Abstract
In-situ phase transformation behavior of a high strength (830 MPa yield stress) quenched and tempered S690QL1 (Fe-0.16C-0.2Si-0.87Mn-0.33Cr-0.21Mo (wt pct)) structural steel during continuous cooling under different mechanical loading conditions has been studied. Time-temperature-load resolved 2D synchrotron diffraction patterns were recorded and used to calculate the phase fractions and lattice parameters of the phases during heating and cooling cycles under different loading conditions. In addition to the thermal expansion behavior, the effects of the applied stress on the elastic strains during the formation of bainite from austenite and the effect of carbon on the lattice parameter of bainitic ferrite were calculated. The results show that small tensile stresses applied at the transformation temperature do not change the kinetics of the phase transformation. The start temperature for the bainitic transformation decreases upon increasing the applied tensile stress. The elastic strains increase with increase in the applied tensile stress.
Similar content being viewed by others
References
NEN-EN 10025-6, Technical report November, 2004.
Blond R, Jimenez-Melero E, Zhao L,Wright JP, Brck E, van der Zwaag S, van Dijk NH (2012) Acta Materialia 60(2):565–577
Blond R, Jimenez-Melero E, van Dijk NH, Brck E, Zhao L, Sietsma J, van der Zwaag S (2011) Diffusion and Defect Data PtB: Solid State Phenomena 172(174):196–201
Offerman SE, van Dijk NH, Sietsma J, Lauridsen EM, Margulies L, Grigull S, Poulsen HF, van der Zwaag S (2006) Nuclear Instruments and Methods in Physics Research, Section B: Beam Interactions with Materials and Atoms 246(1):194–200
Offerman SE, van Dijk NH, Sietsma J, Grigull S, Lauridsen EM, Margulies L, Poulsen HF, Rekveldt MT, van der Zwaag S (2002) Science 298(5595):1003–1005
Dai H, Francis JA, Stone HJ, Bhadeshia HKDH, Withers PJ (2008) Metallurgical and Materials Transactions A: Physical Metallurgy and Materials Science 39(13):3070–3078
Stone HJ, Bhadeshia HKDH, Withers PJ (2008) Materials Science Forum 571(572):393–398
Taleb L, Cavallo N, Waeckel F (2001) International Journal of Plasticity 17:1–20
Bhadeshia HKDH (2004) Materials Science and Engineering A 378(1-2 SPEC ISS.):34–39
Withers PJ, Bhadeshia HKDH (2001). Materials Science and Technology 17(4):366–375
Dutta RK, Amirthalingam M, Hermans MJM, Richardson IM (2013) Materials Science and Engineering A 559:86–95
Dutta RK, Huizenga RM, Amirthalingam M, Hermans MJM, King A, Richardson IM (2013) Metallurgical and Materials Transactions A: Physical Metallurgy and Materials Science 44(9):4011–4014
J.C. Labiche, O. Mathon, S. Pascarelli, M.A. Newton, G.G. Ferre, C. Curfs, G. Vaughan, A. Homs, and D.F. Carreiras: Rev. Sci. Instrum., 2007, vol. 78 (9), p. 091301.
Hammersley AP, Svensson SO, Hanfland M, Fitch AN, Husermann D (1996) High Pressure Research 14(4-5):235–248
van Dijk NH, Butt AM, Zhao L, Sietsma J, Offerman SE, Wright JP, van der Zwaag S (2005) Acta Materialia 53(20):5439–5447
van Bohemen SMC, Sietsma J (2008) International Journal of Materials Research 99(7):739–747
van Bohemen SMC (2010) Metallurgical and Materials Transactions A: Physical Metallurgy and Materials Science 41(2):285–296
Pati SR, Cohen M (1969) . Acta. Metall.. Mater.. 17(3):189–199
van Bohemen SMC, Sietsma J (2010) Materials Science and Engineering A 527(24-25):6672–6676
Chester NA, Bhadeshia HKDH (1997) J Phys IV 7:41–46
van Bohemen SMC, Sietsma J (2009) Materials Science and Technology 25(8):1009–1012
Bhadeshia HKDH (1981) Metal Science 15(4):175–177
H.K.D.H. Bhadeshia: Bainite in Steels, 2nd ed., The Institute of Materials, London, 2001.
Koistinen DP, Marburger RE (1959) Acta Metallurgica 7(1):59–60
Babu SS, Specht ED, David SA, Karapetrova E, Zschack P, Peet M, Bhadeshia HKDH (2005) Metallurgical and Materials Transactions A: Physical Metallurgy and Materials Science 36(12):3281–3289
Dyson DJ, Holmes B (1970) J Iron Steel Inst (London) 208(pt 5):469–74
Bhadeshia HKDH, David SA, Vitek JM, Reed RW (1991) Materials Science and Technology 7(8):686–698
M. Amirthalingam, M.J.M. Hermans, R.M. Huizenga, S.E. Offerman, J. Sietsma, and I.M. Richardson: in In-Situ Studies with Photons, Neutrons and Electrons Scattering, T. Kannengiesser, S.S. Babu, Y. Komizo, A.J. Ramirez, eds., Springer, Berlin. ISBN 978-3-642-14793-7, 2010, pp. 133–48
Amirthalingam M, Hermans MJM, Zhao L, Richardson IM (2010) Metallurgical and Materials Transactions A 41:431–439
Barabash OM, Babu SS, David SA, Vitek JM, Barabash RI (2003) Journal of Applied Physics 94(1):738–742
de Cooman BC (2004) Current Opinion in Solid State and Materials Science 8(34):285–303
Wang J, van der Zwaag S (2001) Metallurgical and Materials Transactions A 32:1527–1539
Rees GI, Bhadeshia HKDH (1992) . Materials Science and Technology 8(11):985–993
N. Luzginova: Ph.D. Thesis, Delft University of Technology, 2008.
Coret M, Calloch S, Combescure A (2002) International Journal of Plasticity 18:1707–1727
Gautier E, Denis S, Liebaut C, Sjostrom S (1994) Journal De Physique IV : JP 4(3):279–284
Acknowledgments
This research is carried out under Project No. M32.8.09333 in the framework of the Research Program of the Materials innovation institute M2i http://www.m2i.nl. The authors thank Allseas Engineering by for providing the financial support for the project.
Author information
Authors and Affiliations
Corresponding author
Additional information
Manuscript submitted May 29, 2013.
Rights and permissions
About this article
Cite this article
Dutta, R.K., Huizenga, R.M., Amirthalingam, M. et al. In-Situ Synchrotron Diffraction Studies on Transformation Strain Development in a High Strength Quenched and Tempered Structural Steel—Part I. Bainitic Transformation. Metall Mater Trans A 45, 218–229 (2014). https://doi.org/10.1007/s11661-013-1992-4
Published:
Issue Date:
DOI: https://doi.org/10.1007/s11661-013-1992-4