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Synthesis of 4-(2,2-dibromovinyl)phenol and its one-pot esterification

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Abstract

In situ treatment of 4-(2,2-dibromovinyl)phenol, which was prepared from 4-hydroxybenzaldehyde and carbon tetrabromide in CH2Cl2 under Corey–Fuchs conditions, with a diverse range of acids in the presence of dicyclohexylcarbodiimide (DCC) and 4-dimethylaminopyridine (DMAP) gave the corresponding esters in high yields.

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Acknowledgments

This work was supported by Program for Science & Technology Innovation Talents in Universities of He’nan Province (No. 2011HASTIT032), Foundation of He’nan Educational Committee (No. 2011C150001) and Foundation of He’nan Scientific and Technological Committee (No. 112300410236, 102300410181).

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Authors and Affiliations

  1. School of Biological and Chemical Engineering, Jiaozuo Teachers’ College, Shanyang Road 998, Jiaozuo, 450001, China

    Wensheng Zhang, Wenjing Xu, Jitao Li, Mei Liu & Wei Li

  2. Jiaozuo Vocational Education Center, Huayuan Road 57, Jiaozuo, 454001, China

    Fei Zhang

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  1. Wensheng Zhang
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  2. Wenjing Xu
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  3. Fei Zhang
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  4. Jitao Li
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  5. Mei Liu
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  6. Wei Li
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Correspondence to Wensheng Zhang.

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Zhang, W., Xu, W., Zhang, F. et al. Synthesis of 4-(2,2-dibromovinyl)phenol and its one-pot esterification. Res Chem Intermed 38, 957–964 (2012). https://doi.org/10.1007/s11164-011-0432-6

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  • DOI: https://doi.org/10.1007/s11164-011-0432-6

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