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Outstanding strength and conductivity of metallic glass composites with multiscale configuration

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Abstract

Cu-based composites with multiscale configuration for electrical contact applications are fabricated via a ball milling (BM)-spark plasma sintering (SPS)-aging process. Synergistic strengthening of the Cu alloy matrix by micro-scale metallic glass particles and nanoscale intracrystalline precipitation phases is realized. The annealing technique achieves the decomposition of solute atoms in the Cu alloy, ensuring the excellent electrical properties of the matrix conductive network. The composite with multiscale configuration achieves an outstanding combination of ultimate compressive strength of (1114 ± 15) MPa and electrical conductivity of 33.0% ± 1.1% International Annealed Copper Standard (IACS) after annealing at 400 °C for 10.0 h. Investigation of the strengthening and conductivity mechanisms suggests that the precipitation of the Cr-rich phase within the matrix crystals is a critical contributor to the concerted enhancement of strength and conductivity. In addition, the positive role of nanocrystals precipitated at the edges of metallic glass particles on the interfacial bonding of composites is addressed.

Graphical abstract

摘要

通过球磨—放电等离子体烧结—时效工艺制备了用于电接触应用的多尺度结构的铜基复合材料。实现了微米级 金属玻璃颗粒和纳米级晶内沉淀相对铜合金基体的协同强化。退火工艺实现了铜合金中溶质原子的脱溶，确保 了基体导电网络的优异电性能。具有多尺度结构的复合材料在400 °C 退火10 h 后达到了(1114±15) MPa 的极 限抗压强度和33.0%±1.1% IACS 的电导率的出色性能组合。对强化机制和导电机制的研究表明，基体晶体中 富铬相的析出是协同增优化强度和导电性的关键因素。此外，还讨论了在金属玻璃颗粒边缘析出的纳米晶体对 复合材料界面结合的积极作用。

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Acknowledgements

The work was financially supported by Shenzhen Knowledge Innovation Plan—Fundamental Research (Discipline Distribution) (No. JCYJ20180507184623297), the National Natural Science Foundation of China (No. 51871077), Guangdong Basic and Applied Basic Research Foundation (No. 2021A1515012626), Shenzhen Science and Technology Plan—Technology Innovation (No. KQJSCX20180328165656256), Development and Reform Commission of Shenzhen Municipality-Shenzhen R&D Center for Al-based Hydrogen Hydrolysis Materials (No. ZX20190229), Startup Foundation from Shenzhen and Startup Foundation from Harbin Institute of Technology (Shenzhen).

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  1. School of Materials Science and Engineering, Harbin Institute of Technology (Shenzhen), Shenzhen, 518055, China

    Wei-Zong Bao, Jie Chen, Jun-Zhi Li, Bo-Hua Yu, Chu-Yuan Liu, Ping Jiang, Zu-Jia Liu, Kai-Tao Hu & Guo-Qiang Xie

  2. State Key Laboratory of Advanced Welding and Joining, Harbin Institute of Technology, Harbin, 150001, China

    Guo-Qiang Xie

  3. Advanced Institute for Materials Research (WPI-AIMR), Tohoku University, Sendai, 980-8577, Japan

    Dmitri V. Louzguine-Luzgin

  4. MathAM-OIL, National Institute of Advanced Industrial Science and Technology (AIST), Sendai, 980-8577, Japan

    Dmitri V. Louzguine-Luzgin

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Bao, WZ., Chen, J., Li, JZ. et al. Outstanding strength and conductivity of metallic glass composites with multiscale configuration. Rare Met. 42, 3099–3113 (2023). https://doi.org/10.1007/s12598-023-02308-x

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