Skip to main content
Log in

Hydrogen Effect on the Defect Structure Formation in the Zr – 1 WT.% Nb Alloy Under Pulsed Electron Beam Irradiation

  • Published:
Russian Physics Journal Aims and scope

Using the methods of X-ray structural analysis and electron and positron spectroscopy, it is found out that an irradiation of the surface of a Zr – 1 wt.% Nb specimen with an electron beam in the melting mode results in the formation of lamellar α+α′-structure, an increase in the dislocation density, a dissolution of the β-Nb phase, and the formation of defects of the vacancy-impurity type. The presence of hydrogen in the alloy irradiated with an electron beam favors the formation of complex hydrogen-vacancy complexes in the surface layer along with dislocations.

This is a preview of subscription content, log in via an institution to check access.

Access this article

Price excludes VAT (USA)
Tax calculation will be finalised during checkout.

Instant access to the full article PDF.

Similar content being viewed by others

References

  1. M. C. Li, S. Z. Hao, H. Wen, and R. F. Huang, Appl. Surf. Sci., 303, 350–353 (2014).

    Article  ADS  Google Scholar 

  2. Y. J. Liu, S. J. Li, H. L. Wang, et al., Acta Mater., 113, 56–67 (2016).

    Article  Google Scholar 

  3. I. P. Mishin, E. N. Stepanova, G. P. Grabovetskaya, et al., Izv. Vyssh. Uchebn. Zaved. Fiz., 55, No. 12/2, 224–227 (2012).

  4. X. D. Zhang, S. Z. Hao, T. Zou, et al., J. Metall., 2012, 762125 (2012).

  5. R. Zenker, Adv. Eng. Mater., 6, 581–588 (2004).

    Article  Google Scholar 

  6. J. X. Zou, K. M. Zhang, S. Z. Hao, et al., Thin Solid Films, 519, 1404–1415 (2010).

    Article  ADS  Google Scholar 

  7. N. S. Pushilina, A. M. Lider, V. N. Kudiyarov, and V. V. Krivosheina, Izv. Vyssh. Uchebn. Zaved. Fiz., 56, No. 11/3, 57–61 (2013).

  8. S. V. Ivanova, Int. J. Hydrog. Energy, 27, 819–824 (2002).

    Article  Google Scholar 

  9. L. D. Panteleev and V. M. Grigoriev, Dimensional Changes in Zirconium and its Alloys under Conditions of Reactor Irradiation. An analytical overview [in Russian], Preprint VNIIMN, Moscow (1976).

  10. G. G. Bondarenko, L. N. Bystrov, L. I. Ivanov, and Yu. M. Platov, Usp.Fiz.N auk, 116, No. 2, 303–314 (1975).

  11. J. Cizek, O. Melikhova, and I. Procházka, J. Alloys Compounds, 645, S312–S315 (2015).

  12. P. Hruška, J. Cizek, F. Lukáč, et al., Defect and Diffusion Forum, 373, 122–125 (2016).

  13. J. Cizek, I. Prochazka, S. Danis, et al., Phys. Rev. B: Condens. Matter, 79, 054108 (2009).

  14. N. N. Koval and Yu. F. Ivanov, Russ. Phys. J., 51, No. 5, 505–516 (2008).

    Article  Google Scholar 

  15. S. S. Gorelik, Yu. A. Skakov, and L. N. Rastorguev, X-Ray Diffraction and Electro-Optical Analysis [in Russian], MISIS, Moscow (2002).

  16. G. K. Williamson and R. E. Smallman, Phil. Mag., 1, No, 1 34–46 (1956).

  17. A. M. Lider, Positron Spectroscopy for Monitoring Structural Changes in the Metal-Hydrogen Systems, Thesis of Dr. Eng. Sci. 05.11.13, NR TPU, Tomsk (2017).

  18. R. Krause-Rehberg and H. S. Leipner, Positron annihilation in semiconductors: Defect studies, Springer Verlag, Berlin, Heidelberg (1999).

  19. J. M.C. Robles, E. Ogando, and F. Plazaola, J. Phys. Conf. Ser., 265, 012006 (2011).

  20. P. S. Chowdhury, P. Mukherjee, N. Gayathri, et al., Bull. Mater. Sci., 34, No. 3, 507–513 (2011).

  21. T. E.M. Staab, R. Krause-Rehberg, and B. Kieback, J. Mater. Sci., 34, 3833–3851 (1999).

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to I. P. Mishin.

Additional information

Translated from Izvestiya Vysshikh Uchebnykh Zavedenii, Fizika, No. 5, pp. 112–117, May, 2019.

Rights and permissions

Reprints and permissions

About this article

Check for updates. Verify currency and authenticity via CrossMark

Cite this article

Mishin, I.P., Grabovetskaya, G.P., Stepanova, E.N. et al. Hydrogen Effect on the Defect Structure Formation in the Zr – 1 WT.% Nb Alloy Under Pulsed Electron Beam Irradiation. Russ Phys J 62, 854–860 (2019). https://doi.org/10.1007/s11182-019-01787-9

Download citation

  • Received:

  • Revised:

  • Published:

  • Issue Date:

  • DOI: https://doi.org/10.1007/s11182-019-01787-9

Keywords

Navigation