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Oxide-Scale Evolution on a New Ni–Fe-Based Superalloy at High Temperature

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Abstract

The isothermal oxidation behavior and oxide-scale evolution on a newly developed Ni–Fe-based superalloy were investigated. Three oxidation stages were generally observed, an initial stage of rapid mass gain, then a second stage of parabolic kinetics, followed by an equilibrium period after about 50, 75, and 100 h at 1000, 1100, and 1200 °C, respectively. Cr2O3 and NiAl2O4 play an important role in protecting the matrix from oxidation at 1000 °C. The chromium supply becomes insufficient to support the continuously growing chromia scale with the increased oxidation temperature. Ultimately, the high-temperature oxidation resistance mainly depends on the formation of the inner continuous α-Al2O3 oxide layer. The quick formation of continuous α-Al2O3 oxide layer at 1200 °C compared to that at 1100 °C leads to a significantly reduced parabolic rate constant, which indicates that the new Ni–Fe-based superalloy has excellent oxidation resistance properties at higher temperatures.

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Acknowledgements

This work is sponsored by Shanghai Sailing Program [17YF1405800] of Shanghai Municipality and Prospective Joint Research Project of Department of Science and Technology of Jiangsu Province [BY2015068-01].

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Authors and Affiliations

  1. Key Laboratory for Microstructures, Institute of Materials, Shanghai University, Shanghai, 200072, China

    Huawei Zhang, Zhi Yang, Zhaoyu Wu, Xiaoyu Hong, Zhong Li, Yulai Xu, Jun Li & Xueshan Xiao

  2. Shanghai University Xinghua Institute of Special Stainless Steels, Xinghua, 225721, Jiangsu, China

    Xueshan Xiao

  3. Jiangsu SHENHONG Alloy Material Technology Co., Ltd., Taizhou, 225700, Jiangsu, China

    Xueshan Xiao

  4. Jinda Electric Appliance (Jiangsu) Co., Ltd., Taizhou, 225755, Jiangsu, China

    Gaojin Ni

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  1. Huawei Zhang
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  2. Zhi Yang
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  4. Xiaoyu Hong
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  5. Zhong Li
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  7. Jun Li
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Correspondence to Xueshan Xiao.

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Zhang, H., Yang, Z., Wu, Z. et al. Oxide-Scale Evolution on a New Ni–Fe-Based Superalloy at High Temperature. Oxid Met 92, 49–65 (2019). https://doi.org/10.1007/s11085-019-09913-1

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  • DOI: https://doi.org/10.1007/s11085-019-09913-1

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