Skip to main content

Advertisement

Log in

Heat Treatment Effects on the Microstructure, Mechanical and Wear Properties of an Al 2024 Cold Spray Additive Manufactured Deposit

  • ORIGINAL RESEARCH ARTICLE
  • Published:
Journal of Thermal Spray Technology Aims and scope Submit manuscript

Abstract

The impact of high-speed micron-sized metallic particles during cold spray additive manufacturing (CSAM) often leads to non-uniform plastic deformation, resulting in work hardening effects that can cause brittleness, poor mechanical properties, and anisotropy in the deposits. This study aimed to characterize the wear, mechanical properties, and mechanical anisotropy of 2024 aluminum alloy deposits and investigate the effects of heat treatments (annealing, solution, aging treatment) on improving these properties. The results revealed that the mechanical property anisotropy of the As-sprayed deposits was not significant. Specifically, the tensile strength of the As-sprayed deposits measured at angles of 0º, 45º, and 90º from the spraying direction are 58 MPa, 52 MPa, and 41 MPa, respectively. Annealing was found to decrease wear resistance and hardness but had a positive impact on mechanical properties. Solution and aging treatment proved to be effective in improving wear resistance. For the solution-treated deposits, the measured tensile strength and elongation at angles of 0º, 45º, and 90º from the spraying direction are 108 MPa, 114 MPa, and 101 MPa, and 6.5%, 5.8%, and 4.8%, respectively. It is worth noting that heat treatment improves the bonding quality, however, the presence of pores generates during the heat treatment limits further improvements in mechanical properties. Overall, this study highlights the importance of heat treatments in enhancing the mechanical properties, wear resistance, and mechanical anisotropy of 2024 aluminum alloy deposits produces through CSAM.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10
Fig. 11
Fig. 12
Fig. 13
Fig. 14

Similar content being viewed by others

References

  1. D.D. Gu, W. Meiners, K. Wissenbach, and R. Poprawe, Laser Additive Manufacturing of Metallic Components: Materials, Processes and Mechanisms, Int. Mater. Rev., 2012, 57, p 133-164.

    Article  CAS  Google Scholar 

  2. S. Yin, N.S. Fan, C.J. Huang, Y.C. Xie, C. Zhang, R. Lupoi, and W.Y. Li, Towards High-Strength Cold Spray Additive Manufactured Metals: Methods, Mechanisms, and Properties, J. Mater. Sci. Technol., 2024, 170, p 47-64.

    Article  Google Scholar 

  3. E. Louvis, P. Fox, and C.J. Sutcliffe, Selective Laser Melting of Aluminium Components, J. Mater. Process. Tech., 2011, 211, p 275-284.

    Article  CAS  Google Scholar 

  4. W.Y. Li and C.J. Li, Optimal Design of a Novel Cold Spray Gun Nozzle at a Limited Space, J. Therm. Spray Technol., 2005, 14, p 391-396.

    Article  CAS  Google Scholar 

  5. W.Y. Li, H.L. Liao, G. Douchy, and C. Coddet, Optimal Design of a Cold Spray Nozzle by Numerical Analysis of Particle Velocity and Experimental Validation with 316L Stainless Steel Powder, Mater. Des., 2007, 28, p 2129-2137.

    Article  CAS  Google Scholar 

  6. C.J. Huang, A. List, L. Wiehler, M. Schulze, F. Gärtner, and T. Klassen, Cold Spray Deposition of Graded Al-SiC Composites, Addit. Manuf., 2022, 59, p 103116.

    CAS  Google Scholar 

  7. S. Yin, P. Cavaliere, B. Aldwell, R. Jenkins, H. Liao, W.Y. Li, and R. Lupoi, Cold Spray Additive Manufacturing and Repair: Fundamentals and applications, Addit. Manuf., 2018, 21, p 628-650.

    CAS  Google Scholar 

  8. W.Y. Li, C.C. Cao, and S. Yin, Solid-State Cold Spraying of Ti and Its Alloys: A Literature Review, Prog. Mater. Sci., 2020, 110, p 100633.

    Article  CAS  Google Scholar 

  9. X.T. Luo, C.X. Li, F.L. Shang, G.J. Yang, Y.Y. Wang, and C.J. Li, High Velocity Impact Induced Microstructure Evolution During Deposition of Cold Spray Coatings: A Review, Surf. Coat. Tech., 2014, 254, p 11-20.

    Article  CAS  Google Scholar 

  10. S. Yin, M. Hassani, Q. Xie, and R. Lupoi, Unravelling the Deposition Mechanism of Brittle Particles in Metal Matrix Composites Fabricated Via Cold Spray Additive Manufacturing, Scr. Mater., 2021, 194, p 113614.

    Article  CAS  Google Scholar 

  11. H. Assadi, H. Kreye, F. Gaertner, and T. Klassen, Cold Spraying—A Materials Perspective, Acta Mater., 2016, 116, p 382-407.

    Article  CAS  Google Scholar 

  12. S. Bagherifard, A.H. Astaraee, M. Locati, A. Nawaz, S. Monti, J. Kondas, R. Singh, and M. Guagliano, Design and Analysis of Additive Manufactured Bimodal Structures Obtained by Cold Spray Deposition, Addit. Manuf., 2020, 33, p 101131.

    CAS  Google Scholar 

  13. C.J. Huang, M. Arseenko, L. Zhao, Y.C. Xie, A. Elsenberg, W.Y. Li, F. Gartner, A. Simar, and T. Klassen, Property Prediction and Crack Growth Behavior in Cold Sprayed Cu Deposits, Mater. Des., 2021, 206, p 109826.

    Article  CAS  Google Scholar 

  14. C.J. Huang, A. List, J.J. Shen, B.L. Fu, S. Yin, T. Chen, B. Klusemann, F. Gartner, and T. Klassen, Tailoring Powder Strengths for Enhanced Quality of Cold Sprayed Al6061 Deposits, Mater. Des., 2022, 215, p 110494.

    Article  CAS  Google Scholar 

  15. K.X. Chen, J.W. Zhang, Y.J. Chen, X.H. Chen, Z.D. Wang, and R. Sandstrom, Slow Strain Rate Tensile Tests on Notched Specimens of as-Cast Pure Cu and Cu-Fe-Co Alloys, J. Alloys Compd., 2020, 822, p 153647.

    Article  CAS  Google Scholar 

  16. R.Z. Huang, M. Sone, W.H. Ma, and H. Fukanuma, The Effects of Heat Treatment on the Mechanical Properties of Cold-Sprayed Coatings, Surf. Coat. Technol., 2015, 261, p 278-288.

    Article  CAS  Google Scholar 

  17. L.S. Tang, W.B. Xie, X.P. Xiao, H.M. Chen, H. Wang, and B. Yang, Evolution of Microstructure and Properties of Cu-4.5 wt.% Ag Alloy Prepared by Vacuum Horizontal Continuous Casting in Solid Solution and Aging Treatment, Mater. Res. Express, 2020, 7, p 126517.

    Article  CAS  Google Scholar 

  18. P. Coddet, C. Verdy, C. Coddet, and F. Debray, Effect of Cold Work, Second Phase Precipitation and Heat Treatments on the Mechanical Properties of Copper–Silver Alloys Manufactured By Cold Spray, Mater. Sci. Eng. A, 2015, 637, p 40-47.

    Article  CAS  Google Scholar 

  19. J. Zhang, L.F. Ma, G.H. Zhao, Z.H. Cai, and C.C. Zhi, Effect of Annealing Temperature on Tensile Fracture Behavior of AZ31/6061 Explosive Composite Plate, J. Mater. Res. Technol., 2022, 19, p 4325-4336.

    Article  CAS  Google Scholar 

  20. M.R. Rokni, C.A. Widener, O.C. Ozdemir, and G.A. Crawford, Microstructure and Mechanical Properties of Cold Sprayed 6061 Al in As-Sprayed and Heat Treated Condition, Surf. Coat. Technol., 2017, 309, p 641-650.

    Article  CAS  Google Scholar 

  21. M.S.H. Al-Furjan, M.H. Hajmohammad, X. Shen, D.K. Rajak, and R. Kolahchi, Evaluation of Tensile Strength and Elastic Modulus of 7075–T6 Aluminum Alloy by Adding SiC Reinforcing Particles Using Vortex Casting Method, J. Alloys Compd., 2021, 886, p 161261.

    Article  CAS  Google Scholar 

  22. M.R. Rokni, C.A. Widener, V.K. Champagne, G.A. Crawford, and S.R. Nutt, The Effects of Heat Treatment on 7075 Al Cold Spray Deposits, Surf. Coat. Technol., 2017, 310, p 278-285.

    Article  CAS  Google Scholar 

  23. K. Petrackova, J. Kondas, and M. Guagliano, Mechanical Performance of Cold-Sprayed A357 Aluminum Alloy Coatings for Repair and Additive Manufacturing, J. Therm. Spray Technol., 2017, 26, p 1888-1897.

    Article  CAS  Google Scholar 

  24. X. Qiu, J.Q. Wang, N.U. Tariq, L. Gyansah, J.X. Zhang, and T.Y. Xiong, Effect of Heat Treatment on Microstructure and Mechanical Properties of A380 Aluminum Alloy Deposited by Cold Spray, J. Therm. Spray Technol., 2017, 26, p 1898-1907.

    Article  CAS  Google Scholar 

  25. K. Yang, W.Y. Li, X. Yang, and Y. Xu, Anisotropic Response of Cold Sprayed Copper Deposits, Surf. Coat. Technol., 2018, 335, p 219-227.

    Article  CAS  Google Scholar 

  26. H. Seiner, J. Cizek, P. Sedlak, R.Z. Huang, J. Cupera, I. Dlouhy, and M. Landa, Elastic Moduli and Elastic Anisotropy of Cold Sprayed Metallic Coatings, Surf. Coat. Technol., 2016, 291, p 342-347.

    Article  CAS  Google Scholar 

  27. P. Coddet, C. Verdy, C. Coddet, and F. Debray, On the Mechanical and Electrical Properties of Copper–Silver and Copper–Silver–Zirconium Alloys Deposits Manufactured By Cold Spray, Mater. Sci. Eng. A, 2016, 662, p 72-79.

    Article  CAS  Google Scholar 

  28. S. Yin, J. Cizek, X. Yan, and R. Lupoi, Annealing Strategies for Enhancing Mechanical Properties of Additively Manufactured 316L Stainless Steel Deposited by Cold Spray, Surf. Coat. Technol., 2019, 370, p 353-361.

    Article  CAS  Google Scholar 

  29. C. Genevois, D. Fabregue, A. Deschamps, and W.J. Poole, On the Coupling Between Precipitation and Plastic Deformation in Relation with Friction Stir Welding of AA2024 T3 Aluminium Alloy, Mater. Sci. Eng. A, 2006, 441, p 39-48.

    Article  Google Scholar 

  30. K. Yang, W. Li, X. Yang, Y. Xu, and A. Vairis, Effect of Heat Treatment on the inherent Anisotropy of Cold Sprayed Copper Deposits, Surf. Coat. Technol., 2018, 350, p 519-530.

    Article  CAS  Google Scholar 

  31. Z. Zhang, F. Liu, E.-H. Han, and L. Xu, Mechanical and Corrosion Properties in 3.5% NaCl Solution of Cold Sprayed Al-Based Coatings, Surf. Coat. Technol., 2020, 385, p 125372.

    Article  CAS  Google Scholar 

  32. B.L. Zheng, Y.J. Lin, Y.Z. Zhou, and E.J. Lavernia, Gas Atomization of Amorphous Aluminum: Part I. Thermal Behavior Calculations, Metall. Mater. Trans. B-Proc. Metall. Mater. Proc. Sci., 2009, 40, p 768-778.

    Article  Google Scholar 

  33. W.Y. Li, D. Wu, K.W. Hu, Y.X. Xu, X.W. Yang, and Y. Zhang, A Comparative Study on the Employment of Heat Treatment, Electric Pulse Processing and Friction Stir Processing to Enhance Mechanical Properties of Cold-Spray-Additive-Manufactured Copper, Surf. Coat. Technol., 2021, 409, p 126887.

    Article  CAS  Google Scholar 

  34. B. Almangour, P. Vo, R. Mongrain, E. Irissou, and S. Yue, Effect of Heat Treatment on the Microstructure and Mechanical Properties of Stainless Steel 316L Coatings Produced by Cold Spray for Biomedical Applications, J. Therm. Spray Technol., 2014, 23, p 641-652.

    Article  CAS  Google Scholar 

  35. D. Wu, W.Y. Li, Y.J. Gao, J. Yang, Y. Su, Q. Wen, and A. Vairis, Effect of an Improved Pin Design on Weld Formability and Mechanical Properties of Adjustable-Gap Bobbin-Tool Friction Stir Welded Al-Cu Aluminum Alloy Joints, J. Manuf. Process., 2020, 58, p 1182-1188.

    Article  Google Scholar 

  36. H. Assadi, H. Kreye, F. Gärtner, and T. Klassen, Cold Spraying—A Materials Perspective, Acta Mater., 2016, 116, p 382-407.

    Article  CAS  Google Scholar 

  37. W. Pantleon, Resolving the Geometrically Necessary Dislocation Content by Conventional Electron Backscattering Diffraction, Scr. Mater., 2008, 58, p 994-997.

    Article  CAS  Google Scholar 

  38. R. Kapoor, N. Kumar, R.S. Mishra, C.S. Huskamp, and K.K. Sankaran, Influence of Fraction of High Angle Boundaries on the Mechanical Behavior of an Ultrafine Grained Al-Mg Alloy, Mater. Sci. Eng. A, 2010, 527, p 5246-5254.

    Article  Google Scholar 

  39. I.N.A. Oguocha and S. Yannacopoulos, Precipitation and Dissolution Kinetics in Al-Cu-Mg-Fe-Ni Alloy 2618 and Al-Alumina Particle Metal Matrix Composite, Mater. Sci. Eng. A, 1997, 231, p 25-33.

    Article  Google Scholar 

  40. P. Sirvent, M.A. Garrido, C.J. Múnez, P. Poza, and S. Vezzù, Effect of Higher Deposition Temperatures on the Microstructure and Mechanical Properties of Al 2024 Cold Sprayed Coatings, Surf. Coat. Technol., 2018, 337(2018), p 461-470.

    Article  CAS  Google Scholar 

  41. K. Yang, W. Li, X. Guo, X. Yang, and Y. Xu, Characterizations and Anisotropy of Cold-Spraying Additive-Manufactured Copper Bulk, J. Mater. Sci. Technol., 2018, 34, p 1570-1579.

    Article  CAS  Google Scholar 

  42. E. Irissou, J.G. Legoux, B. Arsenault, and C. Moreau, Investigation of Al-Al2O3 Cold Spray Coating Formation and Properties, J. Therm. Spray Technol., 2007, 16, p 661-668.

    Article  CAS  Google Scholar 

  43. W.Y. Li, C.L. Yang, and H.L. Liao, Effect of Vacuum Heat Treatment on Microstructure and Microhardness of Cold-Sprayed TiN Particle-Reinforced Al Alloy-Based Composites, Mater. Des., 2011, 32, p 388-394.

    Article  CAS  Google Scholar 

  44. K. Spencer, D.M. Fabijanic, and M.X. Zhang, The Use of Al-Al2O3 Cold Spray Coatings to Improve the Surface Properties of Magnesium Alloys, Surf. Coat. Technol., 2009, 204, p 336-344.

    Article  CAS  Google Scholar 

  45. J.M. Shockley, S. Descartes, P. Vo, E. Irissou, and R.R. Chromik, The Influence of Al2O3 Particle Morphology on the Coating Formation and Dry Sliding Wear Behavior of Cold Sprayed Al-Al2O3 Composites, Surf. Coat. Technol., 2015, 270, p 324-333.

    Article  CAS  Google Scholar 

  46. S. Kumar, S.K. Reddy, and S.V. Joshi, Microstructure and Performance of Cold Sprayed Al-SiC Composite Coatings with High Fraction of Particulates, Surf. Coat. Technol., 2017, 318, p 62-71.

    Article  CAS  Google Scholar 

Download references

Acknowledgments

This work is supported by the National Natural Science Foundation of China (52061135101, 51875471), and the State Key Laboratory of Solidification Processing (NPU, China) (2021-TZ-01).

Author information

Authors and Affiliations

Authors

Corresponding authors

Correspondence to Wenya Li or Xiawei Yang.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Wu, D., Li, W., Yang, X. et al. Heat Treatment Effects on the Microstructure, Mechanical and Wear Properties of an Al 2024 Cold Spray Additive Manufactured Deposit. J Therm Spray Tech 32, 2378–2393 (2023). https://doi.org/10.1007/s11666-023-01668-1

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11666-023-01668-1

Keywords

Navigation