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Homocondensation of acetylferrocene under ultrasonic conditions

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Abstract

The cyclocondensation of 1-acetylferrocene was studied in the presence of p-toluenesulfonic acid under ultrasonic conditions at 80 °C. The reaction was found to produce ethyl ferrocenoate along with 1,3,5-triferrocenylbenzene and 1,3-diferrocenylbenzene. The structure of ethyl ferrocenoate was studied by NMR spectroscopy and X-ray diffraction.

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Authors and Affiliations

  1. A. N. Nesmeyanov Institute of Organoelement Compounds, Russian Academy of Sciences, 28 ul. Vavilova, 119991, Moscow, Russian Federation

    R. A. Dvorikova & A. I. Kovalev

  2. National Research Center “Kurchatov Institute”, 1 ul. Akad. Kurchatova, 123182, Moscow, Russian Federation

    P. V. Dorovatovski

  3. Peoples’ Friendship University of Russia (RUDN University), 6 ul. Miklukho-Maklaya, 117198, Moscow, Russian Federation

    A. V. Mitrophanova & V. N. Khrustalev

  4. N. D. Zelinsky Institute of Organic Chemistry, Russian Academy of Sciences, 47 Leninsky prosp., 119991, Moscow, Russian Federation

    V. N. Khrustalev

Authors
  1. R. A. Dvorikova
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  2. P. V. Dorovatovski
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  3. A. V. Mitrophanova
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  4. V. N. Khrustalev
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  5. A. I. Kovalev
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Corresponding author

Correspondence to R. A. Dvorikova.

Additional information

Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 4, pp. 717–721, April, 2022.

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Dvorikova, R.A., Dorovatovski, P.V., Mitrophanova, A.V. et al. Homocondensation of acetylferrocene under ultrasonic conditions. Russ Chem Bull 71, 717–721 (2022). https://doi.org/10.1007/s11172-022-3471-9

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  • DOI: https://doi.org/10.1007/s11172-022-3471-9

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