Skip to main content
Log in

Deformation Mechanisms of 316L Austenitic Stainless Steel Tubes under Equal Channel Angular Pressing

  • Published:
Journal of Materials Engineering and Performance Aims and scope Submit manuscript

Abstract

This study investigates the deformation mechanisms of 316L austenitic stainless steel tubes processed by equal channel angular pressing (ECAP) at room temperature. Nanoindentation tests were used to study the influence of the 1-pass ECAP process on mechanical properties. The microstructure evolution of specimens subjected to 1-pass ECAP process was systematically analyzed using a variety of characterization methods. The results from microstructures observed through cross sections and longitudinal sections of deformed samples at different areas showed that the grains were refined significantly by the 1-pass ECAP process, and numerous deformation twins were generated. The microstructures also showed that the 1-pass ECAP process can cause uneven refinement of grains due to inhomogeneous strain distribution. Significant changes in grain orientation and micro-texture were found during the 1-pass ECAP process. The deformation mechanisms of samples subjected to the 1-pass ECAP process consisted of two stages: dislocation slip and twinning. The observed plastic deformation by dislocation slip occurred prior to activate twinning, and severe plastic deformation mainly occurred near grain boundaries or twin boundaries.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Fig. 1
Fig. 2
Fig. 3
Fig. 4
Fig. 5
Fig. 6
Fig. 7
Fig. 8
Fig. 9
Fig. 10

Similar content being viewed by others

References

  1. J.-S. Li, W.-D. Gao, Y. Cao, Z.-W. Huang, B. Gao, Q.-Z. Mao, and Y.-S. Li, Microstructures and Mechanical Properties of a Gradient Nanostructured 316L Stainless Steel Processed by Rotationally Accelerated Shot Peening, Adv. Eng. Mater., 2018, 20(10), p 1800402

    Article  Google Scholar 

  2. K.H. Lo, C.H. Shek, and J.K.L. Lai, Recent Developments in Stainless Steels, Mater. Sci. Eng.: R: Rep., 2009, 65(4–6), p 39–104

    Article  Google Scholar 

  3. M. Naghizadeh and H. Mirzadeh, Microstructural Evolutions During Reversion Annealing of Cold-Rolled AISI, 316 Austenitic Stainless Steel, Metall. Mater. Trans. A, 2018, 49(6), p 2248–2256

    Article  CAS  Google Scholar 

  4. S. Wang, K. Wei, J. Li, Y. Liu, Z. Huang, Q. Mao, and Y. Li, Enhanced Tensile Properties of 316L Stainless Steel Processed by a Novel Ultrasonic Resonance Plastic Deformation Technique, Mater. Lett., 2019, 236, p 342–345

    Article  CAS  Google Scholar 

  5. D.M. Xu, G.Q. Li, X.L. Wan, R.L. Xiong, G. Xu, K.M. Wu, M.C. Somani, and R.D.K. Misra, Deformation Behavior of High Yield Strength—High Ductility Ultrafine-Grained 316LN Austenitic Stainless Steel, Mater. Sci. Eng., A, 2017, 688, p 407–415

    Article  CAS  Google Scholar 

  6. A. Belyakov, Y. Kimura, and K. Tsuzaki, Microstructure Evolution in Dual-Phase Stainless Steel During Severe Deformation, Acta Mater., 2006, 54(9), p 2521–2532

    Article  CAS  Google Scholar 

  7. R.Z. Valiev, R.K. Islamgaliev, and I.V. Alexandrov, Bulk Nanostructured Materials from Severe Plastic Deformation, Prog. Mater. Sci., 2000, 45, p 103–189

    Article  CAS  Google Scholar 

  8. I. Gutierrez-Urrutia, S. Zaefferer, and D. Raabe, The Effect of Grain Size and Grain Orientation on Deformation Twinning in a Fe-22 wt.% Mn-0.6 wt.% C TWIP Steel, Mater. Sci. Eng., A, 2010, 527(15), p 3552–3560

    Article  Google Scholar 

  9. N. Guo, Z. Zhang, Q. Dong, H. Yu, B. Song, L. Chai, C. Liu, Z. Yao, and M.R. Daymond, Strengthening and Toughening Austenitic Steel by Introducing Gradient Martensite Via Cyclic Forward/Reverse Torsion, Mater. Des., 2018, 143, p 150–159

    Article  CAS  Google Scholar 

  10. Y. Kitano, M. Yuasa, H. Miyamoto, M.H. Farshidi, and E. Bagherpour, Improving Hydro-Formability of Stainless Steel Tubes by Tube Channel Pressing, IOP Conf. Ser.: Mater. Sci. Eng., 2017, 194, p 012007

    Article  Google Scholar 

  11. X.H. An, Q.Y. Lin, S.D. Wu, Z.F. Zhang, R.B. Figueiredo, N. Gao, and T.G. Langdon, The Influence of Stacking Fault Energy on the Mechanical Properties Of Nanostructured Cu and Cu-Al Alloys Processed by High-Pressure Torsion, Scripta Mater., 2011, 64(10), p 954–957

    Article  CAS  Google Scholar 

  12. Z.K. Low, T. Chaise, D. Bardel, S. Cazottes, P. Chaudet, M. Perez, and D. Nelias, A Novel Approach to Investigate Delta Phase Precipitation in Cold-Rolled 718 Alloys, Acta Mater., 2018, 156, p 31–42

    Article  CAS  Google Scholar 

  13. M. Kawasaki, Z. Horita, and T.G. Langdon, Microstructural Evolution in High Purity Aluminum Processed by ECAP, Mater. Sci. Eng., A, 2009, 524(1–2), p 143–150

    Article  Google Scholar 

  14. S. Sabbaghianrad, S.A. Torbati-Sarraf, and T.G. Langdon, An investigation of the limits of grain refinement after processing by a combination of severe plastic deformation techniques: A comparison of Al and Mg alloys, Mater. Sci. Eng., A, 2018, 712, p 373–379

    Article  CAS  Google Scholar 

  15. K. Matsubara, Y. Miyahara, Z. Horita, and T.G. Langdon, Developing Superplasticity in a Magnesium Alloy Through a Combination of Extrusion and ECAP, Acta Mater., 2003, 51(11), p 3073–3084

    Article  CAS  Google Scholar 

  16. W. Skrotzki, N. Scheerbaum, C.-G. Oertel, R. Arruffat-Massion, S. Suwas, and L.S. Tóth, Microstructure and Texture Gradient in Copper Deformed by Equal Channel Angular Pressing, Acta Mater., 2007, 55(6), p 2013–2024

    Article  CAS  Google Scholar 

  17. J. Li, F. Li, W. Wang, X. Ma, and J. Li, Achieving Grain Refinement and Related Mechanical Property Improvement of an Al-Zn-Mg-Cu Alloy Through Severe Plastic Deformation, J. Mater. Eng. Perform., 2018, 27(12), p 6690–6700

    Article  CAS  Google Scholar 

  18. M. Toofaninejad and M.N. Ahmadabadi, Effect of Equal Channel Angular Pressing on the Microstructure and Mechanical Properties of AISI, Type 304 Austenitic Stainless Steel, Adv. Mater. Res., 2013, 829, p 86–90

    Article  Google Scholar 

  19. H. Ueno, K. Kakihata, Y. Kaneko, S. Hashimoto, and A. Vinogradov, Nanostructurization Assisted by Twinning During Equal Channel Angular Pressing of Metastable 316L Stainless Steel, J. Mater. Sci., 2011, 46(12), p 4276–4283

    Article  CAS  Google Scholar 

  20. L. Chen, F.P. Yuan, P. Jiang, and X.L. Wu, Mechanical Properties and Nanostructures in a Duplex Stainless Steel Subjected to Equal Channel Angular Pressing, Mater. Sci. Eng., A, 2012, 551, p 154–159

    Article  CAS  Google Scholar 

  21. J.A. Muñoz, O.F. Higuera, A.H. Expósito, A. Boulaajaj, R.E. Bolmaro, F.D. Dumitru, P.R. Calvillo, A.M. Jorge, and J.M. Cabrera, Thermal Stability of ARMCO Iron Processed by ECAP, Int. J. Adv. Manuf. Technol., 2018, 98(9–12), p 2917–2932

    Article  Google Scholar 

  22. M. Odnobokova, A. Belyakov, and R. Kaibyshev, Effect of Severe Cold or Warm Deformation on Microstructure Evolution and Tensile Behavior of a 316L Stainless Steel, Adv. Eng. Mater., 2015, 17(12), p 1812–1820

    Article  CAS  Google Scholar 

  23. J. Li, Y. Cao, B. Gao, Y. Li, and Y. Zhu, Superior Strength and Ductility of 316L Stainless Steel with Heterogeneous Lamella Structure, J. Mater. Sci., 2018, 53(14), p 10442–10456

    Article  CAS  Google Scholar 

  24. X. Ma, F. Li, Z. Sun, J. Hou, J. Li, and X. Fang, Strain Rate Dependence of the Indentation Size Effect in Ti-10 V-2Fe-3Al Alloy, Mater. Sci. Technol., 2019, 35(9), p 1107–1113

    Article  CAS  Google Scholar 

  25. F. Djavanroodi, A.A. Zolfaghari, M. Ebrahimi, and K.M. Nikbin, Equal Channel Angular Pressing of Tubular Samples, Acta Metall. Sinica (Engl. Lett.), 2013, 26(5), p 574–580

    Article  Google Scholar 

  26. M. Muhammad, J.W. Pegues, N. Shamsaei, and M. Haghshenas, Effect of Heat Treatments on Microstructure/Small-Scale Properties of Additive Manufactured Ti-6Al-4V, The International Journal of Advanced Manufacturing Technology, 2019, 103(9–12), p 4161–4172

    Article  Google Scholar 

  27. D.M. Jafarlou, E. Zalnezhad, M.A. Hassan, M.A. Ezazi, N.A. Mardi, A.M.S. Hamouda, M. Hamdi, and G.H. Yoon, Severe Plastic Deformation of Tubular AA 6061 Via Equal Channel Angular Pressing, Mater. Des., 2016, 90, p 1124–1135

    Article  CAS  Google Scholar 

  28. P.P. Bhattacharjee, M. Joshi, V.P. Chaudhary, J.R. Gatti, and M. Zaid, Texture Evolution During Cross Rolling and Annealing of High-Purity Nickel, Metall. Mater. Trans. A, 2013, 44(6), p 2707–2716

    Article  CAS  Google Scholar 

  29. S. Qu, C.X. Huang, Y.L. Gao, G. Yang, S.D. Wu, Q.S. Zang, and Z.F. Zhang, Tensile and Compressive Properties of AISI, 304L Stainless Steel Subjected to Equal Channel Angular Pressing, Mater. Sci. Eng., A, 2008, 475(1–2), p 207–216

    Article  Google Scholar 

  30. S. Ranjbar Bahadori, K. Dehghani, and F. Bakhshandeh, Microstructure, Texture and Mechanical Properties of Pure Copper Processed by ECAP and Subsequent Cold Rolling, Mater. Sci. Eng., A, 2013, 583, p 36–42

    Article  CAS  Google Scholar 

  31. V.S.A. Challa, X.L. Wan, M.C. Somani, L.P. Karjalainen, and R.D.K. Misra, Strain Hardening Behavior of Phase Reversion-Induced Nanograined/ultrafine-Grained (NG/UFG) Austenitic Stainless Steel and Relationship with Grain Size and Deformation Mechanism, Mater. Sci. Eng., A, 2014, 613, p 60–70

    Article  CAS  Google Scholar 

  32. D. Xu, X. Wan, J. Yu, G. Xu, G. Li, Effect of Cold Deformation on Microstructures and Mechanical Properties of Austenitic Stainless Steel, Metals, 8(7), (2018)

    Article  Google Scholar 

  33. H. Chen, F. Li, J. Li, X. Ma, J. Li, and Q. Wan, Hardening and Softening Analysis of Pure Titanium Based on the Dislocation Density During Torsion Deformation, Mater. Sci. Eng., A, 2016, 671, p 17–31

    Article  CAS  Google Scholar 

  34. Y.F. Shen, X.X. Li, X. Sun, Y.D. Wang, and L. Zuo, Twinning and Martensite in a 304 Austenitic Stainless Steel, Mater. Sci. Eng., A, 2012, 552, p 514–522

    Article  CAS  Google Scholar 

  35. Y.F. Shen, N. Jia, Y.D. Wang, X. Sun, L. Zuo, and D. Raabe, Suppression of Twinning and Phase Transformation in an Ultrafine Grained 2 GPa Strong Metastable Austenitic Steel: Experiment and Simulation, Acta Mater., 2015, 97, p 305–315

    Article  CAS  Google Scholar 

  36. J. Lu, L. Hultman, E. Holmström, K.H. Antonsson, M. Grehk, W. Li, L. Vitos, and A. Golpayegani, Stacking Fault Energies in Austenitic Stainless Steels, Acta Mater., 2016, 111, p 39–46

    Article  CAS  Google Scholar 

  37. J. Li, B. Gao, Z. Huang, H. Zhou, Q. Mao, and Y. Li, Design for Strength-Ductility Synergy of 316L Stainless Steel with Heterogeneous Lamella Structure Through Medium Cold Rolling and Annealing, Vacuum, 2018, 157, p 128–135

    Article  CAS  Google Scholar 

  38. X.H. Chen, J. Lu, L. Lu, and K. Lu, Tensile Properties of a Nanocrystalline 316L Austenitic Stainless Steel, Scripta Mater., 2005, 52(10), p 1039–1044

    Article  CAS  Google Scholar 

  39. F.K. Yan, G.Z. Liu, N.R. Tao, and K. Lu, Strength and Ductility of 316L Austenitic Stainless Steel Strengthened by Nano-Scale Twin Bundles, Acta Mater., 2012, 60(3), p 1059–1071

    Article  CAS  Google Scholar 

Download references

Acknowledgments

The authors are very grateful for the support received from the National Natural Science Foundation of China (Grant Nos. 51674004 and 51805002).

Author information

Authors and Affiliations

Authors

Corresponding authors

Correspondence to Jinghui Li or Zhenyi Huang.

Additional information

Publisher's Note

Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Zhang, J., Han, W., Rui, W. et al. Deformation Mechanisms of 316L Austenitic Stainless Steel Tubes under Equal Channel Angular Pressing. J. of Materi Eng and Perform 29, 1253–1261 (2020). https://doi.org/10.1007/s11665-020-04683-3

Download citation

  • Received:

  • Revised:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11665-020-04683-3

Keywords

Navigation