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Microstructure and Mechanical Properties of Ti50Ni(50-X)FeX Alloys Fabricated by Powder Metallurgy Process

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Abstract

This paper investigates the microstructure and mechanical properties of Ti50Ni(50−X)FeX alloys fabricated by powder metallurgy technique. Here, sintering temperatures varied from 1100 °C to 1200 °C for the compacted milled powder mixture. Microstructure, chemical composition, phase formation, porosity, density, hardness, wear, shape memory effect, and compressive strength of the sintered sample were carried out using SEM, EDS, XRD, and mechanical tests, respectively. The SEM and XRD analysis results show that the microstructure of alloys consists of (Ni, Fe)-rich, Ti-rich phases with less retained pore. The densification and hardness increase with increasing the sintering temperature. The 4 at. pct Fe sample sintered at 1200 °C shows higher densification, a lower friction coefficient, and a higher hardness value. The 4 at. pct Fe sample sintered at 1150 °C shows higher compressive, and yield strengths of 132.57 and 116.86 MPa, respectively, and the 6 at. pct Fe sample sintered at 1200 °C shows a higher shape memory effect of 3.37 pct, which are higher in comparison to other compositions and other sintering temperature samples. Abrasive wear of the sample has been carried out, and it found that there is a decrease in friction coefficient value with an increase in sintering temperature from 1150 °C to 1200 °C of the sample.

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Acknowledgments

This is a part of academic research work and is under the support of the Department of Metallurgical and Materials Engineering, National Institute of Technology, Rourkela, India.

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  1. Department of Metallurgical and Materials Engineering, National Institute of Technology, Rourkela, Odisha, 769008, India

    Jagadish Parida, Subash Chandra Mishra & Ajit Behera

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All authors are agreed to the publication of the above manuscript. The contribution of all the authors is given below: JP: writing-original draft preparation, data accumulation, analysis, SCM: supervision, execution, and AB: conceptualist, analysis, supervision, review, modification.

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Correspondence to Ajit Behera.

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Parida, J., Mishra, S.C. & Behera, A. Microstructure and Mechanical Properties of Ti50Ni(50-X)FeX Alloys Fabricated by Powder Metallurgy Process. Metall Mater Trans A 54, 2585–2604 (2023). https://doi.org/10.1007/s11661-023-07037-5

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