Skip to main content
Log in

Dyeing of Wool Yarn with Aqueous Extract of Opuntia ficus-indica Fruit Containing Betalain Colorant Employing Ascorbic Acid as a Bio-mordant Under Varied Circumstances of Dyeing

  • Regular Article
  • Published:
Fibers and Polymers Aims and scope Submit manuscript

Abstract

Opuntia ficus-indica well adapts to extreme climate conditions and grows rapidly in low water and poor soil requirement. In this study, the Opuntia ficus-indica fruit was used for natural dyeing of wool yarn. The Opuntia ficus-indica fruit has a reddish-purple color, due to the presence of water-soluble betalain colorants. When using this fruit as a natural dye, it is possible to obtain various color shades, because its color changes depending on the dyeing conditions. However, it is difficult to control the dyeing environment to reproduce the original color of Opuntia ficus-indica fruits. The aim of this study is to examine the effect of various dyeing conditions on the color strength, and color shades of Opuntia ficus-indica fruit. Ascorbic acid as a bio-mordant was applied for enhancing the stability of the betalain colorants. For this purpose, the betalain dye was extracted from Opuntia ficus-indica fruit by an aqueous extraction and used for dyeing wool samples in the presence of ascorbic acid at different dyeing process conditions. The dyed wool samples presented a red, pale red, orange, pale brown, and brown color by varying the applied pH (3, 5.5, and 8) of the dye bath, and dyeing temperature (40, 65, and 90 °C). Applying ascorbic acid as an antioxidant enhanced the color strength (~ 110%), thermal stability (~ 22%), and color fastness values. In addition, the presence of ascorbic acid did not have any significant effect on the tensile properties of the dyed wool yarns.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8

Similar content being viewed by others

Data Availability

All data generated or analyzed during this study are included in this published article.

References

  1. C.-W. Kan, C.K.Y. Lo, W.S. Man, Color. Technol. 132, 4 (2016)

    Article  CAS  Google Scholar 

  2. L. Lara, I. Cabral, J. Cunha, Sustainability 14, 8353 (2022)

    Article  CAS  Google Scholar 

  3. P. Chowdhary, R.N. Bharagava, S. Mishra, N. Khan, in Environmental Concerns and Sustainable Development, 1st edn., ed. by V. Shukla, N. Kumar, vol. 1 (Springer Singapore, Singapore, 2020), pp. 235–256

  4. M. Yusuf, M. Shabbir, F. Mohammad, Nat. Prod. Bioprospect. 7, 123 (2017)

    Article  CAS  PubMed  PubMed Central  Google Scholar 

  5. P. Brudzyńska, A. Sionkowska, M. Grisel, Materials 14(13), 3484 (2021)

    Article  PubMed  PubMed Central  Google Scholar 

  6. L.D. Ardila-Leal, R.A. Poutou-Piñales, A.M. Pedroza-Rodríguez, B.E. Quevedo-Hidalgo, Molecules 26(13), 3813 (2021)

    Article  CAS  PubMed  PubMed Central  Google Scholar 

  7. M. Shahid, S.-U. Islam, F. Mohammad, J. Cleaner Prod. 53, 310 (2013)

    Article  CAS  Google Scholar 

  8. C.E. Russell, P. Felker, Econ. Bot. 41, 433 (1987)

    Article  Google Scholar 

  9. M. Aragona, E.R. Lauriano, S. Pergolizzi, C. Faggio, Nat. Prod. Res. 32, 2037 (2018)

    Article  CAS  PubMed  Google Scholar 

  10. E.M. Yahia, C. Sáenz, in Postharvest Biology and Technology of Tropical and Subtropical Fruits, 1st edn., ed. by E.M. Yahia, vol. 2, (Woodhead Publishing Limited, Cambridge, 2011), pp. 290–331

  11. J.H. Cota-Sánchez, in Nutritional Composition of Fruit Cultivars, 1st edn., ed. by M.S.J. Simmonds, V.R. Preedy (Elsevier, Amsterdam, 2016), pp. 691–712

  12. W.S. Choo, in Bioactive Molecules in Food-Reference Series in Phytochemistry, 1st edn., ed. by J.M. Mérillon, K. Ramawat (Springer International Publishing, Cham, 2018), pp. 1–28

  13. P. Ganesan, T. Karthik, J. Text. Inst. 108, 1173 (2017)

    Article  CAS  Google Scholar 

  14. A. Guesmi, N. Ben Hamadi, N. Ladhari, F. Sakli, Ind. Crops Prod. 37, 493 (2012)

    Article  CAS  Google Scholar 

  15. N.F. Ali, R.S.R. El-Mohamedy, J. Saudi Chem. Soc. 15(3), 257 (2011)

    Article  CAS  Google Scholar 

  16. A. Guesmi, N. Ben Hamadi, N. Ladhari, F. Sakli, Ind. Crops Prod. 42, 63 (2013)

    Article  CAS  Google Scholar 

  17. K.M. Herbach, F.C. Stintzing, R. Carle, J. Food Sci. 71(4), R41 (2006)

    Article  CAS  Google Scholar 

  18. A. Guesmi, N. Ladhari, N. Ben Hamadi, M. Msaddek, F. Sakli, J. Clean. Prod. 39, 97 (2013)

    Article  CAS  Google Scholar 

  19. M.M. Giusti, R.E. Wrolstad, in Current Protocols in Food Analytical Chemistry, ed. by M.M. Giusti, R.E. Wrolstad (John Wiley and Sons, Inc., Hoboken, 2001), pp. F1.2.1.–F1.2.13

  20. T. Fuleki, F.J. Francis, J. Food Sci. 33, 72 (1968)

    Article  CAS  Google Scholar 

  21. H.M.C. Azeredo, Int. J. Food Sci. Technol. 44, 2365 (2009)

    Article  CAS  Google Scholar 

  22. R. Castellar, J.M. Obón, M. Alacid, J.A. Fernández-López, J. Agric. Food Chem. 51, 2772 (2003)

    Article  CAS  PubMed  Google Scholar 

  23. R. Reynoso, F.A. Garcia, D. Morales, E. Gonzalez De Mejia, J. Agric. Food Chem. 45, 2884 (1997)

    Article  CAS  Google Scholar 

  24. U. Merin, S. Gagel, G. Popel, S. Bernstein, I. Rosenthal, J. Food Sci. 52, 485 (1987)

    Article  CAS  Google Scholar 

  25. J.M. Obon, M.R. Castellar, M. Alacid, J.A. Fernández-López, J. Biotechnol. 131, S139 (2007)

    Article  Google Scholar 

  26. C. Albano, C. Negro, N. Tommasi, C. Gerardi, G. Mita, A. Miceli, L. de Bellis, F. Blando, Antioxidants 4, 269 (2015)

    Article  CAS  PubMed  PubMed Central  Google Scholar 

  27. D. Butera, L. Tesoriere, F. Di Gaudio, A. Bongiorno, M. Allegra, A.M. Pintaudi, R. Kohen, M.A. Livrea, J. Agric. Food Chem. 50, 6895 (2002)

    Article  CAS  PubMed  Google Scholar 

  28. J.A. Fernández-López, L. Almela, J.M. Obón, R. Castellar, Plant Foods Hum. Nutr. 65, 253 (2010)

    Article  PubMed  Google Scholar 

  29. M.G. Miguel, Antioxidants 7(4), 53 (2018)

    Article  PubMed  PubMed Central  Google Scholar 

  30. E. Akbar Hussain, Z. Sadiq, M. Zia-Ul-Haq, in Betalains: Biomolecular Aspects, 1st edn. (Springer International Publishing, Cham, 2018), pp. 125–137

  31. E. Akbar Hussain, Z. Sadiq, M. Zia-Ul-Haq, in Betalains: Biomolecular Aspects, 1st edn. (Springer International Publishing, Cham, 2018), pp. 33–55

  32. F. Delgado-Vargas, A.R. Jiménez, O. Paredes-López, Crit. Rev. Food Sci. Nutr. 40, 173 (2000)

    Article  CAS  PubMed  Google Scholar 

  33. H.E. Gharras, Nat. Prod. Commun. 6, 1425 (2011)

    PubMed  Google Scholar 

  34. D. Cristea, G. Vilarem, Dyes Pigm. 70, 238 (2006)

    Article  CAS  Google Scholar 

  35. C.H. Giles, J. Appl. Chem. 15, 541 (1965)

    Article  CAS  Google Scholar 

  36. D. Gupta, Colourage 46(7), 35 (1999)

    CAS  Google Scholar 

  37. F.A. Faiz, J.S.K. Ngo, K.B. Bujang, Res. J. Text. Apparel 20, 74 (2016)

    Article  Google Scholar 

Download references

Acknowledgements

The authors would like to thank the support of the Department of Carpet, Faculty of Art, University of Birjand. Also, we appreciate and thank Mrs. Khaleghi, who helped during the implementation of this project in the Dyeing and Fiber Science lab, Department of Carpet, Faculty of Art, University of Birjand.

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Hossein Barani.

Ethics declarations

Conflict of Interest

The authors declare no conflict of interest.

Supplementary Information

Below is the link to the electronic supplementary material.

Supplementary file1 (DOCX 17 KB)

Rights and permissions

Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Barani, H., Rahmani, F. Dyeing of Wool Yarn with Aqueous Extract of Opuntia ficus-indica Fruit Containing Betalain Colorant Employing Ascorbic Acid as a Bio-mordant Under Varied Circumstances of Dyeing. Fibers Polym 24, 2785–2797 (2023). https://doi.org/10.1007/s12221-023-00274-w

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s12221-023-00274-w

Keywords

Navigation