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Catalytic synthesis of 3-glycidoxypropyltriethoxysilane over silica-supported chitosan-platinum complex

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Abstract

An efficient and cost-effective method for the synthesis of 3-glycidoxypropyltriethoxysilane from the hydrosilylation reaction of allyl glycidyl ether with triethoxysilane using a silica-supported chitosan-platinum complex as catalyst is described for the first time. By an orthogonal experimental design method, the optimum parameters for the process were determined. The product yield can reach 78.9%, and the catalyst can be recovered and reused six times without noticeable loss of activity.

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Authors and Affiliations

  1. Henan Key Laboratory of Surface & Interface Science, Zhengzhou University of Light Industry, Zhengzhou, 450002, P.R.China

    Jianbo Zhao, Bing Xie, Guoqing Wang, Shiqiu Song & Yu’an Sun

Authors
  1. Jianbo Zhao
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  2. Bing Xie
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  3. Guoqing Wang
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  4. Shiqiu Song
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  5. Yu’an Sun
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Correspondence to Jianbo Zhao.

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Zhao, J., Xie, B., Wang, G. et al. Catalytic synthesis of 3-glycidoxypropyltriethoxysilane over silica-supported chitosan-platinum complex. React Kinet Catal Lett 96, 101–108 (2009). https://doi.org/10.1007/s11144-009-5360-8

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  • DOI: https://doi.org/10.1007/s11144-009-5360-8

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