  • Chamberlain EJ, Gow AJ (1979) Effect of freezing and thawing on the permeability and structure of soils. Eng Geol 13(1):73–92

    Article  Google Scholar 

  • Cui ZD, Jia YJ (2013) Analysis of electron microscope images of soil pore structure for the study of land subsidence in centrifuge model tests of high-rise building groups. Eng Geol 164:107–116

    Article  Google Scholar 

  • Cui ZD, Zhang ZL (2015) Comparison of dynamic characteristics of the silty clay before and after freezing and thawing under the subway vibration loading. Cold Reg Sci Technol 119:29–36

    Article  Google Scholar 

  • Cui ZD, He PP, Yang WH (2014) Mechanical properties of a silty clay subjected to freezing-thawing. Cold Reg Sci Technol 98:26–34

    Article  Google Scholar 

  • Cui ZD, Zhao LZ, Yuan L (2016) Microstructures of consolidated Kaolin clay at different depths in centrifuge model tests. Carbonates Evaporites 31(1):47–60

    Article  Google Scholar 

  • Dathe A, Eins S, Niemeyer J et al (2001) The surface fractal dimension of the soil-pore interface as measured by image analysis. Geoderma 103(1):203–229

    Article  Google Scholar 

  • De Boever W, Derluyn H, Van Loo D et al (2015) Data-fusion of high resolution X-ray CT, SEM and EDS for 3D and pseudo-3D chemical and structural characterization of sandstone. Micron 74:15–21

    Article  Google Scholar 

  • Ewa KM (2015) SEM investigations of clay subjected to 200MPa pressure. Procedia Earth Planet Sci 15:791–796

    Article  Google Scholar 

  • Hattab M, Fleureau JM (2010) Experimental study of kaolin particle orientation mechanism. Geotechnique 60(5):323–331

    Article  Google Scholar 

  • Hattab M, Fleureau JM (2011) Experimental analysis of kaolinite particle orientation during triaxial path. Int J Numer Anal Meth Geomech 35(8):947–968

    Article  Google Scholar 

  • Hemes S, Desbois G, Urai JL et al (2015) Multi-scale characterization of porosity in Boom Clay (HADES-level, Mol, Belgium) using a combination of X-ray μ-CT, 2D BIB-SEM and FIB-SEM tomography. Microporous Mesoporous Mater 208:1–20

    Article  Google Scholar 

  • Liu JY, Zhang LJ (2014) The microstructure characters of saline soil in Qarhan Salt Lake area and its behaviors of mechanics and compressive strength. Arab J Sci Eng 39(12):8649–8658

    Article  Google Scholar 

  • Liu ZB, Shi B, Inyang HI et al (2005) Magnification effects on the interpretation of SEM images of expansive soils. Eng Geol 78(1):89–94

    Article  Google Scholar 

  • Liu Z, Liang HC, Zhang J (2010) The SEM analysis of rock-soil mini-structure after saturation. GeoShanghai 2010 international conference. Shanghai, China

  • Liu C, Shi B, Zhou J et al (2011) Quantification and characterization of microporosity by image processing, geometric measurement and statistical methods: application on SEM images of clay materials. Appl Clay Sci 54(1):97–106

    Article  Google Scholar 

  • Meisel LV (1991) Perimeter-area analysis, the slit-island method and the fractal characterization of metallic fracture surfaces. J Phys D Appl Phys 24(6):942

    Article  Google Scholar 

  • Ninjgarav E, Chung SG, Jang WY et al (2007) Pore size distribution of Pusan clay measured by mercury intrusion porosimetry. KSCE J Civil Eng 11(3):133–139

    Article  Google Scholar 

  • Othman MA, Benson CH (1993) Effect of freeze-thaw on the hydraulic conductivity and morphology of compacted clay. Can Geotech J 30(2):236–246

    Article  Google Scholar 

  • Otsu N (1975) A threshold selection method from gray-level histograms. IEEE Trans Syst Man Cybern 9(1):62–66

    Article  Google Scholar 

  • Pillai RJ, Robinson RG, Boominathan A (2011) Effect of microfabric on undrained static and cyclic behavior of kaolin clay. J Geotech Geoenviron Eng 137(4):421–429

    Article  Google Scholar 

  • Shi B, Wu Z, Inyang H et al (1999) Preparation of soil specimens for SEM analysis using freeze-cut-drying. Bull Eng Geol Environ 58(1):1–7

    Article  Google Scholar 

  • Tang YQ, Cui ZD, Zhang X et al (2008) Dynamic response and pore pressure model of the saturated soft clay around the tunnel under vibration loading of Shanghai subway. Eng Geol 98(3):126–132

    Article  Google Scholar 

  • Tang YQ, Zhou J, Hong J et al (2012) Quantitative analysis of the microstructure of Shanghai muddy clay before and after freezing. Bull Eng Geol Environ 71(2):309–316

    Article  Google Scholar 

  • Tarquis AM, McInnes KJ, Key JR et al (2006) Multiscaling analysis in a structured clay soil using 2D images. J Hydrol 322(1):236–246

    Article  Google Scholar 

  • Vasseur G, Djeran Maigre I, Grunberger D et al (1995) Evolution of structural and physical parameters of clays during experimental compaction. Mar Pet Geol 12(8):941–954

    Article  Google Scholar 

  • Wang LB, Frost JD, Lai JS (2004) Three-dimensional digital representation of granular material microstructure from X-ray tomography imaging. J Comput Civil Eng 18(1):28–35

    Article  Google Scholar 

  • Wei X, Hattab M, Fleureau JM et al (2013) Micro-macro-experimental study of two clayey materials on drying paths. Bull Eng Geol Environ 72(3):495–508

    Article  Google Scholar 

  • Zhang LM, Li X (2010) Microporosity structure of coarse granular soils. J Geotech Geoenviron Eng 136(10):1425–1436

    Article  Google Scholar 

  • Zhou J, Tang YQ (2015) Artificial ground freezing of fully saturated mucky clay: thawing problem by centrifuge modeling. Cold Reg Sci Technol 117:1–11

    Article  Google Scholar 

Download references

Acknowledgements

This work presented in this paper was supported by the Fundamental Research Funds for the Central Universities (2015XKMS016).

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Correspondence to Zhen-Dong Cui.

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Zhang, ZL., Cui, ZD. Analysis of microscopic pore structures of the silty clay before and after freezing–thawing under the subway vibration loading. Environ Earth Sci 76, 528 (2017). https://doi.org/10.1007/s12665-017-6879-z

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