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A novel hydrothermal releasing synthesis of modified SiO2 material and its application in phenol removal process

  • Environmental Engineering
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Abstract

A modified SiO2 material (MSM) was successfully synthesized by using Na2SiO3 and a novel CO2SM in the presence of CTAB through an innovative hydrothermal releasing treatment protocol. The MSM was systemically characterized using several techniques, including N2 adsorption-desorption isotherm, thermogravimetric analysis (TGA), Fourier transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and X-ray diffraction (XRD). The CO2SM as a platform for CO2 capturing and releasing can be reversibly used for multiple cycles without significant loss of capabilities. The optimum conditions for the preparation of MSM were identified as follows: Na2SiO3 concentration, 0.2mol/L; hydrothermal temperature, 120 °C; CO2SM dosage, 6 g; CTAB concentration, 24 g/L, reaction time, 12 h. Additionally, the MSM exhibited high efficiency for the removal of phenol from aqueous solution: it showed a phenol adsorption capacity of 91.29mg/g when shaken with the aqueous phenol solution at 180 rpm for 1 h at 25 °C.

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  1. College of Chemical Engineering, Inner Mongolia University of Technology, Hohhot, 010051, China

    Xinyu Yang, Xiaoyao Liu, Wenjing Tang, Yajun Gao, Huijuan Ni & Jianbin Zhang

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  1. Xinyu Yang
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  2. Xiaoyao Liu
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Yang, X., Liu, X., Tang, W. et al. A novel hydrothermal releasing synthesis of modified SiO2 material and its application in phenol removal process. Korean J. Chem. Eng. 34, 723–733 (2017). https://doi.org/10.1007/s11814-016-0311-3

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