There are many experimental studies in the literature that examine the occurrence of de-saturation (air-entry point) from the evolution of degree of saturation against suction typically obtained during air-drying of reconstituted (initially saturated) soil samples under unconfined (or very low) stress conditions (e.g. [18, 21, 57, 69, 75]). To include, in such experimental investigations, the influence that dry density (or plastic volumetric strain) has on the air-entry point, it is useful to conduct the same type of air-drying paths on several samples that have been previously pre-consolidated to different values of stress. On subsequent application of drying, the various saturated samples are expected to de-saturate at different air-entry values of suction because of the different initial stress histories. From these observations, the influence of dry density (or plastic volumetric strain) on de-saturation can be assessed.
Simulations of air-drying tests on OC samples of Barcelona clayey silt [13]
Boso [13] conducted a series of air-drying tests at a very low vertical stress on samples of reconstituted Barcelona clayey silt. This low-activity soil has 17% clay content and the following basic properties: liquid limit 32%, plastic limit 16% and unit weight of solids 26.7 kN/m3 [13]. The reconstituted samples had mono-modal pore size distributions [13]. Each sample was initially one-dimensionally consolidated (under saturated conditions) to a vertical effective stress \(\sigma ^{\prime }_{\text{v0}}\) of 100, 300 or 500 kPa, then unloaded to very low stress conditions and slightly reloaded to 14 kPa to accommodate the sample into a monitored suction shear box with high-range tensiometers [16], before conducting the air-drying path [68]. Several samples were tested with each value of saturated vertical pre-consolidation stress (100, 300 or 500 kPa), and the various samples within each group were finally air-dried to different values of suction.
The stress paths followed in these experimental tests are illustrated in Fig. 6. All stress paths start at the same saturated initial state A on the saturated 1D normal compression line (ncl). The initial very low stress is assumed equal to 1 kPa in the simulations of the tests presented later. The specific volume at this point thus corresponds to the intercept \(\bar{N}\) of the saturated 1D ncl because, at this stage, s = 0 kPa and the vertical net stress \(\bar{\sigma }_{\text{v0}}\), vertical saturated effective stress \(\sigma ^{\prime }_{\text{v0}}\) and vertical Bishop’s stress \(\sigma_{\text{v0}}^{ *}\) all have a value of 1 kPa. An initial vertical consolidation was simulated first, from A to the appropriate vertical effective stress \(\sigma ^{\prime }_{\text{v0}}\) at B, C or D (Fig. 6). After unloading each sample to the very low stress conditions at E, the simulations include a small reloading, as the vertical effective stress was increased from 1 to 14 kPa (as indicated by EF in Fig. 6). An air-drying path was subsequently simulated (at a constant stress of 14 kPa) to the final value of s at G (see Fig. 6). As expected, the different amounts of mechanical yielding experienced by the samples at B, C and D led to different values of suction at de-saturation (air-entry points) in both experiments and simulations.
The model parameter values used in the simulations are summarised in Table 1, where the upper bar indicates that they correspond to 1D loading (zero lateral strain), rather than isotropic loading. The intercept \(\bar{N}\) and gradient \(\bar{\lambda }\) of the saturated 1D ncl, together with the gradient \(\bar{\kappa }\) of a 1D unloading–reloading line (url), were determined from a saturated oedometric test on a reconstituted sample of Barcelona clayey silt that had been previously vertically consolidated to 100 kPa [13]. The simulation of this saturated test is presented in the v:\(\ln \sigma ^{\prime }_{\text{v}}\) plane in Fig. 7, where the experimental results are indicated by symbols.
Table 1 Values of soil constants for the model simulations for Boso [13] tests
The gradient \(\lambda_{\text{s}}\) of the main drying curve in the S
r
:lns* plane was estimated from the experimental evolution of S
r
observed during the initial stages of the drying paths presented in Fig. 8. In doing so, it was necessary to ensure that no plastic volumetric compression occurred during the section of retention response considered to estimate this gradient. This was a reasonable assumption for the first part of each drying path, because, as confirmed later, the high values of overconsolidation ratio OCR of all the reconstituted samples, immediately before drying, meant that the corresponding position of the M yield surface was far away from the current stress point and the decreases in S
r
during the initial stages of drying involved yielding on only the DR yield surface (with no plastic compression). Hence, the initial part of each test followed a constant \((\varepsilon_{\text{v}}^{\text{p}} )\) main drying curve.
The value of the soil constant \(\bar{k}_{2}\) was determined by examining the air-entry values of modified suction \(s_{e}^{*}\) for the three groups of tests corresponding to the three values of vertical pre-consolidation stress (100, 300 and 500 kPa). The experimental value of \(s_{e}^{*}\) for each value of vertical pre-consolidation stress was first determined by best-fitting the experimental data for the early part of the drying retention curves for the appropriate group of tests by a straight line of gradient \(\lambda_{\text{s}}\) in the S
r
:lns* plane (using the value of \(\lambda_{\text{s}}\) already determined) and then finding the intersection of this line with S
r
= 1. These three air-entry values \(s_{\text{e}}^{*}\) should be related to the vertical pre-consolidation stress \(\sigma ^{\prime }_{\text{v0}}\) through the equation of the de-saturation line (equivalent to Eq. 3, but with \(p^{\prime }_{0}\) replaced by \(\sigma ^{\prime }_{\text{v0}}\), to reflect the 1D conditions). The three pairs of values of \(s_{\text{e}}^{*}\) and \(\sigma ^{\prime }_{\text{v0}}\) were plotted in the ln \(s_{\text{e}}^{*}\):ln \(\sigma ^{\prime }_{\text{v0}}\) plane and the gradient of the best-fit straight line through these points was used to determine the value of \(\bar{k}_{2}\) (see Eq. 3).
The values of the three remaining soil constants R, \(\bar{N}^{*}\) and \(\bar{k}_{1}\) (see Appendix) were determined using an iterative procedure, intended to optimise the fit of the model simulations to the experimental variations of v and S
r
. This procedure made use of experimental data from the subsequent constant water content loading stages of Boso [13] (discussed in the next section) as well as the air-drying stages discussed in this section, because determination of a value for the model parameter R requires experimental data involving yielding on both WR and DR yield surfaces.
Table 2 provides details of the common initial state (prior to the saturated pre-consolidation stage) used for all model simulations, corresponding to point A in Fig. 9, lying on the saturated 1D ncl (Fig. 7). Hence, the initial value of the mechanical hardening parameter (defining the initial position of the M surface) was \(\sigma ^{\prime }_{\text{v0A}} = 1\;{\text{kPa}}\). Inserting this value into Eq. 3 of the de-saturation line (together with the appropriate model parameter values, see Table 1) gave the corresponding air-entry value of modified suction at A, which defines the initial position of the DR yield surface (\(s_{\text{eA}}^{*}\) in Fig. 9). Although not used in the simulations presented in this section, the initial position of the WR yield surface was also determined using \(s_{\text{exA}}^{*} = s_{\text{eA}}^{*} /R\), where \(s_{\text{exA}}^{*}\) is the air-exclusion at point A. The initial positions of the MW and MD curves introduced earlier, together with the saturation and de-saturation lines, are also included in Fig. 9 for completeness.
Table 2 Initial state for model simulations for Boso [13] tests
The experimental and simulated responses for the drying stress paths FG plotted in Fig. 6 are shown for the three different pre-consolidation stresses (100, 300 and 500 kPa) in Figs. 10, 11 and 12, respectively. The results in each of the three figures are presented in four parts. Part (a) shows the variation of matric suction s against vertical net stress \(\bar{\sigma }_{\text{v}}\) (the defined stress path, used as input for the simulations), whereas part (b) presents the variation of modified suction s* against vertical Bishop’s stress \(\sigma_{\text{v}}^{*}\). Parts (c) and (d) show, respectively, the evolution of specific volume v and of degree of saturation S
r
against \(\sigma_{\text{v}}^{*}\). All three examples start at the same initial state A on the saturated ncl, as illustrated in Figs. 7 and 9 (see also Table 2). In Figs. 10, 11 and 12, the continuous thicker line represents the model response on drying, whereas the dotted thicker line corresponds to the model response for the initial pre-consolidation stage (still under saturated conditions). Continuous thinner lines indicate the position of the M and DR yield surfaces just before drying (Figs. 10a, b, 11a, b, 12a, b) (this is difficult to see in Fig. 10a, b, because the elastic region is so small in this case). Note that for clarity the position of the WR surface is not included in the plots. The de-saturation line is indicated by a thick dashed line (Figs. 10a, b, 11a, b, 12a, b), and the positions of the MD curve at initial and final points of the air-drying simulation are indicated by lines with plain symbols (Figs. 10a, b, 11a, b, 12a, b).
As expected, mechanical yielding occurs throughout the initial saturated pre-consolidation stage AB, AC or AD (see Fig. 6) and the specific volume reduces, following the one dimensional saturated normal compression line (1D ncl), as illustrated in Figs. 10c, 11c and 12c. The occurrence of mechanical yielding on loading produces a coupled movement of the DR and WR surfaces to higher values of modified suction (increasing both air-entry and air-exclusion values of suction). The value of vertical Bishop’s stress (identical to vertical effective stress for these saturated conditions) at B, C or D defines the position of the M yield surface at the end of the pre-consolidation stage and also controls the positions of the DR and WR yield surfaces at this stage (Figs. 10b, 11b, 12b). During the subsequent elastic unloading and reloading paths applied just before drying (BEF, CEF or DEF; see Fig. 6) the positions of the three yield surfaces remain unchanged.
The increase in matric suction during the air-drying path (at constant vertical net stress) leads to increases in the vertical Bishop’s stress and modified suction (see Eqs. 1 and 2, respectively). The increase in \(\sigma_{\text{v}}^{*}\) during drying causes initial elastic compression in all three simulations. De-saturation then occurs where the DR yield surface is reached (see points X in Figs. 10a, b, 11a, b, 12a, b). Due to the different amounts of coupled movement of the DR yield surface at B, C or D (see Fig. 6), de-saturation is predicted at different values of modified suction in the three sets of tests. Not surprisingly, de-saturation occurs at higher values of modified suction (or matric suction) in the tests where greater mechanical yielding was experienced by the soil during the initial pre-consolidation (see Figs. 10a, b, 11a, b, 12a, b). This result is consistent with the experimental tests of Boso [13] and is in general agreement with the interpretation given by Tarantino [68].
The relatively high values of OCR at point F in all tests prevent the occurrence of mechanical yielding during the initial stage FX of drying, while the soil sample is still saturated (the saturated section of the MD curve at B, C or D is sufficiently far away from the stress point at F, and is consistently further away the larger was the applied vertical pre-consolidation stress \(\sigma ^{\prime }_{\text{v0}}\), see Figs. 10b, 11b, 12b, respectively). The variations of v during this initial stage of drying (when the soil is still saturated, up to point XB, XC or XD) follow an elastic unloading–reloading line in the v:\(\sigma_{\text{v}}^{*}\) plot (see Figs. 10c, 11c, 12c) because no mechanical yielding is predicted.
De-saturation occurs at X, and from X to Y, plastic decreases in S
r
are predicted as a consequence of yielding on only the DR surface. Note that, in all cases, the stress point is to the left of the de-saturation line at point X where de-saturation occurs (see Figs. 10b, 11b, 12b), because the soil is still in an overconsolidated state (not on the M yield surface) at this point (as discussed previously). The irreversible decrease in S
r
predicted by the model after point X matches reasonably well the experimental data, although some scatter exists in the experimental data (Figs. 10d, 11d, 12d).
Immediately after de-saturation, the increases in \(\sigma_{\text{v}}^{*}\) cause only elastic shrinkage (Figs. 10c, 11c, 12c), because the model predicts yielding on only the DR yield surface (the M yield surface has not yet been reached). Consequently, the evolution of S
r
initially follows a constant \((\varepsilon_{\text{v}}^{\text{p}} )\) main drying curve when plotted in the S
r
:s* plane, consistent with the earlier assumption adopted in the determination of λ
s (Fig. 8). The variation of v during this elastic shrinkage still follows the elastic unloading–reloading line in the v: \(\sigma_{\text{v}}^{*}\) plot, but is now able to pass beyond the saturated 1D ncl, because the soil is in an unsaturated condition (see Figs. 10c, 11c, 12c).
For the two simulations in which the drying path was conducted on specimens that experienced lower amounts of mechanical yielding during the pre-consolidation stage (Figs. 10c, 11c), the stress path reaches the current MD curve at Y (see Figs. 10b, 11b). This corresponds to reaching the M yield surface, and simultaneous plastic compression and plastic decreases in S
r
are therefore predicted for the remainder of the drying stage. The discontinuity of gradient in the predicted response of S
r
at Y (Figs. 10d, 11d) corresponds to this intersection and is consistent with previous comments on the influence of plastic compression on a main drying curve. This particular aspect of the predicted retention behaviour is illustrated more clearly in Fig. 8, where it can be seen that the simulations for the two drying paths conducted with lower pre-consolidation stresses converge at YC. Interestingly, this pattern of behaviour on drying would also have been observed beyond point YD for the final simulation (with the highest pre-consolidation stress) if the simulations for all dryings had been extended further (see Fig. 8). This is consistent with a number of experimental studies on retention behaviour available in the literature. In particular, Jotisankasa [34] and Jotisankasa et al. [35] observed a similar response when investigating various drying paths on a compacted silty clay for three different as-compacted states. On drying, the two tests subjected to lower compaction stresses converged first (i.e. at a lower value of suction), and all three converged later at a larger value of suction.
For the simulation of the tests performed with the highest value of pre-consolidation stress (see Fig. 12), the increase in suction during the air-drying path was not sufficient to reach the M yield surface (or, equivalently, the current position of the MD curve at D), as shown in Fig. 12b. Consequently, only elastic shrinkage was predicted throughout the drying (Fig. 12c), consistent with the variation of S
r
on a constant \((\varepsilon_{\text{v}}^{\text{p}} )\) main drying curve (see Fig. 8).
Simulations of air-drying tests on NC and lightly OC samples
All the air-drying tests of Boso [13] discussed above were performed on samples that were in a heavily overconsolidated state at the start of drying (OCR = 7.1, 21.4 or 35.7), with the initial stress state far inside the M yield surface. As a consequence, in all of the GCM simulations of Boso’s tests presented in Figs. 8, 9, 10, 11, and 12, the drying stress path reached the DR yield surface first, where the soil de-saturated, and only subsequently was the M yield surface reached. However, this will not always be the case, and for drying tests on samples that are normally consolidated or lightly overconsolidated at the start of drying, the DR and M yield surfaces will be reached in a different sequence. Examples of such drying tests on normally consolidated or lightly overconsolidated reconstituted soil samples include those reported by Vicol [75], Fleureau et al. [21] and Cunningham [17].
Figures 13 and 14 show GCM simulations of drying tests performed on a normally consolidated sample (Fig. 13) and a lightly overconsolidated sample (Fig. 14). The labelling in Figs. 13 and 14 follows the same system as used in Figs. 8, 9, 10, 11, and 12, with F representing the start of the drying stage, X the point of de-saturation (air-entry point) on the DR yield surface, Y the point of yielding on the M yield surface (onset of plastic shrinkage) and G the end of the drying stage. Also shown by a dashed line in Figs. 13a and 14a is the saturated 1D normal compression line (1D ncl).
For the normally consolidated sample shown in Fig. 13, mechanical yielding on the M surface occurs from the start of drying (Y′ coincides with F′) and de-saturation on the DR yield surface only occurs later, at X′ (see Fig. 13b). Between F′ and X′, the compression curve in Fig. 13a follows the saturated 1D ncl. For the lightly overconsolidated sample shown in Fig. 14, mechanical yielding on the M surface occurs at Y″, while the soil is still saturated, and de-saturation on the DR yield surface occurs later at X″. Between F″ and Y″, the compression curve in Fig. 14a follows an elastic unloading-reloading line (url), and between Y″ and X″, it follows the saturated 1D ncl. The GCM predictions shown in Figs. 13a and 14a are consistent with expected shrinkage behaviour for drying tests on normally consolidated or lightly overconsolidated reconstituted soil samples (e.g. [15, 70]) and match well the experimental behaviour reported by Vicol [75], Fleureau et al. [21], Marinho [42], Cunningham et al. [18], Tarantino et al. [69] and Al Haj and Standing [1].