Abstract
The present work aims to describe in detail the petrophysical properties of the Bahariya Formation (Abu Sennan field) through processing the core sample data and finding out the possible relations between permeability and other reservoir parameters such as porosity, specific internal surface, formation factor, and nuclear magnetic resonance to obtain reliable permeability prediction model of the Upper Cretaceous formation. The core samples have a length range of 2–4 cm with a diameter of 2.54 cm. Many petrophysical reservoir parameters were measured, such as permeability, porosity, density, formation factor, and special measurements such as spectral induced polarization, nuclear magnetic resonance, and specific internal surface. The samples cover a wide range of porosity (11.82–23.68 %) and permeability (0.06–133.65 mD). The porosity-permeability relationship indicates the increase of the permeability with porosity increase for the studied samples. The reservoir quality index ranges from 0.02 to 0.78 μm. The flow zone indicator ranges from 0.09 to 3.39 μm where pore throat radius (R35) ranges from 0.10 to 7.40 μm. The reservoir quality index (RQI) and flow zone indicator (FZI) cross-plot show a better understanding of the formation evaluation. The hydraulic flow units are (0.09 μm < FZI ≤ 3.39 μm) and RQI < (1 μm). NMR longitudinal relaxation time T1 range is 1.21–175 ms, NMR transversal relaxation time T2(100) range is 0.70–91.77 ms, and T2(600) range is 0.74–75.86 ms. Models that incorporate porosity and NMR relaxation times will be more accurate and suitable for permeability prediction. Using multiple regression to determine the exponents of the power-law equation and replacing the porosity with the formation factor can improve the permeability prediction for the samples under investigation. The utilizing of NMR in predicting the permeability through a robust model considers an additional value for the Upper Cretaceous rocks in Egypt.
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Introduction
Sandstone is a sedimentary rock (clastic type) composed of sand grains that originally were accumulated sediments subjected to diagenetic processes as cementation to join them into a rock. There are several types of sandstone. A rock is called sandstone if its components are mostly silicate. Different types of rocks are the host of the oil reserve all over the world, among them the sandstone reservoirs that should be porous and permeable. Sandstone petroleum reservoir mostly composed of quartz grains, rock fragments, feldspars, other minerals, and fluid (oil, water, gas) saturated spaces. Sandstone reservoirs mostly have porosity values ranges from 5 to 30% or more, while permeability ranges from 10 to 200 mD or more.
Most of the important hydrocarbon reservoirs in Egypt are in the Western Desert especially the Upper Cretaceous (Cenomanian) Bahariya Formation. Sandstone, limestone, shale, and siltstone are the main components of the Bahariya Formation. Several studies focused on the stratigraphy, tectonic, and sedimentology of the subsurface of the Bahariya Formation due to the importance of this formation in the hydrocarbon production (Soliman et al. 1970; El Gezeery et al. 1972; Franks 1982; Dominik 1985; Catuneanu et al. 2006; El Sayed et.al. 1998; Matthias et.al. 2009; El Sayed 2011; and El Sayed et al. 2019; Farouk et al. 2022 and Harishidayat et al. 2022). The Bahariya Formation was deposited in fluvio-marine to shallow marine conditions at the beginning of the Cenomanian transgression. The depositional environment experienced a coastal back stepping comprising coarsening upward cyclothems and the deposition of sandstones and siltstones and then a shallow marine with tidal flat to marine shelf environment settings. The Bahariya Formation is more or less conformably underlain by the Kharita Formation, where it is conformably overlain by the sandy limestone marker bed that constitutes the basal part of the Upper Cenomanian Abu Roash “G” Member. The Southwest Abu Sennan (SWS) field (the study area) that was located in the Abu Sennan concession is the main reservoir and the highest production in the Bahariya Formation. The location of the concession is between latitudes 29° 32′ and 29° 49′ N and longitudes 28° 35′ and 28° 59′ E in the Western Desert, 260 km west of Cairo and 160 km south of the Mediterranean coast. The concession approximately covers 3600 km2 (Fig. 1).
Location map of the study area, Abu Sennan field in the Western Desert along with the major structural features (Qr, Qattara Ridge; Sr, Sharib-Sheiba Ridge; Kr, Kattaniya Ridge). Adapted from Shalaby and Sarhan (2021)
The stratigraphic sequence of the (SWS) field is part of the North-Western Desert stratigraphic regime, which can be described in terms of the Upper Cretaceous and Tertiary Age. It is marked at many levels by unconformities of different magnitudes at the end of Kharita Formation, Abu Roash “E” Member, and also the end of Abu Roash “A” Member.
Concerning the present work, absolute permeability at the core scale is provided from laboratory measurements, which differ from the reservoir permeability. NMR is the valuable tool for estimating the in situ permeability (Hidajat et al. 2002 and Glover et al. 2006). The effect of the paramagnetic minerals such as iron oxide on the surface relaxivity can cause a shift in the relaxation distribution to a shorter times (Dodge et al. 1995). Previous studies proved a significant effect of the iron-bearing minerals on the permeability measurements using T2 NMR (Lala and El Sayed 2015). The aim of this study is to investigate the rock petrophysical characteristics, process the data from core samples, and then create a petrophysical model to predict permeability from nuclear magnetic resonance (NMR) data, focusing on the Upper Cretaceous Bahariya Formation in Abu Sennan field. The prediction of permeability is considered very important in the oil production and field development phases. The utilizing of NMR in predicting the permeability through a robust model considers an additional value for the Upper Cretaceous rocks in Egypt.
Methodology
Sample preparation and techniques
All the samples of the Upper Cretaceous Bahariya Formation (Abu Sennan field) that were used in this study were cored using a diamond drilling machine; the sample length range is 2–4 cm and with a diameter of 2.54 cm. A solvent has been used to clean the studied samples, and then all the samples were dried in an oven to a constant weight at 105 °C to remove the remaining pore water and cleaning solvent. After the drying process, a petrophysical laboratory investigation was performed to estimate the petrophysical parameters for reservoir, such as density, permeability, porosity, formation factor, and special measurements such as spectral induced polarization, nuclear magnetic resonance, and specific internal surface. The porosity was measured using Core Lab’s Helium Porosimeter; serial no. A–8222, model 3020–062, Dallas, TX, USA. The permeability was measured using Core Lab’s Permeameter, the Mini Permeameter, model 302138, Dallas, TX, USA, and serial no. A–3148. The specific internal surface was measured using the nitrogen adsorption technique. The spectral induced polarization (SIP) was measured using the method mentioned in the “Spectral induced polarization” section. Relaxation measurements were performed with an NMR Rock Core Analyzer mentioned in the “Nuclear magnetic resonance” section.
Porosity
The definition of reservoir rock porosity Φ is the fraction of the reservoir bulk volume that is occupied with fluids to the solid framework of the reservoir (Tiab and Donaldson 2015). Mathematically, it can be expressed as Eq. (1):
Φ is the porosity, frac. ; Vb is the bulk volume, cm3; Vg is the grain volume, cm3; Vp is volume of pore space, cm3.
Porosity controls the reservoir storage capacity which explains how important it is for determining the stored volume of reservoir fluids. Well logs and depositional environment interpretation were used for the prediction of reservoir evaluation (Al-Ghuribawi and Faisal 2021).
Permeability
Rock permeability is the ability of a porous material to transmit fluid. Darcy’s law describes permeability in porous media. Permeability depends on multiple parameters like cementation, pore geometry, texture of the rock, grain size, and shape. Many studies investigated the porosity-permeability relationship (e.g., Carman 1937; Timur 1968; Scheidegger 1974; Herron 1987; Adler et al. 1990; Schön 1996; Tiab and Donaldson 2015 and Lala and El Sayed 2017). Nitrogen gas permeameter was used to measure the permeability of the studied samples. The gas permeability (k) is determined in a steady-state flow experiment using the pressure difference of upstream pressure (P1) and downstream pressure (P2) to calculate the flow rate q as shown in Eq. (2), the Darcy equation that relates the permeability to the compressible fluids.
k is the permeability of the porous media, mD. μ is the fluid viscosity, centipoises (cP). q is the flow rate cm3/s. L is the rock sample length, cm. A is the cross-sectional area of the rock, cm2. P1 and P2 are the inlet and outlet pressures, atm/cm.
Flow unit
The reservoir heterogeneity and quality were determined using the hydraulic flow unit introduced by Amaefule et al. (1993), where RQI and FZI were defined as per Eqs. (3) and (4):
RQI is the reservoir quality index, μm. K is the permeability, mD. Φ is the porosity, frac. FZI is flow zone indicator, μm.
Estimated pore throat sizes (R35) from core-based porosity-permeability properties have been done.
Specific internal surface
In the inhomogeneous and isotropic rocks, porosity is the available fraction of the rock for fluid flow. However, the individual pore sizes that control the fluid flow are not be identified using porosity as an input data. Therefore, it is crucial to evaluate the average pore size and/or the pore throat size as input for permeability prediction models. We focus on using the surface area per unit pore volume (Spor, cm−1) to estimate the pore size. Based on a capillary bundle model, the Spor is inversely proportional to the pore radius (r, μm), where (A) is the total surface of the sample in cm2 and vp is the pore volume.
Equation (6) shows that Spor can be calculated using the mass-related specific internal surface (Sm) in cm2/g when the porosity in (frac.) and the grain density (dg, g/cm3) of the material are known.
Measuring the specific internal surface is done by using BET method through nitrogen gas adsorption technique (after Brunauer et al., 1938).
Spectral induced polarization
The specific internal surface Spor also affects the spectral induced polarization (SIP). The rock induced polarization (IP) is affected by the electrical double layer (EDL) that forms along with the solid-liquid interface; this phenomenon has been thoroughly studied using theoretical and conceptual models where the polarization of the EDL surrounding a mineral grain and the polarization of pore throats were considered (e.g., Lesmes and Morgan 2001; Revil and Florsch 2010; Marshall and Madden 1959; and Titov et al. 2002). A linear relation between Spor and the electrical conductivity imaginary part and/or the normalized chargeability (mn) was identified by Weller et al. (2010b). The samples were saturated using 0.526 g/l (σw ≈ 0.1 S/m) sodium chloride solution (Abuseda et al. 2016). The saturated samples were installed in a core holder connected to two tanks with platinum current electrodes. The voltage was recorded by using the chlorinated silver wire rings that surround the sample as an electrode. All measurements were recorded in a climate controlled cabinet which also acts as a Faraday cage to reduce the influence of external electromagnetic noise. The temperature used was 20 °C. The error of the resistivity amplitude of the repeated SIP measurements is less than 3%, while the phase angles of complex resistivity determination error is less than 0.5 mrad.
Nuclear magnetic resonance
Another estimation of Spor can be obtained using NMR. Coates et al. (1999) presented an excellent review of the NMR logging principles, while we only provide a brief fundamentals summary. Both the free pore fluid slow relaxation and pore surface’s direct vicinity fast relaxation control the magnetic relaxation of excited hydrogen nuclei in a wetting pore fluid. If a fast diffusion exchange between the fluid at the pore surface and free pore fluid is present, a uniform pores’ magnetization will exist, and the relaxation time will be proportional to the ratio of volume to surface. It is important to determine the spectrum of different relaxation times in the case of varying pore size distributions which can be differentiated from the different types of relaxation times. The relation between the relaxation times and the surface to volume ratio which corresponds to the Spor (Kenyon, W.E., 1992) is expressed as follows:
where T1,2 are NMR longitudinal and transversal relaxation times. β is the surface relaxivity.
In free fluids, no large difference is observed between T1 and T2, because the relaxation time depends on the fluid viscosity. In natural rocks, the diffusion of the hydrogen nuclei in an inhomogeneous magnetic field generates dephasing effects that shorten T2 due to the susceptibility distribution. An NMR Rock Core Analyzer (Magritek) operating at a Larmor frequency of 2 MHz was used for the relaxation measurements at ambient pressure and temperature. We used a constant and short echo spacing of 600 μs to eliminate the effect of diffusion. The sample axis was perpendicularly oriented with respect to the instrument’s horizontal static magnetic field. The T1 and T2 relaxation times accuracy was in the order of 10%.
Results and discussions
The samples cover a wide range of porosity (11.82–23.68%) with an average value of 18.25%, permeability (0.06–133.65 mD) with an average value of 51.02 mD, formation factor (12.45–62.40) with an average value of 26.23, specific internal surface (1.35–147.91 1/μm) with an average value of 40.33 1/μm, and imaginary sigma (0.04–0.32 mS/m) with an average value of 0.15 mS/m. NMR longitudinal relaxation time T1 range is 1.21–175 ms with an average value of 60.19 s, NMR transversal relaxation time T2(100) range is 0.70–91.77 ms with an average value of 35.99 s, T2(600) range is 0.74–75.86 ms with an average value of 28.85 s, the reservoir quality index ranges from 0.02 to 0.78 μm with an average value 0.39 μm, flow zone indicator ranges from 0.09 to 3.39 μm with an average value 1.52 μm, and lastly pore throat radius (R35) ranges from 0.10 to 7.40 μm with an average value 3.40 μm.
Petrophysical relationships
The main objective in this paper is to reveal the relationships between different petrophysical parameters and design a petrophysical model to estimate an important reservoir property that is difficult to be measured either in the laboratory or in the field.
Porosity-bulk density
An inverse relationship between bulk density and porosity is shown for Upper Cretaceous sandstone samples in Fig. 2. The following equation controls the relationship
Coefficient of determination (R2 = 0.87).
where the bulk density db given in g/cm3 and the porosity Φ as a fraction. The sandstone samples are characterized by high porosity and low density.
Permeability-porosity
In the present work, Fig. 3 shows the porosity-permeability cross-plot of the investigated samples. The data follows the expected positive trend between porosity and permeability. The relationship is characterized by a weak coefficient of determination of 0.42. The samples generally show lower porosity and permeability indicating that the samples are filled by clay minerals that cause a decrease in porosity and permeability (Abuseda and El Sayed 2022). The relation is controlled by the following equation:
Reservoir quality index-porosity
Figure 4 displays the relationship between the porosity and the reservoir quality index (RQI) for all samples. The samples are characterized by RQI > 1 μm. These values indicate a fair to impervious reservoir quality. The porosity-RQI relationship reads:
It is characterized by a low coefficient of correlation (R2 =0.37).
Reservoir quality index-permeability
Considering the definition of the RQI in Eq. (3), a strong correlation is expected between permeability and RQI. Figure 5 displays the nearly linear relationship between the permeability (k) and the RQI. We got the following equation:
It is characterized by a coefficient of correlation (R2 =0.997). The reservoir quality index reflects mainly changes in permeability.
Flow zone indicator-porosity
Figure 6 shows the relationship between the flow zone indicator and porosity for the studied Upper Cretaceous sandstone samples. Considering all data points, the graph elucidates a weak relationship between FZI and porosity. The data points follow the expected positive trend between porosity and flow zone indicator for all investigated samples.
Flow zone indicator-permeability
Figure 7 shows the FZI as a function of the permeability for the studied rock samples, which are described by the following equation:
Considering the definition of FZI in Eq. (4), we found that the FZI depends mainly on permeability with a high coefficient of determination (R2 = 0.97).
Hydraulic flow units (HFUs)
Many authors used HFUs for permeability modeling and rock typing (e.g., Farouket al. 2021; Kassab and Taema 2018). The core analysis data were provided for the analysis of hydraulic flow units (HFU) (Amaefule et al. 1993). Equations (3) and (4), respectively, were used to calculate RQI and FZI values. We plotted RQI as a function of NPI in Fig. 8 to characterize the flow properties, while three hydraulic flow units (HFU) are demarcated based on the FZI thresholds. The studied Upper Cretaceous samples are assigned to 0.09 μm < FZI < 3.39 μm. Generally, rock pore systems containing clays in the form of filling, lining, and bridging as well as poorly sorted, fine-grained sands tend to display higher surface area and lower FZI values, whereas coarse-grained, well-sorted, and clean sands show lower surface areas and higher FZI values. A cross-plot between RQI and FZI provides a better understanding of the formation evaluation. Figure 9 displays that 0.02 μm < RQI ≤ 0.78 μm and refers to impervious to fair reservoir quality. We empirically derived the pore throat radius (R35) as a function of core-porosity and permeability using the Kolodzie model (1980). Estimated (R35) ranges from 0.10 to 7.40 μm and is plotted against RQI and FZI (Fig. 10 A and B). The Upper Cretaceous sandstone sample reservoir is comprised of meso-microporosity (0.10 μm < R35 ≤ 2 μm) and macro-porosity (2μm < R35 ≤10 μm). Based on core-based reservoir characterization, we summarize that the macro-porosity of the Upper Cretaceous sandstone have the fair reservoir quality and hydraulic flow units (0.09 μm < FZI ≤ 3.39 μm); RQI < (1 μm).
Formation factor-porosity
The cross plot between the log values of the formation factor and porosity is shown (Fig. 11). The data points follow the expected trend with a decrease of formation factor with increasing porosity. The fitting equation is
where F is the formation factor, with a cementation factor m = 1.85 results in a high coefficient of determination (R2 = 0.70).
Permeability-formation factor
The relation between permeability and formation factor is displayed (Fig. 12). Large formation factor values indicate lower porosity samples. The relationship is characterized by the determination coefficient R2 = 0.68 which is considerably higher than that of Eq. (9) and controlled by the following equation:
Permeability-internal surface (Spor)
The specific internal surface (Spor) and pore radius are related according to Eq. (5) and also controls permeability beside the porosity. Figure 13 shows the correlation between the permeability and internal surface, where coefficient of determination R2 = 0.73 and the fitting equation reads:
Longitudinal and transversal relaxation time comparison
As shown in Figs. 14 and 15, samples of higher porosity and permeability have longer relaxation times, and a very close linear relationship is observed between the T1 and T2(100) mean relaxation times with a determination coefficient R2=0.96 and controlled by the following equation:
T 2(100) is the NMR transversal relaxation time at 100 s.
On the other hand, a nearly linear relationship is observed between the T1 and T2(600) mean relaxation times with a coefficient of determination R2=0.95 and controlled by the following equation:
T 2(600) is the NMR transversal relaxation time at 600 s.
Assuming that the pore size distribution estimation based on the two mean relaxation times in the investigated sandstones in a similar way is valid, the T1/T2(100) ratio is slightly higher for samples T2(100)/T1= 0.58 in comparison with T2(600)/T1= 0.47. The observed differences in the ratio T1/T2 can be caused by the ferromagnetic contribution of the Fe-chlorite that causes faster decay of transversal relaxation and stronger inhomogeneity in the magnetic field (Abuseda et al. 2016) which agrees with the observations in Keating and Knight (2007) performed on iron oxide-coated sands.
Petrophysical model for permeability prediction
A petrophysical model is usually made to predict a necessary reservoir parameter that is hard to measure. The model should be created to conclude this parameter from an easily measurable other physical parameters. Many theoretical models are applied for estimating the permeability using other petrophysical reservoir parameters.
Permeability prediction
We compared the permeability prediction models used for the Upper Cretaceous sandstone samples to evaluate the model predictive power, and also the root means square (rms) deviation between the measured permeability (k) and predicted permeability (k*) is determined:
where n is the number of samples.
The average deviation between calculated and measured permeability is given by
A value of d = 1 indicates an average absolute deviation of one order of magnitude, in other words, a factor of 10.
Permeability prediction using spectral induced polarization
Figure 12 shows the strong relation between permeability and formation factor, where the equation that determines the predicted permeability is as follows:
where a and b values are resulted from the relation itself. The predictive quality of equation (20) with b= −5.62 resulting in rms = 0.746 and d =0.626. Figure 16 shows good agreement between the measured and predicted permeability for the majority of samples. Table 1 shows the resulting factors (a and R2) and the values of rms and d.
The previous research used the parameters derived from spectral induced polarization (SIP) as inputs in different permeability prediction models (e.g., Börner et al. 1996; Weller et al. 2010a). A general model is used here to integrate the formation factor and conductivity imaginary part (σ″) measured at 1 Hz frequency for the fully saturated samples with a 100 mS/m fluid conductivity. Equation (21) was used to predict permeability:
where multiple regression has been used to determine a, b, and c. Equation (22) considers the conductivity imaginary part
where k* is in mD and σ" in mS/m. Figure 17 shows a good agreement between the measured and predicted permeability in most samples, while Table 1 summarizes the factors and rms and d values. The deviation between the measured and predicted permeability is shown with the two dashed lines to both sides of the diagonal. Only one sample shows deviation more than one order of magnitude. The prediction quality will slightly improve by integrating the conductivity imaginary part.
Permeability prediction using specific internal surface (Spor)
Figure 13 shows excellent correlation between permeability and Spor; the following equation predicts the permeability using Spor:
The relation between internal surface (Spor) and permeability is used to determine the factor a and the exponents b, with prediction quality calculated using Eq. (23) of b= −1.76 resulting in rms = 0.688 and d =0.539. Figure 18 shows a good agreement between the measured and predicted permeability for the majority of samples, and Table 1 summarizes the factors and rms and d values.
Replacing the porosity with the specific internal surface (Spor) will improve the permeability prediction for our set samples. Equation 15 is a considerably higher coefficient of determination than Eqs. 9 and 14, and multiple regression is used to determine the exponents of the power law. The equation of permeability prediction using the internal surface and formation factor (F) reads is as follow:
with Spor in 1/μm., k* in mD, and F as unitless. Figure 19 shows that the rms and d confirms the excellent predictive quality for specific internal surface (Spor) based on the measured permeability and the predicted permeability using Eq. (24). The factors and the rms and d values are in Table 1.
Permeability prediction from NMR
The Kenyon empirical equation (Kenyon 1997) is commonly used for permeability estimation using the porosity and mean relaxation time
The factors a1,2 depend on the corresponding relaxation times of T1 or T2. The exponent of 2 for the relaxation time is based on the proportionality consideration between the pore radius r and relaxation time in Eq. (7). The porosity exponent was previously determined in empirical studies (Coates et al. 1999; Dunn et al. 2002). Equation (25) is used for predicting the permeability by inputting the porosity, mean longitudinal relaxation time T1, and the mean transversal relaxation time T2. The factors a1 and a2 were determined by minimizing the root mean square (rms) and average deviation (d) between the measured and predicted permeability, as shown in Figs. 20, 21, and 22, and also by replacing the porosity with the formation factor. The resulting equation will be as follows:
with T1 and T2 in sec. and k* in mD and F as unitless. Figures 23 and 24 show excellent prediction quality between the measured permeability and the permeability prediction using Eqs. (26) and (27), respectively, and the values of rms and d are summarized in Table 1.
Summary
An investigation has been done for the relations between different petrophysical parameters of the Upper Cretaceous Bahariya Formation. The high values of porosity and the permeability occur mainly in quartz arenite which characterized by coarse to medium grains with the absence of detrital materials, while the low values of porosity and the permeability occur in quartz wackes which are fine grains, silty sizes, and clays. Significant correlations between a variety of parameters to porosity and/or permeability have been proven. Permeability prediction based on porosity is not as accurate as using the formation factor because of the large scattering in the relevant cross plot. Also considering the superiority of the formation factor in ability of describing the connected pore space effectively, a better understanding of the formation evaluation was provided by the cross-plot between RQI and FZI; it typically has 0.02 μm < RQI ≤ 0.78 μm indicating impervious to fair reservoir quality. Estimated (R35) range is (0.10–7.40 μm). The Upper Cretaceous sandstone reservoir is comprised of meso-microporosity (0.10 μm < R35 ≤ 2 μm) and macro-porosity (2 μm < R35 ≤ 10 μm). Based on core-based reservoir characterization, the macro-porosity of the Upper Cretaceous sandstone have the fair reservoir quality and hydraulic flow units (0.09 μm < FZI ≤ 3.39 μm); RQI < (1 μm). The cross-plot between the log values of porosity and formation factor is an expected trend, i.e., decreasing formation factor with increasing porosity, and gives a cementation factor m = 1.85 which results in a high coefficient of determination (R2 = 0.70). Our study confirms the importance of the formation factor in predicting the permeability of Upper Cretaceous sandstone samples. The conductivity imaginary part is proved to be with less importance. The specific internal surface has more importance for permeability prediction than the porosity and formation factor. The NMR relaxation times and porosity models have been proven to be more adequate and accurate for permeability prediction. Replacing the porosity with the formation improves the permeability prediction. Multiple regression should be used to determine the exponents of the power law equation, and a slightly better permeability prediction is achieved by using the transversal relaxation time T2(600).
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Abuseda, H.H., El Sayed, A.M.A.A. & Elnaggar, O.M. Permeability modeling of Upper Cretaceous Bahariya Formation rocks, Abu Sennan field, Western Desert, Egypt. Arab J Geosci 16, 211 (2023). https://doi.org/10.1007/s12517-023-11218-2
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DOI: https://doi.org/10.1007/s12517-023-11218-2