Abstract
Friction stir processing (FSP) of Al 5059 is studied in which subsequent heat treatment is conducted to investigate its effects on grain size and hardness. It was found that mainly elongated and rhomboidal morphologies of Al6(Mn,Fe) particles are present in the alloy both before and after FSP, where the rhomboidal particles are more effective in pinning grain boundaries during heat treatment. The stir zone reached a temperature of 705 K (432 °C), and ThermoCalc modeling confirmed that the Al6(Mn,Fe) particles will remain stable at this temperature. Negligible grain growth was observed during FSP of the Al 5059 due to low grain boundary mobility resulting from slow diffusion associated with a high Mg content in the alloy. During heat treatment at 448 K (175 °C) grain growth could be correlated with time using a particle-controlled grain growth model. Microhardness values indicate that Hall–Petch behavior occurs in the processed alloy, while dislocation density and particle dispersion play a minor role in strengthening.
Similar content being viewed by others
References
M.L. Santella, T. Engstrom, D. Storjohann, T.Y. Pan, Scripta Mater. 53 (2005) 201–6.
N. Sun, D. Apelian, JOM 63 (2011) 44–50.
K. Oh-Ishi, T.R. McNelley, Metall. Mater. Trans. A, 35A (2004) 2951–61.
K. Nakata, Y.G. Kim, H. Fujii, T. Tsumura, T. Komazaki, Mater. Sci. Eng. A 437 (2006) 274–80.
Y. Morisada, H. Fujii, T. Nagaoka, M. Fukusumi, Mater. Sci. Eng. A 419 (2006) 344–8.
H. Izadi, A.P. Gerlich, Carbon 50 (2012) 4744–49.
Y. Morisada, H. Fujii, T. Mizuno, G. Abe, T. Nagaoka, M. Fukusumi, Surf. Coat. Technol. 204 (2010) 2459–64.
B. Zahmatkesh, M.H. Enayati, Mater. Sci. Eng. A 527 (2010) 6734–40.
K.J. Hodder, H. Izadi, A.G. McDonald, A.P. Gerlich, Mater. Sci. Eng. A., 2012, vol. 556, pp. 114–21.
E.A. El-Danaf, M.M. El-Rayes, M.S. Soliman, Mater. Des. 31 (2010) 1231–36.
P. Cavaliere, P.P. De Marco, Mater. Sci. Eng. A 462 (2007) 393–97.
Y. Sato, M. Urata, H. Kokawa, Metall. Mater. Trans. A 33A (2002) 625–35.
F.J. Humphreys, M. Hatherly, Recrystallization AND Related Annealing Phenomena, Elsevier, Amsterdam, 2004.
R.S. Mishra, Z.Y. Ma, Mater. Sci. Eng. R, 50, 2005, pp. 1–78.
A. Yazdipour, A. Shafiei, M.K. Dehghani, Mater. Sci. Eng. A, 527, 2009, 192–97.
A. Gerlich, M. Yamamoto, T.H. North, Metall. Mater. Trans. A 38 (2007) 1291–1302.
M. Grujicic, B. Pandurangan, C.F. Yen, B.A. Cheeseman, J. Mater. Eng. Perform., 32, 2011, 1–11.
J.D. Robson, L. Campbell, Sci. Technol. Weld. Joining 15 (2010) 171–76.
K. Chen, W. Gan, K. Okamoto, K. Chung, R.H. Wagoner, Metall. Mater. Trans. A 42 (2011) 488–507.
F.J. Humphreys, Acta Mater. 45 (1997) 5031–39.
S. Jana, R.S. Mishra, J.A. Baumann, G. Grant, Mater. Sci. Eng. A 528 (2010) 189–199.
I. Charit, R.S. Mishra, M.W. Mahoney, Scripta Mater. 47 (2002) 631–36.
K.A.A. Hassan, A.F. Norman, D.A. Price, P.B. Prangnell, Acta Mater. 51 (2003) 1923–936.
G. Ipekoğlu, G. Çam, Metall. Mater. Trans. A 45 (2014) 3074–87.
Y.S. Sato, H. Watanabe, H. Kokawa, Sci. Technol. Weld. Joining 12 (2007) 318–23.
M.A. Safarkhanian, M. Goodarzi, S.M.A. Boutorabi, J. Mater. Sci 44 (2009) 5452–58.
M.M. Attallah, H.G. Salem, Mater. Sci. Eng. A 391 (2005) 51–59.
H. Aydin, A. Bayram, I. Durgun, Mater. Des. 31 (2010) 2568–77.
Z. Zhang, B.L. Xiao, and Z.Y. Ma: Adv. Mater. Res., 2012, vol. 409, pp. 299–304.
S.J. Hales, W.A. Tayon: Como, vol 10, 2011, pp. 2496-2501.
T. Minton, J. Au: Key Eng. Mater., 2009, vol. 410–11, pp. 117-125.
D. Kim, H. Badarinarayan, J.H. Kim, C. Kim, K. Okamoto, R.H. Wagoner, K. Chung, Eur. J. Mech., A/Solids 29 (2010) 204–215.
E. Cerri: Mater. Sci. Forum, vol 683, 2011, pp. 249-54.
A. Goloborodko, T. Ito, X. Yun, Y. Motohashi, G. Itoh, Mater. Trans. 45 (2004) 2503–08.
I. Charit, R.S. Mishra, Scripta Mater. 58 (2008) 367–71.
M. Furukawa, Z. Horita, M. Nemoto, R.Z. Valiev, T.G. Langdon, Acta Mater. 44 (1996) 4619–29.
J. Wang, Y. Iwahashi, Z. Horita, M. Furukawa, M. Nemoto, R.Z. Valiev, T.G. Langdon, Acta Mater. 44 (1996) 2973–82.
V.L. Tellkamp, S. Dallek, D. Cheng, E.J. Lavernia, J. Mater. Res. 16 (2001) 938–44.
J. Wang, M. Furukawa, Z. Horita, M. Nemoto, R.Z. Valiev, T.G. Langdon, Mater. Sci. Eng. A 216 (1996) 41–46.
D.G. Morris, M.A. Muñoz-Morris, Acta Mater. 50 (2002) 4047–60.
G.E. Dietre, Mechanical Metallurgy, McGraw-Hill, New York, 1988.
Y.S. Sato, M. Urata, H. Kokawa, K. Ikeda, Mater. Sci. Eng. A 354 (2003) 298–305.
M.M. Attallah, C.L. Davis, M. Strangwood, J. Mater. Sci. 42 (2007) 7299–7306.
E. Huskins, B. Cao, K. Ramesh, Mater. Sci. Eng. A 527 (2010) 1292–98.
E. Hall, Proc. Phys. Soc., 64 (1951) 747.
N. Petch, J. Iron Steel Inst., 174 (1953) 25–28.
J. Zander, R. Sandström, L. Vitos, Comput. Mater. Sci. 41 (2007) 86–95.
Ø. Ryen, B. Holmedal, O. Nijs, E. Nes, E. Sjölander, H.-E. Ekström, Metall. Mater. Trans. A 37A (2006) 1999–2006.
M.P. Liu, H.J. Roven, M.Y. Murashkin, R.Z. Valiev, A. Kilmametov, Z. Zhang, Y. Yu, J. Mater. Sci. 48 (2013) 1–8.
J. Gubicza, N. Chinh, T. Csanadi, T. Langdon, T. Ungar, Mater. Sci. Eng. A 462 (2007) 86–90.
Y.S. Sato, S.H.C. Park, H. Kokawa, Metall. Mater. Trans. A 32 (2001) 3033–42.
Y. Sun, H. Fujii, N. Takaki, Y. Okitsu, Sci. Technol. Weld. Joining 16 (2011) 605–12.
K. Elangovan, V. Balasubramanian, Mater. Charact. 59 (2008) 1168–77.
K.N. Krishnan, J. Mater. Sci. 37 (2002) 473–80.
E. Cerri, P. Leo, Mater. Des. 32 (2011) 3465–75.
A. Simar, Y. Bréchet, B. De Meester, A. Denquin, C. Gallais, T. Pardoen, Prog. Mater. Sci. 57 (2012) 95–183.
Y.H. Yin, N. Sun, T.H. North, S.S. Hu, Mater. Charact., 61 (2010) 1018–28.
P.A. Colegrove, H.R. Shercliff, Sci. Technol. Weld. Joining 11 (2006) 429–41.
A. Gerlich, G. Avramovic-Cingara, T.H. North, Metall. Mater. Trans. A 37 (2006) 2773–86.
G. Gottstein, L.S. Shvindlerman, Grain Boundary Migration in Metals: Thermodynamics, Kinetics, Applications, CRC Press, Boca Raton, FL, 2010.
T.R. Malow, C.C. Koch, Acta Mater., 45 (1997) 2177–86.
C.B. Fuller, M.W. Mahoney, Metall. Mater. Trans. A 37 (2006) 3605–15.
R. Goswami, G. Spanos, P.S. Pao, R.L. Holtz, Mater. Sci. Eng. A 527 (2010) 1089–95.
J.S. Vetrano, S.M. Bruemmer, L.M. Pawlowski, I.M. Robertson, Mater. Sci. Eng. A 238 (1997) 101–07.
G.S. Frankel, Z. Xia, Corrosion 55 (1999) 139–50.
R. Verma, P.A. Friedman, A.K. Ghosh, S. Kim, C. Kim, Metall. Mater. Trans. A (1996) 1889–98.
M.M. Attallah, M. Strangwood, C.L. Davis, Scripta Mater. 63 (2010) 371–74.
W. Wen, Y. Zhao, J.G. Morris, Mater. Sci. Eng. A 392 (2005) 136–44.
R.W. Fonda, P.S. Pao, H.N. Jones, C.R. Feng, B.J. Connolly, A.J. Davenport, Mater. Sci. Eng. A 519 (2009) 1–8.
S.M. De La Puente, B. Verlinden, L. Delaey, J. Mater. Sci. 29 (1994) 6167–74.
P. Ratchev, B. Verlinden, P. Van Houtte, Acta Metall. Mater. 43 (1995) 621–29.
R.S. Mishra, M.W. Mahoney, Friction Stir Welding and Processing, ASM, Materials Park, Ohio, 2007.
J.Q. Su, T.W. Nelson, R. Mishra, M. Mahoney, Acta Mater. 51 (2003) 713–29.
D.H. Choi, B.W. Ahn, D.J. Quesnel, S.B. Jung, Intermetallics 35 (2013) 120–27.
R. Sandsttröm, Acta Metall. 25 (1977) 905–11.
W. Roberts, B. Ahlblom, Acta Metall. 26 (1978) 801–13.
A.A. Mazilkin, B.B. Straumal, E. Rabkin, B. Baretzky, S. Enders, S.G. Protasova, O.A. Kogtenkova, R.Z. Valiev, Acta Mater. 54 (2006) 3933–39.
D.A. Molodov, U. Czubayko, G. Gottstein, L.S. Shvindlerman, Mater. Sci. Forum, vol 217-222, 1996, pp. 523-528.
V.A. Ivanov: PhD Thesis, Institut für Metallkunde und Metallphysik, RWTH University Aachen, 2006.
J.C. Verhasselt, G. Gottstein, D.A. Molodov, L.S. Shvindlerman, Acta Mater. 47 (1999) 887–92.
Y. Huang, F.J. Humphreys, Mater. Chem. Phys. 132 (2012) 166–74.
N. Kamp, A. Sullivan, R. Tomasi, J.D. Robson, Acta Mater. 54 (2006) 2003–14.
W.F. Gale, T.C. Totemeier, Smithells Metals Reference Book, Elsevier Science, London, 2003.
S. Saimoto, J.I. Cooley, B.J. Diak, H. Jin, R.K. Mishra, Acta Mater. 57 (2009) 4822–34.
Acknowledgments
The authors would like to recognize the Natural Sciences and Engineering Council (NSERC) of Canada and Defence R&D Canada for financial assistant with this project. The authors also acknowledge Mojtaba Izadi for assistance with using Matlab, and Meysam Haghshenas and Saman Sahraeinejad for the help with temperature measurements.
Author information
Authors and Affiliations
Corresponding author
Additional information
Manuscript submitted February 17, 2014.
Rights and permissions
About this article
Cite this article
Izadi, H., Sandstrom, R. & Gerlich, A.P. Grain Growth Behavior and Hall–Petch Strengthening in Friction Stir Processed Al 5059. Metall Mater Trans A 45, 5635–5644 (2014). https://doi.org/10.1007/s11661-014-2492-x
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11661-014-2492-x