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Ultrasonic assisted preparation of nano-plate molybdenum(VI) coordination complex as a precursor for molybdenum trioxide nanoparticles preparation

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Abstract

In this work, a new nano-sized complex of molybdenum(VI) with the Schiff base ligand, [MoO2(C11H13NO3).(CH3OH)](1); C11H13NO3 = 2-methoxy-6-[(2-oxidopropyl)iminom-ethyl] phenolate, has been synthesized by ultrasonic irradiation and characterized by X-ray powder diffraction (XRD), IR and NMR spectroscopy. The crystallinity of nano-plate compound 1 was studied by XRD and compared with XRD simulation of the single crystal data. These nano-structures of compound 1 were obtained by sonochemical process. The molybdenum(VI) trioxide nano-particles were obtained by direct calcination of compound 1 as nano-structure at 673 K. The obtained molybdenum(VI) trioxides were characterized by X-ray diffraction and scanning electron microscopy.

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Acknowledgments

Supporting of this investigation by Shahid Bahonar University is gratefully acknowledged.

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Authors and Affiliations

  1. Department of Chemistry, Faculty of Sciences, Shahid Bahonar University, P.O. Box 76169-133, Kerman, Islamic Republic of Iran

    Zohreh Rashidi Ranjbar & Iran Sheikhshoaie

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  1. Zohreh Rashidi Ranjbar
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  2. Iran Sheikhshoaie
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Correspondence to Zohreh Rashidi Ranjbar.

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Ranjbar, Z.R., Sheikhshoaie, I. Ultrasonic assisted preparation of nano-plate molybdenum(VI) coordination complex as a precursor for molybdenum trioxide nanoparticles preparation. Res Chem Intermed 41, 955–963 (2015). https://doi.org/10.1007/s11164-013-1248-3

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