Abstract
The condensation of 1-iodo-1,2,2-trifluoro-1,2-dichloroethane induced by granulated Zn in the presence of catalytic amounts of AcOEt without a solvent results in 1,2,3,4-tetrachlorohexafluorobutane in high yield.
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Published in Russian in Izvestiya Akademii Nauk. Seriya Khimicheskaya, No. 10, pp. 2236–2238, October, 2004.
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Karimova, N.M., Glazkov, A.A., Ignatenko, A.V. et al. Synthesis of 1,2,3,4-tetrachlorohexafluorobutane. Russ Chem Bull 53, 2336–2337 (2004). https://doi.org/10.1007/s11172-005-0125-7
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DOI: https://doi.org/10.1007/s11172-005-0125-7