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X-ray Diffraction and Magnetic Investigations of Lithium-Zinc Ferrites Synthesized by Electron Beam Heating

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Abstract

Li0.5(1−x )ZnxFe2.5−0.5x O4 ferrites (x = 0.2; 0.4) were produced by thermal and radiation-thermal (RT) synthesis from Li2CO3-Fe2O3-ZnO powder mixtures and then studied using x-ray diffraction (XRD) and saturation magnetization analysis. The RT synthesis was carried out by 2.4 MeV electron beam heating of samples from the first batch at the temperatures of 600°C, 700°C, 750°C and isothermal exposure time of 0 min, 10 min, 20 min, 30 min, 60 min, and 120 min. For comparative analysis, thermal heating of samples from the second batch was performed in a resistance laboratory furnace using the same time and temperature regimes. XRD analysis of samples showed the formation of lithium-zinc ferrites with greater homogeneous phase composition at lower values of temperature and time during RT synthesis compared to the samples obtained by thermal heating. Also, RT-synthesized ferrites are characterized by significantly higher values of saturation magnetization at all time and temperature regimes. It was established that a regime of RT synthesis at 750°C–30 min provides the formation of lithium-zinc ferrites with a high degree of final phase composition.

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References

  1. P.D. Baba, G.M. Argentina, W.E. Courtney, G.F. Dionne, and D.H. Temme, IEEE Trans. Magn. 8, 83 (1972).

    Article  Google Scholar 

  2. K. Zhou, W. Chen, X. Wu, W. Wu, C. Lin, and J. Wu, J. Electron. Mater. 46, 4618 (2017). https://doi.org/10.1007/s11664-017-5466-0.

    Article  Google Scholar 

  3. I. Ahmad, S.M. Shah, M.N. Ashiq, F. Nawaz, A. Shah, M. Siddiq, I. Fahim, and S. Khan, J. Electron. Mater. 45, 4979 (2016).

    Article  Google Scholar 

  4. G.O. White and C.E. Patton, Magn. Magn. Mater. 9, 299 (1978).

    Article  Google Scholar 

  5. S.H. Gee, Y.K. Hong, M.H. Park, D.W. Erickson, and P.J. Lamb, J. Appl. Phys. 91, 7586 (2002).

    Article  Google Scholar 

  6. M.S. Ruiz and S.E. Jacobo, Phys. B 407, 3274 (2012).

    Article  Google Scholar 

  7. M. Kavanlooee, B. Hashemi, H. Maleki-Ghaleh, and J. Kavanlooee, J. Electron. Mater. 41, 3082 (2012).

    Article  Google Scholar 

  8. S.K. Gurav, S.E. Shirsath, R.H. Kadam, S.M. Patange, K.S. Lohar, and D.R. Mane, Mater. Res. Bull. 48, 3530 (2013).

    Article  Google Scholar 

  9. A.V. Malyshev, E.N. Lysenko, and V.A. Vlasov, Ceram. Int. 41, 13671 (2015).

    Article  Google Scholar 

  10. M. Shahjahan, N.A. Ahmed, S.N. Rahman, S. Islam, N. Khatun, and M.S. Hossain, Int. J. Innov. Techol. Explor. Eng. 3, 48 (2014).

    Google Scholar 

  11. E. De Fazio, P.G. Bercoff, and S.E. Jacobo, J. Magn. Magn. Mat. 323, 2813 (2011). https://doi.org/10.1016/j.jmmm.2011.06.022.

    Article  Google Scholar 

  12. A.N. Yusoff and M.N. Abdullah, J. Magn. Magn. Mater. 269, 271 (2004). https://doi.org/10.1016/S0304-8853(03)00617-6.

    Article  Google Scholar 

  13. M. Yasuoka, Y. Nishimura, T. Nagaoka, and K. Watari, J. Therm. Anal. Calorim. 83, 407 (2006).

    Article  Google Scholar 

  14. A.M. Ibrahim, M.M. Abd El-Latif, and M.M. Mahmoud, J. Alloy. Compd. 506, 201 (2010).

    Article  Google Scholar 

  15. H.M. Widatallah, X.L. Ren, and I.A. Al-Omari, J. Mater. Sci. 41, 6333 (2006).

    Article  Google Scholar 

  16. V. Berbenni, A. Marini, P. Matteazzi, R. Ricceri, and N.J. Welham, J. Eur. Ceram. Soc. 23, 527 (2003).

    Article  Google Scholar 

  17. V.V. Boldyrev, Russ. Chem. Rev. 75, 177 (2006).

    Article  Google Scholar 

  18. D. Michael, P. Mingos, and D.R. Baghurst, Chem. Soc. Rev. 20, 1 (1991).

    Article  Google Scholar 

  19. M. Oghbaei and O. Mirzaee, J. Alloy. Compd. 494, 175 (2010).

    Article  Google Scholar 

  20. N.Z. Lyakhov, V.V. Boldyrev, A.P. Voronin, O.S. Gribkov, I.G. Bochkarev, S.V. Rusakov, and V.L. Auslender, J. Therm. Anal. Calorim. 43, 21 (1995).

    Article  Google Scholar 

  21. V.V. Boldyrev, A.P. Voronin, O.S. Gribkov, E.V. Tkachenko, G.R. Karagedov, B.I. Yakobson, and V.L. Auslender, Solid State Ion. 36, 1 (1989).

    Article  Google Scholar 

  22. V.L. Auslender, I.G. Bochkarev, V.V. Boldyrev, N.Z. Lyakhov, and A.P. Voronin, Solid State Ion. 101–103, 489 (1997).

    Article  Google Scholar 

  23. V.A. Neronov, A.P. Voronin, M.I. Tatarintseva, T.E. Melekhova, and V.L. Auslender, J. Less Common Metals 117, 391 (1986).

    Article  Google Scholar 

  24. V.G. Kostishin, V.G. Andreev, V.V. Korovushkin, D.N. Chitanov, N.A. Yudanov, A.T. Morchenko, A.S. Komlev, AYu Adamtsov, and A.N. Nikolaev, Inorgan. Mater. 50, 1317 (2014).

    Article  Google Scholar 

  25. U.V. Ancharova, M.A. Mikhailenko, B.P. Tolochko, N.Z. Lyakhov, M.V. Korobeinikov, A.A. Bryazgin, V.V. Bezuglov, and E.A. Shtarklev I.O.P. Conf. Ser. Mater. Sci. Eng. 81, 012122 (2015).

    Article  Google Scholar 

  26. V.A. Zhuravlev, E.P. Naiden, R.V. Minin, V.I. Itin, V.I. Suslyaev, and E.Y. Korovin I.O.P. Conf. Ser. Mater. Sci. Eng. 81, 012003 (2015). https://doi.org/10.1088/1757-899X/81/1/012003.

    Article  Google Scholar 

  27. E.P. Naiden, R.V. Minin, V.I. Itin, and V.A. Zhuravlev, Russ. Phys. J. 56, 674 (2013).

    Article  Google Scholar 

  28. A.P. Surzhikov, A.M. Pritulov, E.N. Lysenko, A.N. Sokolovskii, V.A. Vlasov, and E.A. Vasendina, J. Therm. Anal. Calorim. 110, 733 (2012). https://doi.org/10.1007/ s10973-011-1947-1

    Article  Google Scholar 

  29. E.N. Lysenko, A.P. Surzhikov, V.A. Vlasov, E.V. Nikolaev, A.V. Malyshev, A.A. Bryazgin, M.V. Korobeynikov, and M.A. Mikhailenko, J. Nucl. Instr. Meth. Phys. Res. B. 392, 1 (2017).

    Article  Google Scholar 

  30. A.P. Surzhikov, E.N. Lysenko, V.A. Vlasov, A.V. Malyshev, and E.A. Vasendina, Mater. Chem. Phys. 176, 110 (2016).

    Article  Google Scholar 

  31. A.V. Malyshev, E.N. Lysenko, V.A. Vlasov, and S.A. Nikolaeva, Ceram. Int. 42, 16180 (2016).

    Article  Google Scholar 

  32. V.L. Auslender, J. Nucl. Instr. Meth. Phys. Res. B. 89, 46 (1994).

    Article  Google Scholar 

  33. R.A. Salimov, V.G. Cherepkov, J.I. Golubenko, G.S. Krainov, B.M. Korabelnikov, S.A. Kuznetsov, N.K. Kuksanov, A.B. Malinin, and P.I. Nemytov, J. Radiat. Phys. Chem. 57, 661 (2000).

    Article  Google Scholar 

  34. V.V. Bezuglov, A.A. Bryazgin, A.Y. Vlasov, E.N. Kokin, and E.A. Shtarklev, Phys. Part. Nucl. Lett. 13, 784 (2016).

    Article  Google Scholar 

  35. E.W. Gorter, J. Philips Res. Rep. 9, 295 (1954).

    Google Scholar 

  36. C.E. Patton, C.A. Edmondson, and Y.H. Liu, J. Appl. Phys. 53, 2431 (1982).

    Article  Google Scholar 

  37. W.D. Wilber, P. Kabos, and C.E. Patton, IEEE Trans. Magn. 19, 1862 (1983). https://doi.org/10.1109/TMAG. 1983.1062727

  38. S. Misra, S. Ram, and R.S. Shinde, AIP Conf. Proc. 1447, 413 (2012). https://doi.org/10.1063/1.4710055.

    Article  Google Scholar 

  39. J. Sláma, M. Šoka, A. Grusková, R. Dosoudil, V. Jančárik, and J. Degmová, J. Magn. Magn. Mater. 326, 251 (2013). https://doi.org/10.1016/j.jmmm.2012.07.016.

    Article  Google Scholar 

  40. Y.M. Annenkov, Russ. Phys. J. 39, 1146 (1996).

    Article  Google Scholar 

  41. A.P. Surzhikov, A.M. Pritulov, E.N. Lysenko, V.A. Vlasov, E.A. Vasendina, and A.V. Malyshev, J. Therm. Anal. Calorim. 112, 739 (2013).

    Article  Google Scholar 

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Authors and Affiliations

  1. Problem Research Laboratory of Electronics, Dielectrics and Semiconductors, Tomsk Polytechnic University, Tomsk, Russia, 634050

    A. P. Surzhikov, E. N. Lysenko, E. A. Sheveleva, A. V. Malyshev, A. L. Astafyev & V. A. Vlasov

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  1. A. P. Surzhikov
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  2. E. N. Lysenko
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  3. E. A. Sheveleva
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  4. A. V. Malyshev
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  5. A. L. Astafyev
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  6. V. A. Vlasov
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Correspondence to V. A. Vlasov.

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Surzhikov, A.P., Lysenko, E.N., Sheveleva, E.A. et al. X-ray Diffraction and Magnetic Investigations of Lithium-Zinc Ferrites Synthesized by Electron Beam Heating. J. Electron. Mater. 47, 1192–1200 (2018). https://doi.org/10.1007/s11664-017-5896-8

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  • DOI: https://doi.org/10.1007/s11664-017-5896-8

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