Skip to main content
Log in

Microstructural Stability and Mechanical Behavior of Pure Mg After One-Pass Equal Channel Angular Pressing Plus Intersection Annealing

  • Published:
Journal of Materials Engineering and Performance Aims and scope Submit manuscript

Abstract

A Fe-clad pure Mg bar was prepared by one-pass equal channel angular pressing at room temperature and was annealed subsequently at different time and temperatures. Microstructures, textures and compressive mechanical properties of the as-annealed samples were investigated. The results show that a large number of equiaxed grains appeared in the microstructure after different annealing treatment, manifesting that static recrystallization (SRX) took place during the annealing process. After intersection annealing at 200 °C × 30 min, microstructure is the most homogeneous and compressive properties are the best due to adequate SRX during annealing, indicating that a steady state has been achieved.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1.
Fig. 2.
Fig. 3.
Fig. 4.
Fig. 5.
Fig. 6.

Similar content being viewed by others

References

  1. S. Kamado and Y. Kojima, Development of Magnesium Alloys with High Performance, Mater. Sci. Forum, 2007, 546–549, p 55–64.

    Article  Google Scholar 

  2. B.L. Mordike and T. Ebert, Magnesium: Properties-Applications-Potential, Mater. Sci. Eng. A, 2001, 302, p 37–45.

    Article  Google Scholar 

  3. R.W.K. Honeycombe, The Plastic Deformation of Metals, Edward Arnold, London, 1968.

    Google Scholar 

  4. A. Muralidhar, S. Narendranath and H. ShivanandaNayaka, Effect of Equal Channel Angular Pressing on AZ31 Wrought Magnesium Alloys, J. Mag. Alloys, 2013, 1, p 336–342.

    Article  CAS  Google Scholar 

  5. X. Huang, K. Suzuki, A. Watazu, I. Shigematsu and N. Saito, Improvement of Formability of Mg-Al-Zn Alloy Sheet at Low Temperatures Using Differential Speed Rolling, J. Alloys Comp., 2009, 470, p 263–268.

    Article  CAS  Google Scholar 

  6. J.B. Lee, T.J. Konno and H.G. Jeong, Effect of Differential Speed Rolling on the Anisotropy of Mechanical Properties and Texture Evolution of AZ31 Mg Alloys, J. Alloys Comp., 2010, 499, p 273–277.

    Article  CAS  Google Scholar 

  7. Y. Huang, R.B. Figueiredo and T. Baudin, Evolution of Strength and Homogeneity in a Magnesium AZ31 Alloy Processed by High-Pressure Torsion at Different Temperatures, Adv. Eng. Mater., 2012, 14, p 1018–1026.

    Article  CAS  Google Scholar 

  8. W.J. Kim, S.I. Hong, Y.S. Kim, S.H. Min, H.T. Jeong and J.D. Lee, Texture Development and Its Effect on Mechanical Properties of an AZ61 Mg Alloy Fabricated by Equal Channel Angular Pressing, Acta Mater., 2003, 51, p 3293–3307.

    Article  CAS  Google Scholar 

  9. X.R. Yang, X.C. Zhao and W.J. Fu, Deformed Microstructures and Mechanical Properties of CP-Ti Processed by Multi-Pass ECAP at Room Temperature, Rare Metal. Mater. Eng., 2009, 38, p 0955–0957.

    Article  CAS  Google Scholar 

  10. S. Biswas, S. Singh Dhinwal and S. Suwas, Room-Temperature Equal Channel Angular Extrusion of Pure Magnesium, Acta Mater., 2010, 58, p 3247–3261.

    Article  CAS  Google Scholar 

  11. K. Xia, J.T. Wang, X. Wu, G. Chen and M. Gurvan, Equal Channel Angular Pressing of Magnesium Alloy AZ31, Mater. Sci. Eng., 2005, A410, p 324.

    Article  Google Scholar 

  12. W.W. Lei, W. Liang, H.X. Wang and H.W. Guo, Evolution of Texture and Mechanical Properties of pure Mg Processed by ECAP at Room Temperature, JOM, 2017, 69, p 2297–2301.

    Article  CAS  Google Scholar 

  13. S. Dash and N. Brown, An Investigation of the Origin and Growth of Annealing Twins, Acta Metall., 1963, 11(9), p 1067–1075.

    Article  CAS  Google Scholar 

  14. L. Jiang, J.J. Jonas and A.A. Luo, Twinning-Induced Softening in Polycrystalline AM30 Mg Alloy at Moderate Temperatures, Scr. Mater., 2006, 54(5), p 771–775.

    Article  CAS  Google Scholar 

  15. X. Li, P. Yang and L.N. Wang, Orientational Analysis of Static Recrystallization at Compression Twins in a Magnesium Alloy AZ31, Mater. Sci. Eng. A, 2009, 517(1), p 160–169.

    Article  Google Scholar 

  16. M.T. Pérez-Prado and O.A. Ruano, Texture Evolution During Annealing of Magnesium AZ31 Alloy, Scr. Mater., 2002, 46(2), p 149–155.

    Article  Google Scholar 

  17. M.T. Pérez-Prado and O.A. Ruano, Texture Evolution During Grain Growth in Annealed MG AZ61 Alloy, Scr. Mater., 2003, 48(1), p 59–64.

    Article  Google Scholar 

  18. G.D. Fan, M.Y. Zheng, X.S. Hu, C. Xu, K. Wu and I.S. Golovin, Effect of Heat Treatment on Internal Friction in ECAP Processed Commercial Pure Mg, J. Alloys Compd., 2013, 549, p 38–45.

    Article  CAS  Google Scholar 

  19. G.D. Fan, M.Y. Zheng, X.S. Hu, C. Xu, K. Wu and I.S. Golovin, Improved Mechanical Property and Internal Friction of Pure Mg Processed by ECAP, Mater. Sci. Eng. A, 2012, 556, p 588–594.

    Article  CAS  Google Scholar 

  20. M.R. Barnett, Z. Keshavarz, A.G. Beer and D. Atwell, Influence of Grain Size on the Compressive Deformation of Wrought Mg-3Al-1Zn, Acta Mater., 2004, 52, p 5093–5103.

    Article  CAS  Google Scholar 

  21. H.D. Fan, S. Aubry, A. Arsenlis and J.A. El-Awady, Orientation Influence on Grain Size Effects in Ultrafine-Grained Magnesium, Scr. Mater., 2016, 112, p 50–53.

    Article  CAS  Google Scholar 

Download references

Acknowledgments

This research was supported by the Doctoral Start-up Foundation of Shanxi Province (No. SD1926), the Scientific and Technologial Innovation Programs of Higher Education Institutions in Shanxi (No. 2020L0196) and the Shanxi Province Science Foundation for Youths (No. 201901D211342).

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Hui Zhang.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Lei, W., Liang, W. & Zhang, H. Microstructural Stability and Mechanical Behavior of Pure Mg After One-Pass Equal Channel Angular Pressing Plus Intersection Annealing. J. of Materi Eng and Perform 30, 2374–2380 (2021). https://doi.org/10.1007/s11665-021-05563-0

Download citation

  • Received:

  • Revised:

  • Accepted:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11665-021-05563-0

Keywords

Navigation