Abstract
A reaction of triphenylantimony with 4-iodophenol in the presence of hydrogen peroxide furnished bis(4-iodophenoxy)triphenylantimony, which when treated with pentaphenylantimony gave 4-iodophenoxytetraphenylantimony. The structure of organoantimony compounds was studied by 1H and 13C NMR spectroscopy and X-ray crystallography.
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Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 3, pp. 0751—0755, March, 2016.
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Sharutin, V.V., Sharutina, O.K. & Senchurin, V.S. Synthesis and structure of bis(4-iodophenoxy)triphenylantimony and 4-iodophenoxytetraphenylantimony. Russ Chem Bull 65, 751–755 (2016). https://doi.org/10.1007/s11172-016-1368-1
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DOI: https://doi.org/10.1007/s11172-016-1368-1