Abstract
In the paper, the structure and static and dynamic mechanical properties of ultrafine-grained A5083 alloy (Al-Mg-Mn) produced by high-pressure torsion (HPT) are reported. The static yield stress and tensile strength were determined in tensile tests at a strain rate of ~ 10−3 s−1, and the dynamic yield stress and spall strength were calculated from free-surface velocity histories obtained during shock-wave loading at a strain rate of 105 s−1. The HPT technique provides strong grain refinement. The average grain size of the alloy after HPT is 100-180 nm and depends on the accumulated true strain. HPT significantly improves the static strength properties of the alloy. The static yield stress is increased by 360-390% and the static ultimate tensile strength by 166-182%. It is shown that the dynamic yield stress improved by 168-181%, while the dynamic spall strength was not improved by HPT. Moreover, the nanostructured alloy with a grain size of ~ 100 nm demonstrates the lowest spall strength.
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs11665-019-04511-3/MediaObjects/11665_2019_4511_Fig1_HTML.png)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs11665-019-04511-3/MediaObjects/11665_2019_4511_Fig2_HTML.png)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs11665-019-04511-3/MediaObjects/11665_2019_4511_Fig3_HTML.jpg)
![](http://media.springernature.com/m312/springer-static/image/art%3A10.1007%2Fs11665-019-04511-3/MediaObjects/11665_2019_4511_Fig4_HTML.png)
Similar content being viewed by others
References
Y. Estrin and A. Vinogradov, Extreme Grain Refinement by Severe Plastic Deformation: A Wealth of Challenging Science, Acta Mater., 2013, 61, p 782–817
R.Z. Valiev, Y. Estrin, Z. Horita, T.G. Langdon, M.J. Zehetbauer, and Y.T. Zhu, Fundamentals of Superior Properties in Bulk NanoSPD Materials, Mater. Res. Lett., 2016, 4(1), p 1–21
I. Sabirov, M.Y. Murashkin, and R.Z. Valiev, Nanostructured Aluminum Alloys Produced by Severe Plastic Deformation: New Horizons in Development, Mater. Sci. Eng., A, 2013, 560, p 1–24
T. Mungole, P. Kumar, M. Kawasaki, and T.G. Langdon, The Contribution of Grain Boundary Sliding in Tensile Deformation of an Ultrafine-Grained Aluminum Alloy Having High Strength and High Ductility, J. Mater. Sci., 2015, 50, p 3549–3561
R.Z. Valiev, M.Y. Murashkin, A. Kilmametov, B. Straumal, N.Q. Chinh, and T.G. Langdon, Unusual Super-Ductility at Room Temperature in an Ultrafine-Grained Aluminum Alloy, J. Mater. Sci., 2010, 45, p 4718–4724
Y.H. Zhao, J.F. Bingert, X.Z. Liao, B.Z. Cui, K. Han, A. Sergueeva, A.K. Mukherjee, R.Z. Valiev, T.G. Langdon, and Y.T. Zhu, Simultaneously Increasing the Ductility and Strength of Ultra-Fine-Grained Pure Copper, Adv. Mater., 2006, 65, p 3472–3475
M.V. Markushev, E.V. Avtokratova, S.V. Krymskiy, and OSh Sitdikov, Effect of Precipitates on Nanostructuring and Strengthening of High-Strength Aluminum Alloys under High Pressure Torsion, J. Alloys Compd., 2018, 743, p 773–779
R.Z. Valiev, N.A. Enikeev, M.Y. Murashkin, V.U. Kazykhanov, and X. Sauvage, On the Origin of the Extremely High Strength of Ultrafine-Grained Al Alloys Produced by Severe Plastic Deformation, Scripta Mater., 2010, 63, p 949–952
M. Ruppert, M. Strebl, H.W. Hoppel, and M. Goken, Mechanical Properties of Ultrafine-Grained AlZnMg(Cu)-Alloys AA7020 and AA7075 Processed by Accumulative Roll Bonding, J. Mater. Sci., 2015, 50, p 4422–4429
E. Avtokratova, O. Sitdikov, M. Markushev, and R. Mulyukov, Extraordinary High-Strain Rate Superplasticity of Severely Deformed Al-Mg-Sc-Zr Alloy, Mater. Sci. Eng., 2012, A538, p 386–390
Y. Estrin and A. Vinogradov, Fatigue Behaviour of Light Alloys with Ultrafine Grain Structure Produced by Severe Plastic Deformation: An Overview, Int. J. Fatigue, 2010, 32, p 898–907
P.H.R. Pereira, Y.C. Wang, Y. Huang, and T.G. Langdon, Influence of Grain Size on the Flow Properties of an Al-Mg-Sc Alloy Over Seven Orders of Magnitude of Strain Rate, Mater. Sci. Eng., A, 2017, 685, p 367–376
J. Jiang, J. Shi, Y. Yao, A. Ma, D. Song, D. Yang, J. Chen, and F. Lu, Dynamic Compression Properties of an Ultrafine-Grained Al-26wt.%Si Alloy Fabricated by Equal-Channel Angular Pressing, J. Mater. Eng. Perform., 2015, 24(5), p 2016–2024
R. Kapoor, J.B. Singh, and J.K. Chakravartty, High Strain Rate Behavior of Ultrafine-Grained Al–1,5 Mg, Mater. Sci. Eng., A, 2008, 496, p 308–315
F. Fereshteh-Saniee, S. Sepahi-Boroujeni, S. Lahmi, and G.H. Majzoobi, An Experimental Investigation on the Strain Rate Sensitivity of a Severely Deformed Aluminum Alloy, Exp. Mech., 2015, 55(3), p 569–576
A.N. Petrova, I.G. Brodova, O.A. Plekhov, O.B. Naimark, and E.V. Shorokhov, Mechanical Properties and Energy Dissipation in Ultrafinegrained AMts and V95 Aluminum Alloys during Dynamic Compression, Tech. Phys., 2014, 59(7), p 989–996
I.G. Brodova, A.N. Petrova, O.B. Naimark, O.A. Plekhov, S.V. Razorenov, and E.V. Shorokhov, The Influence of the Structure of Ultrafine-Grained Aluminium Alloys on Their Mechanical Properties under Dynamic Compression and Shock-Wave Loading, IOP Conf. Ser.: J. Phys., 2017, 894, p 012016
S. Zhang, Y. Chun Wang, A.P. Zhilyaev, E. Korznikova, S. Li, G.I. Raab, and T.G. Langdon, Temperature and Strain Rate Dependence of Microstructural Evolution and Dynamic Mechanical Behaviour in Nanocrystalline Ti, Mater. Sci. Eng., 2015, A641, p 29–36
O. Plekhov, V. Chudinov, V. Leont’ev, and O. Naimark, Experimental Investigations of the Laws of Energy Dissipation during Dynamic Deformation of Nanocrystalline Titanium, Tech. Phys. Lett., 2009, 351, p 92–95
K.V. Ivanov, S.V. Razorenov, and G.V. Garkushin, Quasi-Static and Shock-Wave Loading of Ultrafine-Grained Aluminum: Effect of Microstructural Characteristics, J/ Mater. Sci., 2018, 53(20), p 14681–14693
A.N. Petrova, I.G. Brodova, and S.V. Razorenov, Strength Properties and Structure of a Submicrocrystalline Al-Mg-Mn Alloy under Shock Compression, Phys. Metals Metall., 2017, 118(6), p 601–607
I.G. Brodova, A.N. Petrova, S.V. Razorenov, and E.V. Shorokhov, Resistance of Submicrocrystalline Aluminum Alloys to High-Rate Deformation and Fracture after Dynamic Channel Angular Pressing, Phys. Metals Metall., 2015, 116(5), p 519–526
R.L. Whelchel, N.N. Thadhani, T.H. Sanders, L.J. Kecskes, and C.L. Williams, Spall Properties of Al 5083 Plate Fabricated Using Equal-Channel Angular Pressing (ECAP) and Rolling, J. Phys: Conf. Ser., 2014, 500, p 112066
S.V. Razorenov, G.I. Kanel, G.V. Garkushin, and O.N. Ignatova, Resistance to Dynamic Deformation and Fracture of Tantalum with Different Grain and Defect Structures, Phys. Solid State, 2012, 54(4), p 790–797
T. Antoun, L. Seaman, D.R. Curran, G.I. Kanel, S.V. Razorenov, and A.V. Utkin, Spall Fracture, Springer, New York, 2003
L.M. Barker and R.E. Hollenbach, Laser Interferometry for Measuring High Velocities of any Reflecting Surface, J. Appl. Phys., 1972, 43, p 4669–4675
M.V. Markushev, C.C. Bampton, MYu Murashkin, and D.A. Hardwick, Structure and Properties of Ultra-Fine Grained Aluminum Alloys Produced by Severe Plastic Deformation, Mater. Sci. Eng., 1997, A234–236, p 927–931
Acknowledgments
Structural investigation and static tensile tests were carried out within the state assignment of Minobrnauki of Russia (theme “Struktura”, No. AAAA-A18-118020190116-6), supported in part by RFBR (Project 18-03-00102). The transmission electron microscopy investigations were carried out at the Center of Collaborative Access “Testing Center of Nanotechnologies and Advanced Materials” of the M.N. Miheev Institute of Metal Physics of Ural Branch of Russian Academy of Sciences. The dynamic experiments were performed using equipment of the Moscow Regional Explosion Research Center of Collective Use of the Russian Academy of Sciences under financial support of the Program of Basic Researches of Presidium of Russian Academy of Sciences (No. 13P) “Condensed matter and plasma under high energy density”.
Author information
Authors and Affiliations
Corresponding author
Additional information
Publisher's Note
Springer Nature remains neutral with regard to jurisdictional claims in published maps and institutional affiliations.
Rights and permissions
About this article
Cite this article
Petrova, A.N., Brodova, I.G., Razorenov, S.V. et al. Grain Size Effects on Static and Dynamic Strength of Ultrafine-Grained Al-Mg-Mn Alloy Produced by High-Pressure Torsion. J. of Materi Eng and Perform 29, 464–469 (2020). https://doi.org/10.1007/s11665-019-04511-3
Received:
Revised:
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11665-019-04511-3