Abstract
Al 5052 alloy sheets were subjected to different pre-annealing temperatures (150, 200, 250, 300, and 350 °C) prior to cryorolling. The process resulted in Al 5052 alloys with different initial microstructures. The pre-annealed alloy sheets were compared with a cryorolled sample not subjected to pre-annealing. The thicknesses of the alloy samples after cryorolling was reduced by 30%. The pre-annealed cryorolled samples exhibited low crystallite size, and high lattice strain. Among them, the cryorolled sample pre-annealed at 300 °C had the lowest crystallite size, and the highest lattice strain. Changes in initial microstructure of this sample resulted in a significant improvement in its hardness (88 Hv), tensile strength (333 MPa), and corrosion resistance. The sample had the highest corrosion resistance among the cryorolled samples.
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References
C.H. Liu and H.C. Lin, Equal Channel Angular Extrusion of AA 6063 Using Conventional Direct Extrusion Press, J. Mater. Eng. Perform., 2015, 24(11), p 4569–4577
J. Lu, X. Wu, Z. Liu, D. Guo, Y. Lou, and S. Ruan, Microstructure and Mechanical Properties of Ultrafine-Grained Al-6061 Prepared Using Intermittent Ultrasonic-Assisted Equal-Channel Angular Pressing, J. Mater. Eng. Perform., 2017, 26(10), p 5107–5117
R.Z. Valiev and T.G. Langdon, Principles of Equal-Channel Angular Pressing as a Processing Tool for Grain Refinement, Prog. Mater. Sci., 2006, 51, p 881–981
N. Kamikawa and T. Furuhara, Accumulative Channel-Die Compression Bonding (ACCB): A New Severe Plastic Deformation Process to Produce Bulk Nanostructured Metals, J. Mater. Process. Technol., 2013, 213, p 1412–1418
A.P. Zhilyaev and T.G. Langdon, Using High-Pressure Torsion for Metal Processing: Fundamentals and Applications, Prog. Mater. Sci., 2008, 53, p 893–979
S.K. Panigrahi and R. Jayaganthan, Effect of Rolling Temperature on Microstructure and Mechanical Properties of 6063 Al Alloy, Mater. Sci. Eng. A, 2008, 492, p 300–305
Y.M. Wang, M.W. Chen, F.H. Zhou, and E. Ma, High Tensile Ductility in a Nanostructured Metal, Nature, 2002, 419, p 912–915
D.F. Guo, M. Li, Y.D. Shi, Z.B. Zhang, H.T. Zhang, X.M. Liu, B.N. Wei, and X.Y. Zhang, High Strength and Ductility in Multimodal-Structured Zr, Mater. Des., 2012, 34, p 275–278
F. Feyissa, D.R. Kumar, and P.N. Rao, Characterization of Microstructure, Mechanical Properties and Formability of cryorolled AA5083 Alloy Sheets, J. Mater. Eng. Perform., 2018, 27(4), p 1614–1626
S.K. Panigrahi, R. Jayaganthan, and V. Pancholi, Effect of Plastic Deformation Conditions on Microstructural Characteristics and Mechanical Properties of Al 6063 Alloy, Mater. Des., 2009, 30, p 1894–1901
Y.B. Lee, D.H. Shin, K.T. Park, and W.J. Nam, Effect of Annealing Temperature on Microstructures and Mechanical Properties of A 5083 Al Alloy Deformed at Cryogenic Temperature, Scr. Mater., 2004, 51, p 355–359
K. Krishna, K.C. Sekhar, R. Tejas, N.N. Krishna, K. Sivaprasad, R. Narayanasamy, and K. Venkateswarlu, Effect of Cryorolling on The Mechanical Properties of AA5083 Alloy and the Portevin–Le Chatelier Phenomenon, Mater. Des., 2015, 67, p 107–117
K.C. Sekhar, R. Narayanasamy, and K. Velmanirajan, Experimental Investigations on Microstructure and Formability of Cryorolled AA 5052 Sheets, Mater. Des., 2014, 53, p 1064–1070
U.G. Gang, S.H. Lee, and W.J. Nam, The Evolution of Microstructure and Mechanical Properties of a 5052 Aluminium Alloy by the Application of Cryogenic Rolling and Warm Rolling, Mater. Trans., 2009, 50, p 82–86
P.N. Rao, A. Kaurwar, D. Singh, and R. Jayaganthan, Enhancement in Strength and Ductility of Al-Mg-Si Alloy by Cryorolling Followed by Warm Rolling, Procedia Eng., 2014, 75, p 123–128
R.J. Immanuel and S.K. Panigrahi, Influence of Cryorolling on Microstructure and Mechanical Properties of a Cast Hypoeutectic Al–Si Alloy, Mater. Sci. Eng. A, 2015, 640, p 424–435
Q.W. Jiang and X.W. Li, Effect of Pre-annealing Treatment on the Compressive Deformation and Damage Behavior of Ultrafine-Grained Copper, Mater. Sci. Eng. A, 2012, 546, p 59–67
D. Singh, P. Nageswara Rao, and R. Jayaganthan, High Cyclic Fatigue Behaviour of Ultrafine Grained Al 5083 Alloy, Mater. Sci. Technol., 2014, 30, p 1835–1842
U.G. Kang, J.C. Lee, S.W. Jeong, and W.J. Nam, The Improvement of Strength and Ductility in Ultra-Fine Grained 5052 Al Alloy by Cryogenic- and Warm-Rolling, J. Mater. Sci., 2010, 45, p 4739–4744
D. Singh, P. Nageswara Rao, and R. Jayaganthan, Microstructures and Impact Toughness Behavior of Al 5083 Alloy Processed by Cryorolling and Afterwards Annealing, Int. J. Miner. Metall. Mater., 2013, 20, p 759–769
D. Guo, M. Li, Y. Shi, Z. Zhang, T. Ma, and H. Zhang, Simultaneously Enhancing the Ductility and Strength of Cryorolled Zr via Tailoring Dislocation Configurations, Mater. Sci. Eng. A, 2012, 558, p 611–615
S.K. Panigrahi, D. Devanand, and R. Jayaganthan, Effect of Ageing on Strength and Ductility of Ultrafine Grained Al 6061 Alloy, Mater. Sci. Forum, 2010, 633–634, p 303–309
P. Bhaskar, A. Dasgupta, V.S. Sarma, U.K. Mudali, and S. Saroja, Mechanical Properties and Corrosion Behaviour of Nanocrystalline Ti-5Ta-1.8Nb Alloy Produced by Cryo-Rolling, Mater. Sci. Eng. A, 2014, 616, p 71–77
N.N. Krishna, K. Sivaprasad, and P. Susila, Strengthening Contributions in Ultra-High Strength Cryorolled Al-4%Cu-3%TiB2 In Situ Composite, Trans. Nonferrous Met. Soc. China, 2014, 24, p 641–647
M. Naseri, M. Reihanian, and E. Borhani, A New Strategy to Simultaneous Increase in the Strength and Ductility of AA2024 Alloy via Accumulative Roll Bonding (ARB), Mater. Sci. Eng. A, 2016, 656, p 12–20
P.N. Rao and R. Jayaganthan, Effects of Warm Rolling and Ageing After Cryogenic Rolling on Mechanical Properties and Microstructure of Al 6061 Alloy, Mater. Des., 2012, 39, p 226–233
P.N. Rao, B. Viswanadh, and R. Jayaganthan, Effect of Cryorolling and Warm Rolling on Precipitation Evolution in Al 6061 Alloy, Mater. Sci. Eng. A, 2014, 606, p 1–10
M. Mirzaei, M.R. Roshan, and S.A. Jenabali, Jahromi, Microstructure and Mechanical Properties Relation in Cold Rolled Al 2024 Alloy Determined by X-ray Line Profile Analysis, Mater. Sci. Eng. A, 2015, 620, p 44–49
B. Gopi, N. Naga Krishna, K. Sivaprasad, and K. Venkateswarlu, Effect of Rolling Temperature on Microstructure and Mechanical Properties of Cryorolled Al-Mg-Si Alloy Reinforced with 3wt.% TiB2 In Situ Composite, Adv. Mater. Res., 2012, 584, p 556–560
C. Hammond, The Basics of Crystallography and Diffraction, 3rd ed., Oxford University Press Inc., New York, 2009
N. Naga Krishna, R. Tejas, K. Sivaprasad, and K. Venkateswarlu, Study on Cryorolled Al-Cu Alloy Using X-ray Diffraction Line Profile Analysis and Evaluation of Strengthening Mechanisms, Mater. Des., 2013, 52, p 785–790
N. Naga Krishna, M. Ashfaq, P. Susila, K. Sivaprasad, and K. Venkateswarlu, Mechanical Anisotropy and Microstructural Changes During Cryorolling of Al–Mg–Si Alloy, Mater. Charact., 2015, 107, p 302–308
H.J. Chen, S.W. Lee, J.S. Park, and D.H. Bae, Positive Deviation from a Hall–Petch Relation in Nanocrystalline Aluminum, Mater. Trans., 2009, 50, p 640–643
S. Thangaraju, M. Heilmaier, B.S. Murty, and S.S. Vadlamani, On the Estimation of True Hall–Petch Constants and Their Role on the Superposition Law Exponent in Al Alloys, Adv. Eng. Mater., 2012, 14, p 892–897
R.W. Armstrong, Hall–Petch Description of Nano-crystalline Cu, Ni and Al Strength Levels and Strain Rate Sensitivities, Philos. Mag., 2016, 96, p 3097–3108
H.J. Choi, S.W. Lee, J.S. Park, and D.H. Bae, Positive Deviation from a Hall–Petch Relation in Nanocrystalline Aluminum, Mater. Trans., 2009, 50, p 640–643
A. Dhal, S.K. Panigrahi, and M.S. Shunmugam, Influence of Annealing on Stain Hardening Behaviour and Fracture Properties of a Cryorolled Al 2014 alloy, Mater. Sci. Eng. A, 2015, 645, p 383–392
B. Gopi, N. Naga Krishna, K. Sivaprasad, and K. Venkateswarlu, Influence of Rolling Temperature on Microstructure and Mechanical Properties of Cryorolled Al-Mg-Si Alloy, World Acad. Sci. Eng. Technol., 2012, 6, p 604–608
N. Rangaraju, T. Raghuram, B.V. Krishna, K.P. Rao, and P. Venugopal, Effect of Cryo-Rolling and Annealing on Microstructure and Properties of Commercially Pure Aluminium, Mater. Sci. Eng. A, 2005, 398, p 246–251
N.N. Krishna, B. Gopi, K. Sivaprasad, and V. Muthupandi, Studies on Potentiodynamic Polarization Behaviour of Cryorolled Al-Mg-Si Alloy, Key Eng. Mater., 2013, 545, p 153–157
K. Gopala Krishna, K. Sivaprasad, T.S.N.S. Narayanan, and K.C. Hari Kumar, Localized Corrosion of an Ultrafine Grained Al-4Zn-2Mg Alloy Produced by Cryorolling, Corros. Sci., 2012, 60, p 82–89
K. Sivaprasad, V. Swarnalatha, V.V. Ravikumar, and V. Muthupandi, Influence of Short Annealing Treatment on Corrosion Behaviour of Cryorolled Commercially Pure Aluminum, Anti Corros. Methods Mater., 2010, 57, p 18–20
Ł. Dolega, B. Adamczyk-Cieslak, J. Mizera, and K.J. Kurzydłowski, Corrosion Resistance of Model Ultrafine-Grained Al–Li Alloys Produced by Severe Plastic Deformation, J. Mater. Sci., 2012, 47, p 3026–3033
X.Y. Zhang, M.H. Shi, C. Li, N.F. Liu, and Y.M. Wei, The Influence of Grain Size on the Corrosion Resistance of Nanocrystalline Zirconium Metal, Mater. Sci. Eng. A, 2007, 448, p 259–263
S. Gollapudi, Grain Size Distribution Effects on the Corrosion Behaviour of Materials, Corros. Sci., 2012, 62, p 90–94
L.Y. Qin, J.S. Lian, and Q. Jiang, Effect of Grain Size on Corrosion Behavior of Electrodeposited Bulk Nanocrystalline Ni, Trans. Nonferrous Met. Soc. China, 2010, 20, p 82–89
A. Balyanov, J. Kutnyakova, N.A. Amirkhanova, V.V. Stolyarov, R.Z. Valiev, X.Z. Liao et al., Corrosion Resistance of Ultra Fine-Grained Ti, Scr. Mater., 2004, 51, p 225–229
I. Sabirov, M.Y. Murashkin, and R.Z. Valiev, Nanostructured Aluminium Alloys Produced by Severe Plastic Deformation: New Horizons in Development, Mater. Sci. Eng. A, 2013, 560, p 1–24
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The authors gratefully thank Universiti Sains Malaysia for funding this study under the RU Grant (1001/PBahan/814197).
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Anas, N.M., Dhindaw, B.K., Zuhailawati, H. et al. Effect of Initial Microstructure on Properties of Cryorolled Al 5052 Alloy Subjected to Different Annealing Treatment Temperatures. J. of Materi Eng and Perform 27, 6206–6217 (2018). https://doi.org/10.1007/s11665-018-3645-7
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DOI: https://doi.org/10.1007/s11665-018-3645-7