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Preparation of gold decorated MoS2/NiO nanocomposite in the production of a new electrochemical sensor for ascorbic acid detection

  • Materials (Organic, Inorganic, Electronic, Thin Films)
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Korean Journal of Chemical Engineering Aims and scope Submit manuscript

Abstract

We investigated electrochemical sensing of ascorbic acid by Au-MoS2/NiO modified glassy carbon electrode. The MoS2, NiO, MoS2/NiO were prepared by hydrothermal, and Au-MoS2/NiO was prepared chemical reduction method. The characterization of Au-MoS2/NiO composite was carried out using X-ray diffraction, Fourier transform infrared spectroscopy, X-ray photoelectron spectroscopy and field emission scanning electron microscopy. The electrochemical characteristics of the Au-MoS2/NiO composite were examined by cyclic voltammetry and electrochemical impedance spectroscopy. Then, differential pulse voltammetry responses of Au-MoS2/NiO modified glassy carbon electrode were detected towards the ascorbic acid in phosphate buffer (0.1 M, pH=7). The ascorbic acid sensor represented low detection limit of 0.13 µM with linear range of 2–50 µM, revealing that this sensor gave satisfactory responses. The practical feasibility of the obtained sensor was assessed for the detection of ascorbic acid in Vitamin C tablet. We believe that this study could help different studies for producing commercially ascorbic acid sensors.

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Acknowledgements

We wish to thank the Scientific Research Projects Commission of Sakarya University (Project number: 2020-9-33-95) for the financial support of this study. M.O is grateful for Turkish Academy of Sciences (TUBA) for partial support.

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Authors and Affiliations

  1. Biomedical, Magnetic and Semiconductor Materials Application and Research Center (BIMAS-RC), Sakarya University, 54187, Sakarya, Turkey

    Keziban Atacan

  2. Akyazi Vocational School of Health Services, Sakarya University of Applied Sciences, 54400, Sakarya, Turkey

    Keziban Atacan

  3. Biomaterials, Energy, Photocatalysis, Enzyme Technology, Nano & Advanced Materials, Additive Manufacturing, Environmental Applications and Sustainability Research & Development Group (BIOENAMS R & D Group), Sakarya University, 54187, Sakarya, Turkey

    Keziban Atacan, Nuray Güy & Mahmut Özacar

  4. Science & Arts Faculty, Department of Chemistry, Sakarya University, 54187, Sakarya, Turkey

    Nuray Güy & Mahmut Özacar

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  1. Keziban Atacan
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Correspondence to Keziban Atacan.

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11814_2021_1039_MOESM1_ESM.pdf

Preparation of gold decorated MoS2/NiO nanocomposite in the production of a new electrochemical sensor for ascorbic acid detection

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Atacan, K., Güy, N. & Özacar, M. Preparation of gold decorated MoS2/NiO nanocomposite in the production of a new electrochemical sensor for ascorbic acid detection. Korean J. Chem. Eng. 39, 2172–2181 (2022). https://doi.org/10.1007/s11814-021-1039-2

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  • DOI: https://doi.org/10.1007/s11814-021-1039-2

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