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Acid Brown-14 preconcentration onto an adsorbent consisting of Fe3O4, carbon nanotube and CeO: optimized by a multi-variable method

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Abstract

This article describes an efficient method to preconcentrate Acid Brown-14 (AB-14) prior to its quantification by UV–Vis spectroscopy. A three-component nanocomposite (mCC) consisting of Fe3O4, carbon nanotube and CeO was synthesized in room temperature with environmentally-friendly materials. The characterization of materials was conducted according to X-ray diffraction, scanning electron microscopy and alternative gradient force magnetometer. AB-14 was adsorbed onto surface of CNT via π–π interaction. Additionally donating electron pairs of AB-14 into empty orbitals of cerium in CeO increased the mCC affinity to adsorb AB-14. Moreover, strong magnetic property of mCC facilitated the separation steps and decreased the preconcentration time. Plackett–Burman Design screened effective parameters on the preconcentration system and then Box–Behnken Design optimized the adsorption condition. These two experimental design methods decreased the adsorbent usage and time requiring finding the optimum conditions. The applicability of adsorbent was investigated with the respect to following figures of merit: (a) limit of detection of 0.50 μg L−1, (b) limit of quantification of 1.66 μg L−1, (c) relative standard deviation of 4.1%, (d) preconcentration factor of 25 and (e) linearity of dynamic range of 50–700 μg L−1. mCC is reusable for twelve cycles and durable for 90 days. Swelling behavior of mCC and adsorption mechanism were investigated. Isotherm, kinetic, and thermodynamic adsorptions were reported. Real samples of wool and silk were successfully applied to preconcentrate AB-14.

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Acknowledgements

Support for this study by the Research Council of the University of Tehran through grants is gratefully acknowledged.

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Authors and Affiliations

  1. School of Chemistry, College of Science, University of Tehran, P.O. Box 14155-6455, Tehran, Iran

    Mina Dana, Parastoo Jamshidi & Farzaneh Shemirani

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  1. Mina Dana
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  2. Parastoo Jamshidi
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  3. Farzaneh Shemirani
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Correspondence to Farzaneh Shemirani.

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Dana, M., Jamshidi, P. & Shemirani, F. Acid Brown-14 preconcentration onto an adsorbent consisting of Fe3O4, carbon nanotube and CeO: optimized by a multi-variable method. Res Chem Intermed 47, 1021–1032 (2021). https://doi.org/10.1007/s11164-020-04314-5

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